1 SFUND RECORDS CTR
2222049
5. Sample Traffic Reports/ Chain-Of-Custody Records
23
2
** F C J A ^ ^ ^ • ' ^
Case No:
USEPA Contract Laboratory Program Inorganic Traffic Report & Chain of Custody Record
DAS No: SDG No:
^ Date Shipped: Carrier Name:
FedEx
Airbill:
793761083622
Shipped to:
Liberty Analytical Corporation 501 Madison Avenue Cary NC 27513 (919)379-4100
Sampler Signature:
Chain of Custody Record
7/26/2010
(Date / Time)
Relinquished B y
For Lab Use Only (Date / Time)
Received B y
!U/W/VVAa-6/>
/^UJ^9^7
Lab Contract No:
T^T\j?yilziho gqi,
Unit Price: Transfer To: Lab Contract No: Unit Price:
INORGANIC SAMPLE No.
MATRIX; SAMPLER
CONC/ TYPE
ANALYSIS/ TURNAROUND
TAG No7 PRESERVATIVH Bottles
SAMPLE COLLECT DATE/TIME
STATION LOCATION
MY71S3
Surface Water/ Tom Fortner
/G
TM/Hg (21)
211 (HN03)(1)
NIMM-SW-1
S: 7/22/2010
14:55
MY71S4
Surface Water/ Tom Fortner
/G
DM/Hg (21)
212 (HNOS) (1)
NIMM-SW-1-F
S: 7/22/2010
14:55
MY71S5
Surface Water/ Tom Fortner
/G
TM/Hg (21)
213 (HNOS) (1)
NIMM-SW-2
S: 7/21/2010
10:00
MY71S6
Surface Water/ Tom Fortner
/G
DM/Hg (21)
214 (HNOS) (1)
NIMM-SW-2-F
S: 7/21/2010
10:00
MY71S7
Surface Water/ Tom Fortner
/G
TM/Hg (21)
217 (HNOS) (1)
NIMM-SW-3
S: 7/21/2010
17:15
MY71S8
Surface Water/ Tom Fortner
/G
DM/Hg (21)
218 (HNOS) (1)
NIMM-SW-3-F
S: 7/21/2010
17:20
MY71S9
Surface Water/ Tom Fortner
/G
TM/Hg (21)
220 (HNOS) (1)
NIMM-SW-4
S: 7/22/2010
17:20
MY71T0
Surface Water/ Tom Fortner
/G
DM/Hg (21)
221 (HN03)(1)
NIMM-SW-4-F
MY71T1
Surface Water/ Tom Fortner
/G
TM/Hg (21)
NIMM-SW-5
S: 7/21/2010
17:00
Surface Water/ Tom Fortner
/G
NIMM-SW-5-F
S: 7/21/2010
17:00
MY71T2
Shi pment for Case Complete ?N
Analysis Key:
DM/Hg (21)
•^
MY71M1, MY71M9, MY71P9, MY71T1, MY71T5, MY71T6 Concentration: L = Low, M = Low/Medium, H = High
Additional Sampler Signature(s):
Type/Designate:
Composite = C, Grab = G
Cooler Temperature Upon Receipt:
S M Of) I J
DM/Hg = CLP TAL Dissolved Metals/Hg, TM/Hg = CLP TAL Total Metals/Hg
TR Number:
FOR LAB USE ONLY Sample Condition On Receipt
•-yiif^
\ jij-
224(HN03)(1)
Sample(s) to be used for laboratory QC:
ORGANIC SAMPLE No.
ORIGINS Chain of Custody Seal Number: .
Custody Seal Intact?
v 7 Shipment Iced?
¥
9-401709578-072610-0001
PR provides preliminary results. Requests for preliminary results will increase analytical costs. Send Copy to: Sample Management Office, Attn: Heather Bauer, CSC, 15000 Conference Center Dr, Chantilly, VA 20151-3819; Phone 703/818-4200; Fax 703/818-4602
F2V5.1.047 Page 6 Of 9
3
SERA Date Shipped:
7/26/2010
Carrier Name:
FedEx
Airbill:
793761083622
Shipped to:
CaseNo:
USEPA Contract Laboratory Program Inorganic Traffic Report & Chain of Custody Record Chain o f Custody Record Relinquished By
(Date / Time)
1 Liberty Analytical Corporation 501 Madison Avenue Cary NC 27513 (919) 379-4100
Sampler Signature: Received By
f
ir^
For Lab Use Only (Date / Time)
Lab Cont ract No:
•^^^l|to o q i S
Unit Pric 5:
MY71T3
3
CONC/ TYPE
ANALYSIS/ TURNAROUND
Surface Water/ Tom Fortner
/G
TM/Hg (21)
226 (HNOS) (1)
NIMM-SW-6
DM/Hg (21)
227(HN03)(1)
MY71T5
Surface Water/ Tom Fortner
/G
TM/Hg (21)
228(HN03), 229(HN03)
MY71T6
Surface Water/ Tom Fortner
/G
DM/Hg (21)
230 (HNOS), 231 (HN03)
MY71T7
Surface Water/ Tom Fortner
/G
TM/Hg (21)
MY71T8
Surface Water/ Tom Fortner
/G
MY71T9
Surface Water/ Tom Fortner
MY71W0
SAMPLE COLLECT DATEfTIME
STATION LOCATION
TAG NoJ PRESERVATIVH Bottles
/G
S: 7/21/2010
S: 7/21/2010
16:25
NIMM-SW-7
S: 7/21/2010
15:05
NIMM-SW-7-F
S: 7/21/2010
15:05
234(HN03)(1)
NIMM-SW-8
S: 7/22/2010
12:15
DM/Hg (21)
235 (HNOS) (1)
NIMM-SW-8-F
S: 7/22/2010
12:15
/G
TM/Hg (21)
257(HN03)(1)
NIMM-SW-9
S: 7/22/2010
13:55
Surface Water/ Tom Fortner
/G
DM/Hg (21)
237 (HNOS) (1)
NIMM-SW-9-F
S: 7/22/2010
13:55
MY71W1
Surface Water/ Tom Fortner
/G
TM/Hg (21)
238 (HNOS) (1)
NIMM-SW-10
S: 7/22/2010
11:45
MY71W2
Surface Water/ Tom Fortner
/G
DM/Hg (21)
239 (HNOS) (1)
NIMM-SW-10-F
S: 7/22/2010
| FOR LAB USE ONLY Sample Condition On Receipt
.y
(2)
:X.r:^
1
/
(2) ywi5//^£.
/
^^t>|^^SD
/
1 /
Sample(s) to be used for laboratory QC:
Additional Sampler Slgnature(s):
MY71M1, MY71M9, MY71P9, MY71T1, MY71T5, L= Low, M = Low/Medium, H = High
"••'' O R G K
Cooler Temperattire Upon Receipt:
niiMAn
Misz-ri-rc
Type/Designate:
Composite = C, Grab = G
^ M O O l ^
DM/Hg = CLP TfivL Disso Ived Metals/Hg, TM/Hg = CLP TAL Total Metals/Hg
TR Number:
ORGANIC SAMPLE No.
16:25
NIMM-SW-6-F
Concentration:
i/fcoo&ii/]
Unit Price:
MATRIX/ SAMPLER
Surface Water/ Tom Fortner
Analysis Key:
m i i 5 ( ^
Lab Cont ract No:
MY71T4
Shi pment for Case Complete ?N
,^/
Transfer To:
4 INORGANIC SAMPLE No.
,
SDONo: f ^ ^ r i l ^ ^
Qt'ww.^T^MA
2
40334
DAS NO: rY\^7i55 / n V l l - ^ ^ 1
ALI^
Chain of Custody Seal Number: V
Custody Seal Intact?
±
~~
~
Shipment Iced?
\ 7 1
9-401709578-072610-0001
PR provides preliminary results. Requests for preliminary results v^ill increase analytical costs. Send Copy to: Sample Management Office, Attn: Heather Bauer, CSC, 15000 (Conference Center D r , Chantilly, VA 20151-3819; Phone 703/818-4200; Fax 703/818-4602
F2V5.1.047 Page 7 Of 9
1
^ F P A ^ ^ ^ " '^^
4
USEPA Contract Laboratory Program Inorganic Traffic Report & Chain of Custody Record
Date Shipped:
7/26/2010
Carrier Name:
FedEx
Airbill:
793761083622
Shipped to:
Liberty Analytical Corporation 501 Madison Avenue Cary NC 27513 (919)379-4100
Chain o f Custody Record
Sampler Signature:
Relinquished By
Received By
(Date / Time)
CaseNo:
,
40334
,tA\lnie^/
^
DAS NO: MN7155 m l l S ^ i
- - m\%iit)mv(ifi/)m/i
^
For Lab Use Only
4Z/Vw>.^H'kys
(Date / Time)
Lab Contract No:
'ptiUA ilzilio m
Unit Price:
^
Transfer To: Lab Contract No: Unit Price:
MATRIX/ SAMPLER
CONC/ TYPE
ANALYSIS/ TURNAROUND
MY71W5
Surface Water/ Tom Fortner
/G
TM/Hg (21)
242 (HNOS) (1)
NIMM-SW-12
S: 7/21/2010
14:05
MY71W6
Surface Water/ Tom Fortner
/G
DM/Hg (21)
243 (HNOS) (1)
NIMM-SW-12-F
S: 7/21/2010
14:05
MY71W9
Surface Water/ Tom Fortner
/G
TM/Hg (21)
246 (HNOS) (1)
NIMM-SW-14
S: 7/21/2010
12:00
MY71X0
Surface Water/ Tom Fortner
/G
DM/Hg (21)
247 (HNOS) (1)
NIMM-SW-14-F
S: 7/21/2010
12:00
MY71X1
Surface Water/ Tom Fortner
/G
TM/Hg (21)
250 (HNOS) (1)
NIMM-SW-15
S: 7/21/2010
18:05
MY71X2
Surface Water/ Tom Fortner
/G
DM/Hg (21)
251 (HNOS) (1)
NIMM-SW-15-F
S: 7/21/2010
18:05
MY71X3
Surface Water/ Tom Fortner
IQ
TM/Hg (21)
253(HN03)(1)
NIMM-SW-16
S: 7/21/2010
8:05
'MY71X4-
SurfQOG Water
/IJ
r i M / H J T ? I)
- 3 C J L ( l - I M m \ [Mf..-
-MrHM^..
'> 7lM-U^^L»
MY71X5
Surface \Nater/ Tom Fortner
/G
TM/Hg (21)
255 (HNOS) (1)
NIMM-SW-17
S: 7/23/2010
18:05 5 ^ ® ' * * n
MY71X6
Surface Water/ Tom Fortner
/G
TM/Hg (21)
258 (HNOS) (1)
BLM-SW-1
S: 7/22/2010
15:25
INORGANIC SAMPLE No.
Shipment forCase Complete'iN
Analysis Key:
TAG NoJ PRESERVATIVH Bottles
Sample(s) to be used for laboratory QC: MY71M1, MY71M9, MY71P9, MY71T1, MY71T5, MY71T6 Concentration: L = Low, M = Low/Medium, H = High
•
STATION LOCATION
SAMPLE COLLECT DATEH'IME
Additional Sampler Signature(s):
Type/Designate:
Composite = C, Grab = G
.
ORGANIC SAMPLE No.
" =
Cooler Temperattire Upon Receipt:
Ih<
N \ f) 0 I ^ ^
DM/Hg = CLP TAL Dissolved Metals/Hg, TM/Hg = CLP TAL Total Metals/Hg
TR Number:
9-401709578-072610-0001
FOR LAB USE ONLY Sample Condition On Receipti
ORIGINA Chain of Custody Seal Number:
Custody Seal Intact?
3
Shipment Iced?
W-
m[B©^^T®^¥ €@\PY
PR provides preliminary results. Requests for preliminary results will increase analytical costs. Send Copy to: Sample Management Office, Attn: Heather Bauer, CSC, 15000 Conference Center D r , Chantilly, VA 20151-3819; Phone 703/818-4200; Fax 703/818^602
F2V6.1.047 Page 8 o f 9
5
^EPA Date Shipped:
7/26/2010
Carrier Name:
FedEx
Airbill:
793761083622
Shipped to:
Liberty Analytical Corporation 501 Madison Avenue Cary NC 27513 (919)379-4100
Chain of Custody Record
Sampler Signature:
Relinquished By
Received By
(Date / Time)
40334
Case No:
USEPA Contract Laboratory Program Inorganic Traffic Report & Chain of Custody Record
Ill3lp\
^^T 55
DAS No: SDG No:
^
For Lab Use Only (Date / Time)
g^(j0O866l
Lab Contract No:
'lA/^yy^VAjy^ Ziiho 0'\ \<;
Unit Price:
__
Transfer To: Lab Contract No: Unit Price:
INORGANIC SAMPLE No.
MATRIX/ SAMPLER
CONC/ TYPE
ANALYSIS/ TURNAROUND
TAG NoJ PRESERVATIVH Bottles
SAMPLE COLLECT DATHTIME
STATION LOCATION
MY71X7
Surface Water/ Tom Fortner
/G
DM/Hg (21)
259 (HNOS) (1)
BLM-SW-1-F
S: 7/22/2010
15:25
MY71X8
Surface Water/ Tom Fortner
/G
TM/Hg (21)
260 (HNOS) (1)
BLM-SW-2
S; 7/22/2010
15:47
MY71X9
Surface Water/ Tom Fortner
/G ,
TM/Hg (21)
102(1)(;M^iO3)
BLM-SW-2-F
S: 7/22/2010
15:47
MY71Y0
Surface Water/ Tom Fortner
/G
TM/Hg (21)
262(HN03)(1)
BLM-SW-3
S: 7/22/2010
16:02'^
MY71Y1
Surface Water/ Tom Fortner
/G
DM/Hg (21)
263(HN03)(1)
BLM-SW-3-F
S: 7/22/2010
16:02
ORGANIC SAMPLE No.
FOR U B USE ONLY Sample Condition On Receipti
^w
ORIGINAL Shi pment for Case Complete TN
Analysis Key:
Sample(s) to be used for laboratory QC: MY71M1, MY71M9, MY71P9, MY71T1, MY71T5, MY71T6 Concentration: L = Low, M = Low/Medium, H = High
Additional Sampler Signature(s):
Type/Designate:
Composite = C, Grab = G
Cooler Temperature Upon Receipt:
C N J ^ D \ ^ ^ Custody Seal Intact?
DM/Hg = CLP TAL Dissolved Metals/Hg, TM/Hg = CLP TAL Total Metals/Hg
TR Number:
9-401709578-072610-0001
Chain of Custody Seal Number:
3!
Shipment Iced?
2
m[E®^/aT®[R¥ (SO[P¥
PR provides preliminary results. Requests for preliminary results v^ill increase analytical costs. Send Copy to: Sample Management Office, Attn: Heather Bauer, CSC, 15000 Conference Center D r , Chantilly, VA 20151-3819; Phone 703/818-4200; Fax 703/818-4602
F2V5.1.047 Page 9 of 9
6
g^\^ fompufhem A Divijiaii Of
Lib erty Anjdy tical Corp., 8/16/2010 GARRETT PETERSON USEPA Region IX 1337 South 46th Street Bldg. 201 Richmond, CA 94804
Attention:
GARRETT PETERSON
Re: EPA Contract*
EPW08067
Subject: Report of Data - Case #:
40334
SDG#: MY71S3
Dear GARRETT PETERSON Enclosed are the results of analysis performed in accordance with the referenced contract. The analytical data contained in this report are associated with field samples belonging to Case Number 40334 If you have any questions regarding this data package, please contact Joan Purdie at (919) 379-4081 or Bob Meierer at (919) 379-4004. Sincerely,
iuLJudLcj2_3 Compuihem a division of Liberty Analytical Corporation
Report Preparation Attachment
7
CompuChem, a division of Liberty Analytical Lab ID
Client ID
WorkOrder
Matrix
Account
Project
1007157-01
MY71S3
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-02
MY71S5
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-03
MY71S7
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-04
MY71S9
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-05
MY71T1
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-06
MY71T3
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-07
MY71T5
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-08
MY71T7
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-09
MY71T9
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-10
MY71W1
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-11
MY71W5
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-12
MY71W9
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-13
MY71X1
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-14
MY71X3
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-15
MY71X5
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-16
MY71X6
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-17
MY71X8
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
1007157-18
MY71Y0
1007157
W
EPA
NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT
8/16/2010
8
. ..••'JS''-.W^'
...
"ii-t"V%V '
*
».
•f
CompuChcMi I Divibion of L»bprt\ Amiyticjl rorpontion«. ''
L
^'^
The sample data package shall include data for all analyses of all samples In one Sample Delivery Group (SDG), including field and analytical samples, reanalyses, blanks, spikes, duplicates, and laboratory control samples. The sample data package consists of the following:
A. Cover Documentation B. Sample Data
LAB CODE : LIBRTY
CONTRACT # : EPW08067
CASE # :
SDG # :
40334
MY71S3
•
"ii
9
A.
Cover Documentation 1. Cover Page 2. SDG Narrative 3. Sample Log-In Sheet (Form DC-1) 4. Full Inorganic Complete SDG File (CSF) Inventory Sheet (Form DC-2) 5. Sample Traffic Reports/ Chain-Of-Custody Records
10
1. Cover Page Inorganic Analyses Data Package The Cover Page includes laboratory information, the Case and SDG numbers, Non-Routine Analytical Service (NRAS) number (if appropriate), the EPA sample numbers in alphanumeric order showing the EPA sample numbers cross-referenced with Lab ID numbers, and completion of the questions on the use of background and interelement correction for the samples.
11
US EPA - CLP COVER PAGE
L a b Name:
COMPUCHEM
Lab Code:
LIBRTY
SOW N o . :
ZLM05.4
Contract: Case No:
40334
SDC3 N o :
NRAS N o . :
EPA S a m p l e N o .
Lab S a m p l e
MY71S3 MY71S5 MY71S7 MY71S9 My71Tl MY71T3 MY71T5 MY71T5D My71T5D MY71T5S My71T5S MY71T7 MY71T9 MY71W1 My71W5 MY71W9 MY71X1 MY71X3 MY71X5 MY71X6
1007157-01 1007157-02 1007157-03 1007157-04 1007157-05 1007157-06 1007157-07 0081015-DUPl 0072822-DUPl 0081015-MSl 0072822-MSl 1007157-08 1007157-09 1007157-10 1007157-11 1007157-12 1007157-13 1007157-14 1007157-15 1007157-16
W e r e ICP-AES a n d ICP-MS I n t e r e l e m e n t applied? Were ICP-AES a n d ICP-MS b a c k g r o u n d applied?
corrections
corrections
If yes/ were raw d a t a g e n e r a t e d b e f o r e a p p l i c a t i o n of b a c k g r o u n d c o r r e c t i o n s ? Comment s :
EPWO8067 MY71S3
ID
ICP-AES
ICP-MS
(Yes/No)
YES
NO
(Yes/No)
YES
NO
(Yes/No)
NO
NO
THE FOLLOWING ANALYTES HAVE BEEN FLAGGED WITH AN " E " TO INDICATE SERIAL DILUTION RESULTS W H I C H ARE NOT V I T H I N CONTROL LIMITS: POTASSIUM
I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package and in the computer-readable data submitted on diskette (or via an altemate means of electronic transmission, if approved in advance by USEPA) has been authorized by the Laboratory Manager or the Manager's designee, as verified by the following signature.
Signature:
Date;
<6 Av^ A ^
Name:
Susan W Bass
Title:
Senior
COVER PAGE
Chemist
ILM05.4
12 u s EPA - C L P
COVER PAGE
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
SOW N o . :
ILMO 5 . 4
Contract: Case No:
40334
EPWO8067
NRAS N o . :
EPA S a n p l e N o .
SDG N o :
My71S3
Lab Sample ID
MY71X8 MY71Y0
1007157-17 1007157-18
ICP-J^S
ICP-MS
Were ICP-AES and ICP-MS interelement corrections applied?
(Yes/No)
YES
NO
Mere ICP-AES and ICP-MS background corrections applied?
(Yes/No)
YES
NO
(Yes/No)
NO
NO
If yes, were raw data generated before application of background corrections? Comments:
THE FOLLOWING ANALYTES HAVE BEEN FLAGGED WITH AN " E " TO INDICATE SERIAL DILUTION RESULTS WHICH ARE NOT WITHIN CONTROL LIMITS: POTASSIUM
I c e r t i f y t h a t t h i s d a t a package i s i n compliance w i t h t h e terms and c o n d i t i o n s of t h e c o n t r a c t , b o t h t e c h n i c a l l y and for completeness, f o r o t h e r t h a n t h e c o n d i t i o n s d e t a i l e d above. Release of t h e d a t a c o n t a i n e d i n t h i s hardcopy d a t a package and i n t h e c o m p u t e r - r e a d a b l e d a t a submitted on d i s k e t t e (or v i a an a l t e m a t e means of e l e c t r o n i c t r a n s m i s s i o n , i f approved i n advance by USEPA) h a s been a u t h o r i z e d by t h e L a b o r a t o r y Manager or t h e Manager's d e s i g n e e , a s v e r i f i e d by t h e f o l l o w i n g s i g n a t u r e .
Signature:
Date:
\fVU3C^^^^J^ \ ^ J ^ ^ y m / ^ y W
\^ I v ^ ^ Y
Name:
Susan W Bass
Title:
Senior
COVER PAGE
Chemist I LMO 5 . 4
13
2. SDG Narrative The SDG Narrative contains laboratory information, the Case and SDG numbers, contract number, and detailed documentation of any QC, sample, shipment, and/or analytical problems encountered in processing the samples. This will include any technical and administrative problems encountered and the resolution or corrective actions taken. The SDG Narrative will also document the alternative means of determining the cooler temperature when a cooler's temperature indicator bottle is absent. The SDG Narrative also provides equations or curves and utilizes raw data from the SDG being reported to demonstrate how sample results are obtained from raw instrument output. The SDG Narrative also includes a discussion of any flexibility Statement of Work (SOW) modification, including attaching a copy of the USEPA approved modification form to the SDG Narrative. Finally, the SDG Narrative will identify and explain any differences between results being provided in the data package and those provided previously as Preliminary Results.
14
CompuChem a Division ofLiberty Analytical Corp. 501 Madison Avenue Ory, NC 27513
SDG N A R R A T I V E CASE #40334 SDG # MY71S3 CONTRACT # EPW08067
The indicated Sample Delivery Group (SDG) consisting of eighteen (18) water samples was received on July 27, 2010. The samples were intact and in good condition with Chain of Custody (COC) Records. In accordance with previous direction from Region 9, the laboratory will note that the region does not require sample tags in the SDG Nairative, and proceed vvith the analysis of the samples. S A M P L E IDs: The following customer IDs are associated with this SDG:
MY71S3, MY71S5, MY71S7, MY71S9, MY71T1, MY71T3, MY71T5, MY71T7, MY71T9, MY71 Wl, MY71W5, MY71W9, MY71X1, MY71X3, MY71X5, MY71X6, MY71X8,MY71Y0 The samples were prepared and analyzed, in accordance with EPA - CLP Statement of Work (SOW) document ILM05.4 for the requested ICP-AES metals and mercury. The cooler temperature indicator bottle was found with the samples, and the sample's temperature was 0.1 to 4.3 degrees Celsius. Temperature was recorded by IR temperature gun.
EQUATIONS FOR LIQUID SAMPLE CALCULATIONS: Equation for obtaining metals sample results in |.ig/L as presented on FORM I data sheets from ICP instrument acquired results in |ig/L (ppb). C X . F I Where C = concentration
(^ig/L)
F = final volume in liters after sample preparation I = initial volume in liters Example: Calcium result in |ig/L from sample MY71S3 1318.246 fig/L (C) X 0.05 L (F) = 1318.2 ^g/L reported as 1320 J iigfL 0.05 L (1)
15
Equation for obtaining mercury sample results in |ig/L as presented on FORM I data sheets from instrument acquired results in pg/L (ppb).
C X D
X
F
I Where C = concentration (ng/L) Hg D = dilution factor to bring sample into analysis range F = final volume in liters (0.1 L) I = initial volume in liters Example: Mercury result in Ug/L
0.084 ng/L(C) X 1 (D)xO.l (F) • 0.084 ng/L reported as 0.084 J pg/L 0.1 L(I)
INSTRUMENTAL QUALITY CONTROL: All calibration verification solutions (ICV, CCV, & CRl), blanks (ICB, & CCB), and interference check samples (ICSA & ICSAB) associated with this data were confirmed to be within EPA CLP allowable limits. SAMPLE PREPARATION QUALITY C O N T R O L : The sample preparation procedure verifications (LCSW & PBW) were found to be witiiin acceptable ranges and the field samples were prepared and analyzed within the contract specified holding limes. MATRIX RELATED QUALITY CONTROL: The ICP sample matrix spike, CCN = 0072821-MSI (MY71T5S) was found to be inside CLP control limits. The mercury sample matrix spike, CCN= 0072822-MSl (MY71T5S) was found to be inside CLP control limits. The ICP sample matrix duplicate, CCN = 0072821-DUPI (MY71T5D) was found to be inside CLP control limits. The mercury sample matrix duplicate, CCN= 0072822-DUPl (MY71T5D) was found to be inside CLP control limits. A five-fold serial dilution of sample, CCN = 1007157-07 (MY71T5L) was performed m accordance with CLP requirements for ICP analysis. The adjusted sample concentrations were inside CLP control limits except potassium.
8
16
The laboratory manager or his designee, as verified by the following signature has authorized release ofthe data contained in this hard copy data package. Susan W. Bass Senior Chemist August 15,2010
Ol
17
Pagel of8
Joan Purdie From:
Blackmon, Jacqueline [
[email protected]]
Sent:
Wednesday, July 28, 2010 11:51 AM
To:
Cathy Dover; Diane Byrd; Joan Purdie; Kenneth Grzybowski
Cc:
[email protected]
Subject:
Region 09 | Case 40334 ( Lab LIBRTY 1 Issue Multiple | FINAL
Attachments: 40334-07-27-10.pdf Joan, ***Sumnnary Start"* -Discrepancies with tags, jars, and/or TR/COCIssue 1: Sannple MY71X9 is listed on the TR/COC as TM, but labeled as DM. Resolution 1: Per Region 9, this sample has been field filtered. The laboratory will note the issue in the SDG Narrative and proceed with the analysis of the samples. Issue 2: The TR/COC lists the analysis as DM for the water samples; however per scheduling, water samples are for unfiltered ICP-AES (Al, Ca, Fe, Mg, K, Na); ICP-MS (Sb, As. Ba, Be. Cd, Cr, Co, Cu, Pb, Mn, Ni, Se, Ag, Tl, V, Zn); and Hg analysis. Can you please confirm that these samples are not dissolved? Resolution 2: Per Region 9, some samples (designated with the letter "F" in the station location) have been field filtered. Please analyze these samples for the exact same parameters as were originally scheduled. The laboratory will note the issue in the SDG Narrative and proceed with the analysis ofthe samples. SMO should schedule 15 water samples for dissolved metals analysis. Issue 3: Only one TFl/COC out of the nine are signed under the "Relinquished By" section. Resolution 3: Per Region 9, the laboratory will note the issue in the SDG Narrative and proceed with the analysis of the samples. issue 4: The matrix for samples MY71L5, -L6, -L7,-L8,-L9, -MO, - M l , -M2 and - M 3 is listed as "Other" on the attached TF^COC. The laboratory stated that these samples resemble soil samples. Please advise if SMO should schedule an additional matrix for these samples, or if these are in fact soil samples. Resolution 4: Per Region 9, these are soil samples. The laboratory will note the issue in the SDG Narrative and proceed with the analysis of the samples. -pH outside allowable limitsIssue 5: Samples MY71X5 and MY71Y1 were both received with ph of 7, which is above the required level. Resolution 5: In accordance with previous direction from Region 9, the laboratory will note the issue in the SDG Narrative, adjust the pH, and proceed with the analysis of the sample. The resolution will be applied to all samples received for this Case with a pH outside of allowable limits. -Insufficient/inappropriate designation of laboratory QCIssue 6: Sample MY71T1 is designated on the TFVCOC for laboratory QC; however samples MY71T5 and MY71T6 are also designated on the TRJCOC for laboratory QC. The lab would like to use sample MY71T5 as QC for TM—AES.MS and sample MY71T6 as QC for DM—AES.MS for the water samples, and not sample MY71T1. Resolution 6: Per Region 9, samples MY71T5 and MY71T6 are acceptable to use as laboratory QC. Sample MY71T1 does not need to be used for lab QC. The laboratory will note the issue in the SDG Narrative and proceed with the analysis of the samples.
10 7/28/2010
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Page 2 of 8
-Return airbill information missing/incompleteissue 7: There is no return information for the coolers. Please provide a contact, third party account, return address, and phone number so that the coolers can be returned. Resolution 7: Per Region 9, the coolers do not need to be returned to the samplers. ***Summary End*** Please let me know if you have any questions or problems. To waive any defect(s) associated with this issue, please contact your PO. Thanks, Jackie Blackmon Environmental Coordinator- Regions 6 and 9
CSC 15000 Conference Center Drive, Ctiantilly VA 20151 Civil Division I office phone 703-818-4184 | fax 703-818-4601 | lblacl
F r o m :
[email protected] [mailto:
[email protected]] On Behalf O f
[email protected] Sent: Wednesday, July 28, 2010 11:33 AM T o : Blackmon, Jacqueline S u b j e c t : Re: UPDATED (7-16) | Case 40334 | Lab LIBRTY | Issue Multiple Issue 1 & 2: Please schedule 15 water samples for dissolved metals analysis. Issues: Revision noted, proceed. Issue 7: These samples are soil.
Region 9 RSCC EPA Region 9 Laboratory Office: 510-412-2389 Fax: 510-412-2302 email:
[email protected]
From:
"Blackmon, Jacqueline"
To:
R9RSCC@EPA
Dale:
07/28/2010 07:57 AM
Subecf
UPDATED (7-16) | Case 40334 | Lab LIBRTY j Issue l^ulliple
Garrett, I have informed the laboratory of the resolutions that were previously provided. Please note the revision of issue 5, and the addition of issue 7 that I noticed when reviewing the TFWCOC. Issues 1 and 2: Would you like SMO to schedule the samples for dissolved metals analysis? If so, please advise how many samples should be scheduled. Issue 5: Sample MY71T1 is designated on the TR/COC for laboratory QC; however samples MY71T5 and MY71T6 are also designated on the TR/COC for laboratory QC. The lab would like to use sample MY71T5 as QC
11 7/28/2010
19
Page 3 of 8
for TM—AES.MS and sample MY71T6 as QC for DM—AES,MS for the water samples, and not sample MY71T1. The lab chose to analyze Hg with ICP-AES since scheduling does not specify AES or MS for Hg. Resolution 5: Per Region 9, samples MY71T5 and MY71T6 are acceptable to use as laboratory QC. Sample MY71T1 does not need to be used for lab QC. The laboratory will note the issue in the SDG Narrafive and proceed with the analysis of the samples. Issue 7: The matrix for samples MY71L5, -L6, -L7,-L8,-L9, -MO, - M l , -M2 and - M 3 is listed as "Other" on the attached TR/COC. The laboratory stated that these samples resemble soil samples. Please advise if SMO should schedule an additional matrix for these samples, or if these are in fact soil samples. Please let me know if you have any questions or problems. Thanks, Jackie Blackmon Environmental Coordinator- Regions 6 and 9 CSC 15000 Conference Center Drive, Chantilly VA 20151 Civil Division I office phone 703-818-4184 I fax 703-818-4601 | iblackmon3(g)fedcsc.com | www.csc.com This is a PRIVATE message. If you are not the intended recipient, please delete without copying and kindly advise us by e-mail of the mistake in delivery. NOTE: Regardless of content, this e-mail shall not operate to bind CSC to any order or olher coniract unless pursuant to explicit written agreement or government initiative expressly permitting the use of e-mail for such purpose.
7/28/10 at 10:44am Phone conversation between Jackie Blackmon, SMO and Joan Purdie, LIBRTY laboratory. Jackie informed Joan that the total list of analytes for ICP-MS were scheduled. Joan confirmed that the issue stating 'The ASR list 11+ the metals you listed for MS not just the ones you listed," is no longer an issue. F r o m : Joan Purdie rmailto:[email protected] Sent: Wednesday, July 28, 2010 9:59 AM To: Blackmon, Jacqueline S u b j e c t : RE: Region 09 | Case 40334 | Lab LIBRTY | Issue Multiple Jackie, Issue 2: The ASR list 11+ the metals you listed for MS not just the ones you listed. The lab chose to analyze Hg with AES since Scheduling does not specify AES or MS for Hg. Thank you, Joan Purdie CompuChem/Liberty EPA Contract Coordinator 919-379-4081 [email protected] F r o m : Blackmon, Jacqueline fmailto:[email protected] S e n t : Wednesday, July 28, 2010 9:30 AM T o : Cathy Dover; Diane Byrd; Joan Purdie; Kenneth Grzybowski S u b j e c t : Region 09 | Case 40334 | Lab LIBRTY | Issue Multiple Joan, Please note the resolutions below for Case 40334. I need to confirm with the Region if the filtered water samples need to be scheduled and then I will provide a final ROC. -Discrepancies w i t h tags, Jars, and/or TR/COCI s s u e l : Sample MY71X9 is listed on the TR/COC as TM, but labeled as DM. Resolution 1: Per Region 9, these samples has been field filtered. The laboratory will note the issue In the SDG Narrative and proceed with the analysis ofthe samples.
12 7/28/2010
20
Page 4 of 8
Issue 2: The TR/COC lists the analysis as DM for the water samples; however per scheduling, water samples are for unfiltered ICP-AES (Al, Ca, Fe. Mg. K, Na); ICP-MS (Sb, As. Ba, Be, Cd, Cr, Co, Cu, Pb, Mn, Ni, Se, Ag, Tl, V, Zn); and Hg analysis. Can you please confirm that these samples are not dissolved? Resolution 2: Per Region 9, some samples (designated with the letter "F" in the station location) have been field filtered. Please analyze these samples for the exact same parameters as were originally scheduled. The laboratory will note the issue in the SDG Narrative and proceed with the analysis ofthe samples. Issue 3: Only one TR/COC out of the nine are signed under the "Relinquished By" section. Resolution 3: Per Region 9, the laboratory will note the issue in the SDG Narrative and proceed with the analysis ofthe samples. -pH outside allowable limitsIssue 4: Samples MY71X5 and MY71 Y l were bolh received with ph of 7, which is above the required level. Resolution 4: In accordance with previous direction from Region 9, the laboratory will note the issue in the SDG Narrative, adjust the pH, and proceed with the analysis of the sample. The resolution will be applied to all samples received for this Case with a pH outside of allowable limits. -Insufficient/inappropriate designation of laboratory QCIssue 5: Sample MY71T1 is designated on the TR/COC for laboratory QC; however samples MY71T5 and MY71T6 are also designated on the TR/COC for laboratory QC. The lab would like to use sample MY71T5 as QC for TM—AES.MS and sample MY71T6 as QC for DM—AES.MS for the water samples, and not sample MY71T1. Resolution 5: Per Region 9, samples MY71T5 and MY71T6 are acceptable to use as laboratory QC. Sample MY71T1 does not need to be used for lab QC. The laboratory will note the issue in the SDG Narrative and proceed with the analysis of the samples. -Return airbill information missing/incompleteIssue 6: There is no return information for the coolers. Please provide a contact, third party account, return address, and phone number so that the coolers can be returned. Resolution 6: Per Region 9, the coolers do not need to be returned to the samplers. Please let me know if you have any questions or problems. Thanks, Jackie Blackmon Environmental Coordinator- Regions 6 and 9
CSC 15000 Conference Center Drive, Chanlilly VA 20151 Civil Division I office phone 703-818-4184 (fax 703-818-4601 | iblackmQn3(g)fedcsc.com j www.csc.com This is a PRIVATE message. If you are nol the intended recipient, please delete wiihout copying and kindly advise us by e-mail of the mistake in delivery. NOTE: Regardless of content, this e-mail shall not operate to bind CSC to any order or other contract unless pursuant to explicit wrillen agreemeni or government initiative expressly permitting the use of e-mail for such purpose.
F r o m : Joan Purdie rmailto:[email protected] S e n t : Tuesday, July 27, 2010 6:08 PM T o : Blackmon, Jacqueline S u b j e c t : RE: REGION 9|C#40334|ISSUE MY71T5 is QC for TM—AES.MS MY71T6 is QC for DM—AES.MS. Thank you, Joan Purdie CompuChem/Liberty EPA Contract Coordinator 919-379-4081 [email protected]
13 7/28/2010
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Page 5 of 8
F r o m : [email protected] rmailto:[email protected] On Behalf Of [email protected] Sent: Tuesday, July 27, 2010 5:02 PM To: Blackmon, Jacqueline S u b j e c t : Re: (7-16) | Case 40334 | Lab LIBRTY | Issue Multiple Issue 1: this samples has been field filtered Issue 2: Some samples (designated with the letter "F" in the station location) have been field filtered. Please analyze these samples for the exact same parameters as were originally scheduled. Issue 3: Note the issue and proceed with analysis. Issue 4: resolved Issue 5: MY71T5 and MY71T6 are OK to use as lab QC. MY71T1 does not need to be used for lab QC. Issue 6: The coolers do not need to be returned to the samplers. •k-fr-k-t-k-A-k-lc-k-lr-tr-k-M-h-k-k-k-k^k-k-k-klr-tr-ie-h-ir-k-it-tc-A-*-*
Region 9 RSCC EPA Region 9 Laboratory Office: 510-412-2389 Fax: 510-412-2302 email: [email protected] ********************•+***•*******
From:
"Blackmon, Jacqueline"
To:
R9RSCC@EPA
Date.
07/27/2010 11:57 AM
g^(j.gj,,
(7-16) I Case 40334 | Lab LIBRTY | Issue Multiple
Garrett, LIBRTY is reporting the following issues for Case 40334. Issue 4 can be resolved with a standard answer; however please advise on how the Region wishes the laboratory to proceed for issues 1, 2, 3, 5 and 6. -Discrepancies with tags, jars, and/or TR/COCIssue 1: Sample MY71X9 is listed on the TR/COC as TM, but labeled as DM. Issue 2: The TR/COC lists the analysis as DM for the water samples; however per scheduling, water samples are for unfiltered ICP-AES (Al, Ca, Fe, Mg, K, Na); ICP-MS (Sb, As, Ba, Be, Cd, Cr, Co, Cu, Pb. Mn, Ni, Se, Ag. Tl. V,
14 7/28/2010
22
Page 6 of 8
Zn); and Hg analysis. Can you please confirm that these samples are not dissolved? Issue 3: Only one TR/COC out of the nine are signed under the "Relinquished By" section. -pH outside allowable limitsIssue 4: Samples MY71X5 and MY71Y1 were both received with ph of 7, which is above the required level. Resolution 4: In accordance wilh previous direction from Region 9, the laboratory will note the issue in the SDG Narrative, adjust the pH, and proceed wilh the analysis of the sample. The resolution will be applied to all samples received for this Case with a pH outside of allowable limits. -Insufficientyinappropriate designation of laboratory QCIssue 5: Sample MY71T1 Is designated on the TR/COC for laboratory QC; however samples MY71T5 and MY71T6 are also designated on the TR/COC for laboratory QC. The lab would like to use samples MY71T5 and MY71T6 as laboratory QC for the water samples, and not sample MY71T1. -Return airbill information missing/incompleteissue 6: There is no return information for the coolers. Please provide a contact, third party account, return address, and phone number so that the coolers can be returned. Please let me know if you have any questions or problems. Thanks. Jackie Blackmon Environmental Coordinator- Regions 6 and 9
CSC 15000 Conference Center Drive, Chantilly VA 20151 Civil Division I office phone 703-318^184 | fax 703-818-4601 j |[email protected] | www.csc.com This is a PRIVATE message. If you are not the intended recipient, please delete wiihout copying and kindly advise us by e-mail of the mistake in delivery. NOTE: Regardless of content, Ihis e-mail shall not operate to bind CSC to any order or other contract unless pursuant lo explicit wriiten agreement or governmeni initiative expressly permitting the use of e-mail for such purpose.
F r o m : Joan Purdie f mailto:[email protected] Sent: Tuesday, July 27, 2010 2:35 PM To: Blackmon, Jacqueline S u b j e c t : RE: REGION 9|C#40334|ISSUE Jackie. The Scheduling (ASR) does not list DM for this Case. Thank you. Joan Purdie CompuChem/Liberty EPA Contract Coordinator 919-379-4081 [email protected]
7/27/10 at 2:15pm Phone conversation between Jackie Blackmon. SMO and Joan Purdie, LIBRTY laboratory. Joan informed Jackie that the she was referencing samples MY71T5 and MY71T6 when she noted that other samples were listed with extra volume for QC. The lab would like to use samples MY71T5 and MY71T6 as laboratory QC for the water samples, and not sample MY71T1.
15 7/28/2010
23
Page 7 of8
F r o m : Blackmon, Jacqueline Sent: Tuesday, July 27, 2010 1:45 PM To: 'Joan Purdie' S u b j e c t : RE: REGION 9|C#40334|ISSUE Joan, Thanks! And for issue 3 below, when you say that other samples were provided with additional volume, are you referencing samples MY71T5 and MY71T6? If so, please advise which sample the lab would like to use for laboratory QC and the SDG number it will be used for. Thanks, Jackie Blackmon Environmental Coordinator- Regions 6 and 9 CSC 15000 Conference Cenier Drive, Chantilly VA 20151 Civil Division I otfice phone 703-818-4184 I fax 703-818-4601 j [email protected] | www.csc.com This is a PRIVATE message. If you are nol the intended recipient, please delete wiihout copying and kindly advise us by e-mail of the mistake in delivery. NOTE: Regardless of content, this e-mail shall not operate to bind CSC to any order or other contraci unless pursuant to explicit written agreement or government initiative expressly permitting the use of e-mail for such purpose.
F r o m : Joan Purdie rmailto:[email protected] Sent: Tuesday, July 27, 2010 1:32 PM T o : Blackmon, Jacqueline S u b j e c t : RE: REGION 9|C#40334|ISSUE Soil. Joan Purdie CompuChem/Liberty EPA Contract Coordinator
919-379-4081 [email protected]
F r o m : Blackmon, Jacqueline rmailto:iblackmon3(g)fedcsc.com1 Sent: Tuesday, July 27, 2010 12:28 PM To: Joan Purdie S u b j e c t : RE: REGION 9|C#40334|ISSUE Joari, For issue 3 in the first email below, you note that there are two other samples with extra volume listed that will be better to use as Qc for the waters. According to the TR/COC, the samples designated for laboratory QC for waters are, MY71T5, and MY71T6, and samples MY71T5 and MY71T6 are listed with extra volume. Are these the samples you are referencing? If so. please advise which sample you would like to use for laboratory QC and the SDG number it will be used for. I also noticed that the matrix for samples MY71L5, -L6, -L7,-L8.-L9, -MO. - M l , -M2 and - M 3 are listed as "Other" on the TR/COC. Were these closer to water or soil samples?
16 7/28/2010
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Page 8 of8
Thanks, Jackie Blackmon Environmental Coordinator- Regions 6 and 9 CSC 15000 Conference Center Drive, Chantilly VA 20151 Civil Division | office phone 703-818-4184 | fax 703-818-4601 | [email protected] [www.csc.com This is a PRIVATE message. If you are riot the intended recipient, please delete withoul copying and kindly advise us by e-mail of the mistake in delivery. NOTE: Regardless of content, this e-mail shall not operate to bind CSC to any order or olher conlracl unless pursuant to explicil written agreement or government initiative expressly permilting ttie use of e-mail for such purpose.
F r o m : Joan Purdie rmailto:[email protected] S e n t : Tuesday, July 27, 2010 12:02 PM T o : Blackmon, Jacqueline S u b j e c t : RE: REGION 9|C#40334IISSUE Jackie, I needed to mention that only 1 TFVCOC out of the 9 were signed under Relinquish By. Joan Purdie CompuChem/Litjerty EPA Contract Coordinator 919-379-4081 jpurdieQjcompuchemlabs.com
F r o m : Joan Purdie Sent: Tuesday, July 27, 2010 11:35 AM T o : 'Blackmon, Jacqueline' Cc: Diane Byrd S u b j e c t : REGION 9|C#40334|ISSUE Jackie, I received this Case today with the following issues: 1: Sample id MY71X9 is listed on the TR/COC as TM but labeled DM. 2: Sample ids MY71X5,Y1 were both received with ph of 7 above required level. 3: Sample id MY71T1 is listed on the TF^COC as Qc but there are 2 other samples with extra volume listed that will be better to use as Qc for the waters. 4: There Is no return information for the coolers. Thank you, Joan Purdie CompuChem/Liberty EPA Contract Coordinator 919-379-4081 [email protected]
[attachment "40334-07-27-10.pdf deleted by Garrett Peterson/R9/USEPA/US]
17 7/28/2010
25
3. Sample Log-ln Sheet (Form DC-1)
18
26
SAMPLE LOG-IN SHEET
yl
Lab Name:LIBERTY ANALYTICAL
Page
Received By (Print Name)
Log-in Uate 07/27/2010
R e c e i v e d By
7ya^NiF6Liy^K)id£^
^B^A^
(Signature)
Case Nuinber 40334
Remarks:
Pfcaefit/Absent* letapt/Broken
2. Custody Seal Nos.
Mod.
Group No. 7133
ORIGINAL:
1. Custody Seal (s)
A n . -1 c
No.
Corresponding Remarks: Condition of Sample Shipment, etc
EPA Sample #
Aqueous sample pH
MY71S3
1.0
NO TAGS
1007157-01
RECEIVED IN ;00D CONDITION
MY71S5
1.0
NO TAGS
1007157-02
RECEIVED IN ;00D CONDITION
MY71S7
1.0
NO TAGS
1007157-03
RECEIVED IN ;00D CONDITION
Sample Tag #
Assigned Labt
* Traffic Reports/ P/e^ent/Absent* Chain of Custody Records (TR/COCs) or Packing Lists
Ref. N/A
4. Airbill
Ai]<^^l/Sticker Pre^fejJt/Absenli*
MY71SS
1.0
NO TAGS
1007157-04
RECEIVED IN ;0GD CONDITION
5. Airbill No.
793761083828
MY71T1
1.0
NO TAGS
1007157-05
RECEIVED IN iOOD CONDITION
MY71T3
1.0
NO TAGS
1007157-06
6. Sample Tags'*
Present/Ab^e^t*
RECEIVED IN OOD CONDITION
MY71T5
1.0
NO TAGS
1007157-07
RECEIVED IN OOD CONDITION
MY71T7
1.0
NO TAGS
1007157-08
RECEIVED IN OOD CONDITION
7. Sample Condition 1/ ^ct/Broken*/ L^s
MY71T9
1.0
NO TAGS
1007157-09
RECEIVED IN OOD CONDITION
t/Absent*
MY71W1
1.0
NO TAGS
1007157-10
RECEIVED IN OOD CONDITION
MY71W5
1.0
NO TAGS
1007157-11
RECEIVED IN ;00D CONDITION
MY71W9
1.0
NO TAGS
1007157-12
RECEIVED IN OOD CONDITION
MY71X1
1.0
NO TAGS
1007157-13
RECEIVED IN OOD CONDITION
MY71X3
1.0
NO TAGS
1007157-14
RECEIVED IN ;00D CONDITION
MY71X5
7.0
NO TAGS
1007157-15
RECEIVED IN OOD CONDITION
MY71xe
1.0
NO TAGS
1007157-16
RECEIVED IN OOD CONDITION
MY71xe
1.0
NO TAGS
1007157-17
RECEIVED IN GOD CONDITION
MY71Y0
1.0
NO TAGS
1007157-18
RECEIVED IN OOD CONDITION
Sample Tag Numbers
Li^^/Not Listed on Chain-of-Custody
8. Cooler Temperature Indicator Bot 9. Cooler Temperture
o
10.Does Informa t i o n / e f e / N o * on TR/COCs and sample tags agree? 11.Date Received at 07/27/2010 Lab 12.Time Received
09:15
bample Transrer Frajs^-irorr
Fraction /~)^ -
•^rfjcHdCi.Atjic On 07/27/2010 * Contact SMO and attach record of resolution Reviewed By Date
Logbook No. Logbook Page No.
«PO/Q FORM DC-1
ILM05
27
4. Full Inorganic Complete SDG File (CSF)lnventory Sheet (Form DC-2)
20
28
FULL INORGANICS COMPLETE SDG FILE (CSF) INVENTORY SHEET
LABORATORY NAME CITY/STATE CASE NO. MJ^t^'^TSDG NO. SDG
NOs.
TO
FOLJJOW
NRAS NO.
f/fviS6mi_
CONTRACT NO. SOW NO.
,
All documents delivered in the Complete SDG File must be original documents where possible. (Reference - Exhibit B Section 2.6) PAGE NOs. FROM I.
Cover Page
2".
SDG Narrative
3.
Sampie Log-In Sheet
4.
Inventory Sheet
5.
Trattic Report/Chain ot Custody Record(s)
LAB
CHECK REGION
/
A
(DC-1)
2D
(DC-2)
y
Inorganic Analysis
y
6.
Data Sheet
(Form I-IN)
7.
Initial & Continuing Calibration Verification (Form IIA-IN)
8.
CRQL Standard (Form IIB-IN)
9.
Blanks (Form III-IN)
y y
10. ICP-AES Interference Check Sample (Form IVA-IN)
/
II. ICP-MS Interterence Check Sample (Form IVB-IN) 12. Matrix Spiice Sample Recovery (Form VA-IN) 13 . Post-Diqestion Spiice Sample Recovery (Form VB-IN) 14. Duplicates
AW y
(Form VI-IN)
15. Laboratory Controi Sample (Form VII-IN)
^
16. ICP-AES and ICP-MS Serial Dilutions (Form VIII-IN) 17. Method Detection Limits (Form IX-IN)
(Annually)
y
18. ICP-AES Interelement Correction Factors (Quarterly) (Form XA-IN) 19. ICP-AES Interelement Correction Factors (Quarterly) (Form XB-IN)
/
20. ICP-AES and ICP-MS Linear Ranges (Form XI-IN)
/
21. Preparation Log
(Quarterly)
y
(Form XII-IN)
FORM DC-2-1
ILM05.4
21
29 PAGE NOs. FROM TO
22. Analysis Run Log 23. ICP-MS Tune
LAB
CHECK REGION
(Form XIII-IN)
(Form XIV-IN)
24. ICP-MS I n t e m a l Standards Relative Intensity Summary (Form XV-IN) 25. ICP-AES Raw Data 26. GFAA Raw Data
m ttr>sm\
(It Applicable)
27. ICP-MS Raw Data 28. Mercury Raw Data 29. Cyanide Raw Data 30. Preparation Logs Raw Data 31. Percent Solids Determination Log 32. USEPA Shipping/Receiving Documents I Airbill
(No. ot Shipments
| )
^
22^
Sample Tags Sample Log-In Sheet (Lab) 33. Misc. Shipping/Receiving Records (list all individual records) Telephone Logs
1/ 34 . Internal Lab Sample Transter Records & Tracking Sheets (describe or list)
35. Internal Original Sample Prep & Analysis Records (describe or list) Prep Records Analysis Records Description 36. other Records (describe or list) Telephone Communications Log
37. Comments:
Completed by: (CLP Lab)
r\cm2\yAr ( P r i n t Name & T i t l e )
A u d i t e d by (USEPA)
v ^
(sighature)
( P r i n t Name & T i t l e )
gii^VO (Date)
^f(^^^ (Date)
22 FORM DC-2-2
ILM05.4
30
ORIGINAL
SAMPLE DELIVERY GROUP (SDG) COVER SHEET SDG N u i n b e r : MY71S3
Laboratory Name Contract No. Analysis Price
COMPUCHEM
EPW08067 $
1,098.00
W.%l'^«iJ^ aboratory
LIBRTY
Code Case No. SDG Turnaround
40334
^ 1 -?^ days
EPA Sample Nmbers in SDG (Listed in Numerical Order) 1) MY71S3
7) MY71T5
13) MY71X1
19)
2) MY71S5
8) MY71T7
14) MY71X3
20)
3) MY71S7
9) MY71T9
15) MY71X5
21)
4) MY71S9
10) MY71W1
16) MY71X6
22)
5) MY71T1
11) My71W5
17) MY71X8
23)
6) MY71T3
12) MY71W9
18) MY71Y0
24) /
MY71S3
7 / / / / •
MY71Y0
First Sample in SDG
Last Sample in SDG
07/27/2010
07/27/2010
F i r s t Sample R e c e i p t Date
Last Sample Receipt Date
Note: There are a maximum of 20 samples (excluding PE Sample) in SDG. Attach TRs to this form in alphanumeric order (the order listed above on this form).
lyi.diiu Signat
Ir^n-^/o Date
ye
31
B. Sample Data 1. Results 2. Quality Control Data 3. Raw Data 4. Digestion and Distillation Logs
LAB CODE : LIBRTY
CONTRACT # : EPW08067
CASE#:
SDG # :
40334
MY71S3
29
32
1. Results Sample results shall be arranged in packets with the Inorganic Analysis Data Sheet [Form IA - IN and Form IB - IN]. These sample packets shall be placed in increasing alphanumeric EPA sample number order, considering both letters and numbers, and shall include all the samples in the SDG.
30
33 u s EPA - CLP lA-IN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE N O . MY71S3
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case N o .
40334
EPW08067 SDG NO.:
NRAS N o . :
Matrix (soil/water):
WATER
Lab Sample ID:
1007157-01
Level (low/med):
LOW
Date Received:
07/27/2010
% Solids:
MY71S3
0.0
Concentration Units (ug/L or mg/kg dry weight): CAS N O .
Analyte
7429-90-5
Aluininum
7440-70-2 7439-89-6 7439-95-4
Magnesium
UG/L Concentration
C
Q
M
200
U
P
Calcium
1320
J
P
Iron
35.4
J
P
0.084
J
CV
207
J
3310
J
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Sodium
P
152000
E
p p
Color Before:
COLORLESS
Clarity Before:
CLRAR
Texture:
Color After:
COLORLESS
Clarity After:
CLEAR
Artifacts:
Comment s:
Form IA-IN
ILM05.4
31
34 u s EPA - CLP lA-IN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. MY71S5 Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case No.; 40334
EPW08067 SDG NO.:
NRAS No.:
Matrix (soil/water):
WATER
Lab Sample ID:
1007157-02
Level (low/med):
LOW
Date Received:
07/27/2010
MY71S3
0.0
% Solids: Concentration Units
( u g / L o r •ei^l'lnis d r y w e i g h t ) :
CAS No.
Analyte
7429-90-5
Aluminiun
7440-70-2
Calcium
7439-89-6
Iron
7439-95-4
Magnesium
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Sodium
UG/L Concentration
C
Q
M
200
U
P
1670
J
P
100
U
P
0.20
U
CV
458
J
4650
J
P
170000 E
P p
Color Before:
COLORLESS
Clarity Before:
CLEAR
Texture:
Color After:
COLORLESS
Clarity After;
CLEAR
Artifacts
Comments:
32 Form l A - I N
ILM05.4
35 u s EPA - C L P lA-IN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. MY71S7
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Matrix Level
Case No. :
(soil/water): (low/med)
% Solids:
Contract: 40334
EPW08067 SDG NO.
NRAS NO.:
WATER
Lab Sample ID:
1007157-03
LOW
Date Received:
07/27/2010
MY71S3
0.0 UG/L
Concentration Units (ug/L or mg/kg dry weight) CAS N o .
Analyte
7429-90-5
Al\imlnum
7440-70-2
Calcium
7439-89-6
Iron
7439-95-4
Magnesixaro
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Sodium
Concentration 200
C
Q
P
12400 100
P
U
P
175000
CV
0.28 920
M
P
U
J
E
P P
13500
Color Before:
COLORLESS
Clarity Before:
CLEAR
Texture:
Color After:
COLORLESS
Clarity After:
CLEAR
Artifacts:
Comment s :
Form
lA-IN
1LM05.4
33
36 u s EPA - CLP IAIN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. MY71S9 Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract Case No.
40334
EPWO8067 SDG NO. I
NRAS No.:
Matrix (soil/water):
WATER
Lab Sample ID:
1007157-04
Level (low/med):
LOW
Date Received:
07/27/2010
% Solids:
MY71S3
0.0 UG/L
Concentration Units (ug/L or mg/kg dry weight)
Concentration
CAS No.
Analyte
7429-90-5
Aluminum
135000
P
7440-70-2
Calcivim
231000
P
C
Q
M
7439-89-6
Iron
502000
P
7439-95-4
Magnesium
272000
P
7439-97-6
Mercury
7440-09-7
Potassitim
7440-23-5
Sodium
0.20 46000
CV
U E .
p p
299000
Color Before:
COLORLESS
Clarity Before:
CLEAR
Texture:
Color After:
YELLOW
Clarity After:
CLEAR
Artifacts:
Comments:
34 Form l A - I N
ILIV105.4
37 u s EPA - CLP lA-IN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. MY71T1
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case No.: 40334
EPWO8067 SDG NO. :
NRAS No.:
Matrix (soil/water):
WATER
Lab Sample XD:
1007157-05
Level (low/med):
LOW
Date Received:
07/27/2010
% Solids:
MY71S3
0.0 UG/L
Concentration Dnits (ug/L or mg/kg dry weight) ; CAS NO.
Analyte
7429-90-5
AluminiJin
128000
P
7440-70-2
Calcium
259000
P
7439-89-6
Iron
325000
P
7439-95-4
Magnesium
295000
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Sodium
Concentration
C
Q
M
P
21.2
D
CV
46200
E
P P
322000
Color
Before:
COLORLESS
Clarity
Before:
CLEAR
Texture:
Color
After:
YELLOW
Clarity
After:
CLEAR
Artifacts:
Comments:
35 Form l A - I N
ILM05.4
38 u s EPA - C L P IAIN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. MY71T3
L a b Name:
COMPUCHEM
Lab Code;
LIBRTY
Matrix Level
Case No.:
(soil/water): (low/med)
54 S o l i d s :
Contract: 40334
EPW08067 SDG NO.
NBAS No.:
WATER
Lab Sample ID:
1007157-06
LOW
Date Received:
07/27/2010
MY71S3
0,0 UG/L
Concentration Units (ug/L or mg/kg dry weight) CAS No.
Analyte
7429-90-5
Aluminum
7440-70-2
Calcium
7439-89-6
Iron
7439-95-4
Magnesium
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Concentration
C
Q
20700
P
106000
P
53200
P P
210000
CV
4,9 10300
E
p p
110000
Sodium
M
Color Before:
COLORLESS
Clarity Before:
CLEAR
Texture:
Color After:
COLORLESS
Clarity After;
CLEAR
Artifacts:
Comments;
36 Form
lA-IN
ILM05.4
39 u s EPA - CLP lA-IN INORGANIC ANALYSIS DATA SHEET BPA SAMPLE NO. My71T5
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Matrix Level
Case No.:
(soil/water) (low/med);
% Solids:
EPWO8067
Contract: 40334
SDG NO. :
NRAS N o . : ID:
1007157-07
Received:
07/27/2010
WATER
Lab Sample
LOW
Date
MY71S3
0.0
UG/L
Concentration Units (ug/L or mg/kg dry woight): CAS No.
Analyte
7429-90-5
AlTjminum
7440-70-2
Calcium
7439-89-6
Iron
7439-95-4
Magnesium
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Sodixun
Concentration
C
Q
M
23500
P
115000
P
43500
P
319000
D
11300
P CV
4.8 E
P p
122000
Color Before;
COLORLESS
Clarity Before:
CLEAR
Texture:
Color After:
COLORLESS
Clarity After:
CLEAR
Artifacts;
Comment s :
37 Form
lA-IM
ILM05.4
40 u s EPA - CLP lA-EN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. MY71T7
L a b Name:
COMPUCHEM
Lab Code:
LIBRTY
Matrix Level
C a s e No.
(soil/water): (low/med):
% Solids:
Contract:
40334
EPW08067 SDG N O . :
NRAS N o . :
WATER
Lab Sample I D :
1007157-08
LOW
Date
07/27/2010
Received:
MY71S3
0.0
Concentration Dnits (ug/L or mg/kg dry weight) i CAS No.
Analyte
7429-90-5
Aluminum
7440-70-2
Calcium
7439-89-6
Iron
7439-95-4
Magnesium
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Sodium
UG/L
Concentration
C
Q
M
23800
P
117000
P
52300
P
293000
P CV
4.6 10600
E
p p
125000
Color Before:
COLORLESS
Clarity Before:
CLEAR
Texture;
Color After:
COLORLESS
Clarity After;
CLEAR
Artifacts:
Comments:
38 Form l A - I N
ILM05.4
41 u s EPA - CLP lA-IN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. MY71T9 Lab Hame:
COMPUCHEM
Lab Code:
LIBRTY
Contract; Case No.
40334
EPW08067
NRAS No.:
SDO NO.
Matrix (soil/water):
WATER
Lab Sample ID:
1007157-09
Level (low/med):
LOW
Date Received:
07/27/2010
% Solids:
MY71S3
0.0 UG/L
Concentration Units (ug/L or mg/kg dry weight) CAS No.
Analyte
7429-90-5
Aluminum
1150
7440-70-2
Calcium
1140
7439-89-6
Iron
7439-95-4
Magnesium
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Sodium
Concentration
C
Q
M P P
J
12500
P
148000
P
0.10
J
226
J
1930
J
CV E
p p
Color Before:
COLORLESS
Clarity
Before:
CLOUDY
Texture:
Color After:
COLORLESS
Clarity
After:
CLEAR
Artifacts:
Comment s :
39 Form l A - I N
ILM05.4
42 u s EPA - CLP IAIN INORGANIC AN/VLYSIS DATA SHEET EPA SAMPLE NO. MY71W1
Lab Name;
COMPUCHEM
Lctb Code:
LIBRTY
Contract: Case No.
40334
EPW08067 SDG NO.
NRAS No.:
Matrix (soil/water)
WATER
Lab Sample JD:
1007157-10
Level (low/med):
LOW
Date Received:
07/27/2010
% Solids:
MY71S3
0.0 UG/L
Concentration Units (ug/L or mg/kg dry weight); CAS No.
Analyte
7429-90-5
Aluminum
7440-70-2
Calcium
7439-89-6
Iron
7439-95-4
Magnesium
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Sodium
Concentration
C
Q
M
4970
P
181000
P
11300
P
369000
D
0.79 12300
P CV
E
P p
213000
Color Before:
COLORLESS
Clarity Before;
CLEAR
Texture:
Color After:
COLORLESS
Clarity After;
CLEAR
Artifacts;
Comments:
40 Form l A - I N
1LM05.4
43 u s EPA - CLP lA-IN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. My71W5
Lab Name:
COMPUCHEM
Lab Coda:
LIBRTY
Contracti Case No.
40334
EPW08067 SDG NO.
NRAS No. :
Matrix (soil/water):
WATER
Lab Sample ID:
1007157-11
Level (low/med):
LOW
Date Received:
07/27/2010
% Solids:
My71S3
0.0 UG/L
Concentration Dnits (ug/L or mg/kg dry weight):
Concentration
CAS NO.
Analyte
7429-90-5
Aluminum
7440-70-2
Calcium
7439-89-6
Iron
7439-95-4
Magnesium
7439-97-6
Mercury
0.20
U
7440-09-7
Potassium
3400
J
7440-23-5
Sodium
62.3
C
Q
P
116000 87.6
M
P
J
P
J
P
215000
CTV E
P P
543000
Color Before:
COLORLESS
Clarity Before:
CLEAR
Texture:
Color After:
COLORLESS
Clarity After:
CLEAR
Artifacts:
Ccanments:
Form l A - I N
ILM05.4
41
44 u s EPA - CLP lA-lN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. MY71W9 Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case No.
40334
EPW08067 SDG NO.: MY71S3
NRAS No.:
Matrix (soil/water):
WATER
Lab Sample ID:
1007157-12
Level (low/med)
LOW
Date Received:
07/27/2010
% Solids:
0.0
Concentration Units (ug/L or mg/kg dry weight) CAS No.
Analyt e
7429-90-5
Aliim-i num
7440-70-2
Calcium
7439-89-6
Iron
UG/L Concentration 200
C
«
M P
U
P
193000 583
P
295000
P
7439-95-4
Magnesium
7439-97-6
Mercury
0.20
7440-09-7
Potassium
6800
7440-23-5
Sodium
D
CV
U E
P P
593000
Color Before:
COLORLESS
Clarity Before:
CLEAR
Texture:
Color After:
COLORLESS
Clarity After:
CLEAR
Artifacts:
Comment s:
42 Form I A-IN
ILM05.4
45
u s EPA - CLP IAIN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. MY71X1 Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract -. Case No.
40334
EPW08067 SDG NO. :
NRAS No.:
Matrix (soil/water):
WATER
Lab Sample ID:
1007157-13
Level (low/med);
LOW
Date Received:
07/27/2010
% Solids:
MY71S3
0.0
Concentration Units (ug/L or mg/kg dry weight): CAS NO.
Analyte
7429-90-5
Aluminum
7440-70-2
Calcium
7439-89-6
Iron
7439-95-4
Magnesium
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Sodium
UG/L Concentration
C
Q
M
24900
P
122000
P
46100
P
324000
D
4.7 11600
P CV
E
p p
127000
Color Before:
COLORLESS
Clarity Before:
CLEAR
Texture:
Color A f t e r :
COLORLESS
Clarity After:
CLEAR
Artifacts:
Comments:
Form
lA-IN
ILM05.4
43
46 u s EPA - CLP lA-IN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. MY71X3
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case No.: 40334
EPW08067 SDG NO. :
NRAS No. i
Matrix (soil/water)
WATER
Lab Sample ID:
1007157-14
Level (low/med):
LOW
Date Received:
07/27/2010
Solids:
MY71S3
0.0 UG/L
Concentration Units (ug/L or mg/kg dry weight) i
Concentration
C
CAS NO.
Analyte
7429-90-5
Aluminum
127000
P
7440-70-2
Calcium
259000
P
7439-89-6
Iron
322000
P
7439-95-4
Magnesium
294000
P
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Sodium
Q
M
20.1
D
CV
45700
E
p p
319000
Color Before:
COLORLESS
Clarity Before:
CLEAR
Texture:
Color After:
YELLOW
Clarity After:
CLEAR
Artifacts:
Comments:
44 Form l A - I N
ILM05.4
47 u s EPA - CLP lA-IN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. MY71X5
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case No.
40334
EPWO8067 SDG NO.
NRAS No. :
Matrix (soil/water)
WATER
Lab Sample ID:
1007157-15
Level (low/med):
LOW
Date Received:
07/27/2010
% Solids:
MY71S3
0.0
Concentration Units (ug/L or mg/kg dry weight); CAS No.
Analyte
7429-90-5
Aluminum
7440-70-2
Calcium
UG/L Concentration
C
Q
M P
200
U
5000
U
P
7439-89-6
Iron
100
U
P
7439-95-4
Magnesium
22.1
J
P
7439-97-6
Mercury
0.20
7440-09-7
Potassium
5000
7440-23-5
Sodium
5000
u u u
CV E
p p
Color Before:
COLORLESS
Clarity Before:
CLEAR
Texture;
Color After:
COLORLESS
Clarity After:
CLEAR
Artifacts:
Comment s:
Form lA-IN
ILM05.4
45
48 u s EPA - CLP lA-IN INORGANIC AN/a.YSIS DATA SHEET EPA SAMPLE NO. MY71X6
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case No.
40334
EPWO8067 SDG NO.
NRAS No.:
Matrix (soil/water)
WATER
Lab Sample ID:
1007157-16
Level (low/med):
LOW
Date Received:
07/27/2010
% Solids:
MY71S3
0.0 UG/L
Concentration Dnits (ug/L or mg/kg dry weight): CAS No.
Analyte
7429-90-5
Aluminum
7440-70-2
Calcium
7439-89-6
Iron
7439-95-4
Magnesium
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Sodium
Concentration
C
Q
M
200
U
P
1110
J
P
100
U
P P
134000 0.20
U
228
J
3040
J
(TV E
P P
Color Before:
COLORLESS
Clarity Before:
CLEAR
Texture:
Color After:
COLORLESS
Clarity After:
CLEAR
Artifacts:
Comment s :
46 Form l A - I N
ILM05.4
49 u s EPA - CLP lA-IN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. MY71X8
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case No.
40334
EPWO8067 SDG NO. :
NRAS No.:
Matrix (soil/water)
WATER
Lab Sample ID:
1007157-17
Level (low/med):
LOW
Date Received:
07/27/2010
% Solids:
MY71S3
0.0 UG/L
Concentration Units (ug/L or mg/kg dry weight) : CAS NO.
Analyte
7429-90-5
Aluminum
7440-70-2
Calcium
7439-89-6
Iron
7439-95-4
Magnesitim
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Sodium
Concentration
C
Q
M
200
U
P
1650
J
P
100
U
P P
156000 0.20
U
327
J
4320
J
CV E
P P
Color Before:
COLORLESS
Clarity
Before:
CLEAR
Texture:
Color After:
COLORLESS
Clarity
After:
CLEAR
Artifacts;
Comments;
Form
lA-IN
ILM05.4
47
50 u s EPA - CLP lA-IN INORGANIC ANALYSIS DATA SHEET EPA SAMPLE NO. MY71Y0
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Matrix Level
Case N o . :
(soil/water): (low/med)
% Solids:
Contract:
40334
EPW080 6 7 SDG NO.
NRAS N o . t ID:
1007157-18
Received:
07/27/2010
WATER
Lab Sample
LOW
Date
MY71S3
0.0
UG/L
Concentration Units (ug/L or mg/kg dry weight) CAS No.
Analyte
7429-90-5
Aluminum
64.2
J
P
7440-70-2
Calcium
1550
J
P
100
U
P
7439-89-6
Iron
7439-95-4
Magnesium
7439-97-6
Mercury
7440-09-7
Potassium
7440-23-5
Soditim
Concentration
C
Q
P
154000 0.20
M
CV
U
339
J
4310
J
E
p p
Color Before:
COLORLESS
Clarity Before:
CLEIAR
Texture:
Color After:
COLORLESS
Clarity After:
CLEAR
Artifacts:
Comments:
48 Form
lA-IN
rLM05.4
51
2. Quality Control (QC) Data a. Initial and Continuing Calibration Verification [Form IIA - IN] b. CRQL Check Standard [Form IIB - IN] c. Blanks [Form III - IN] d. ICP-AES Interference Check Sample [Form IVA - IN] e. Matrix Spike Sample Recovery [Form VA - IN] f. Post Digest Spike Sample Recovery [Form VB - IN] g. Duplicates [Form VI - IN] h. Laboratory Control Sample [Form Vll - IN] i. ICP-AES Serial Dilutions [Form Vlll - IN] j . Method Detection Limits (Annually) [Form IX - IN] k. ICP-AES Interelement Correction Factors (Quarterly) [Form XA - IN] I. ICP-AES Interelement Correction Factors (Quarterly) [Form XB - IN] m. ICP-AES Linear Ranges (Quarterly) [Form XI - IN] n. Preparation Log [Form XII - IN] o. Analysis Run Log [Form XIII - IN]
49
52
u s EPA - CLP 2A-IN INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name:
COMPUCHEM
Lab c o d a :
LIBRTY
Contract: Case No.
40334
EPWO8067 SDG NO.: My71S3
NRAS NO.:
Initial Calibration Verification Source:
EPA-0307
Continuing Calibration Verification Source:
HP091809BWL
Concentration Units: ug/L Initial Calibration Verification Analyte
True
Aluminum Calcium
Pound
Continuing Calibration Verification True
Found
103
50000.0
50339.57
%R(1)
%R(1)
Pound
101
50658.27
'SR(l)
M
101
P
2521.0
2599.33
10026,0
9925.32
99
50000.0
49663,38
99
49172.43
98
P
100
25000.0
25106.37
100
25090.79
100
P
Iron
5082.0
5100.92
Magnesitim
6074.0
6018.63
99
50000.0
50277.04
101
50365.39
101
P
4.0
4.15
104
5.0
4,97
99
5.05
101
CV
10021.0
9772.56
98
50000.0
48408.31
97
48695.32
97
P
10193.45
101
50000.0
50731.84
101
51131.05
102
P
Mercury Potassium Sodium
10097.0
•
(1)
Control Limits:
Mercury 80-120;
Other Metals 90-110;
Form IIA-IN
•
•
•
1
Cyanide 85-115 ILM05.4
50
53
US EPA - CLP 2A-IN INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Initial
Contract: Case N o . :
Calibration Verification
40334
SDG NO. :
NRAS N o . :
MY71S3
EPA-0307
Source:
Continuing Calibration Verification
EPW08067
HP091809BWL
Source:
Concentration Units: ug/L Initial Calibration Verification Analyte
Continuing Calibration
Verification
True
Fotmd
Aluminum
50000.0
50834.94
102
Calcium
50000.0
50042.84
100
Iron
25000.0
25310.34
Magnesium
50000.0
True
Fotmd
%R(1)
«SR(1)
Found
?SR(1)
M
50659.14
101
P
49672.52
99
P
101
25361.64
101
P
50923.36
102
51008.63
102
P CV
5.0
5.27
105
Potassitim
50000.0
48792.02
98
48741.27
97
p
Soditim
50000.0
51497.68
103
50963.10
102
p
Mercury
1
(1)
Control Limits:
Mercury 80-120;
Other Metals 90-110;
Form IIA-IN
Cyanide 85-115 ILM05.4
51
54 u s EPA - CLP 2A-IN INITIAL AND CONTINULNG CALIBRATION VERIFICATION
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case No.
40334
EPWO8067 SDG NO. : MY71S3
NRAS No. :
Initial Calibration Verification Source:
EPA-0307
Continuing Calibration Verification Source:
HP091809BWL
Concentration Units: ug/L I n i t i a l Calibration Verification Analyte
True
Found
Continuing Calibration %R(1)
True
Found
Verification
%R{1)
Found
%R(1)
M
Aluininum
50000.0
50606.64
101
50700.44
101
P
Calcitim
50000.0
49690.04
99
49728.04
99
P
Iron
25000.0
25486.95
102
25530.42
102
P
Magnesitim
50000.0
51315.88
103
51342.24
103
P
Potassium
50000.0
48679.68
97
48882.56
98
P
Sodium
50000.0
50788.75
102
50420.65
101
P
- •
:
(1)
Control Limits:
Mercury 80-120;
Other Metals 90-110;
Form IIA-IN
1
Cyanide 85-115 ILM05.4
52
55
u s EPA - CLP 2A-IN INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name:
COMPUCHEM
Lab C o d e :
LIBRTY
Contract: Case No. :
40334
EPW08067 SDG NO. : MY71S3
NRAS No. :
Initial Calibration Verification Source:
EPA-0307
Continuing Calibration Verification Source:
HP091809BWL
Concentration Units: ug/L I n i t i a l Calibration Verification Analyte
Continuing C a l i b r a t i o n True
Fotmd
50000.0
50796.35
Calcitim
50000.0
Iron
25000.0
Magnesitim
True
1
Found
SSR(I)
Verification
5&R(1)
Found
"-sRd)
M
102
P
49688.40
99
P
25646.07
103
P
50000.0
51508.30
103
P
Potassitim
50000.0
49127.27
98
P
Soditim
50000.0
50622.30
101
P
Aluminum
(1)
Control Limits:
Mercury 80-120;
Other Metals 90-110;
Form IIA-IN
Cyanide 85-115 ILM05.4
53
56
u s EPA - CLP 2A-IN INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name:
COMPUCHEM
Lab c o d e :
LIBRTY
Contract: Case No.:
40334
EPWO8067 SDG NO. : MY71S3
NRAS No.:
Initial Calibration Verification Source:
EPA-0307
Continuing Calibration Verification Source:
HP091809BWL
Concentration Units: ug/L Initial Calibration Verification Analyte
True
j
Found
Continuing Calibration
| %R(1)
True
Found
Verification
SfeRd)
Fotmd
%R(1)
M
2547.65
101
50000.0
49706.83
99
49641,61
99
P
10026.0
10223.87
102
50000.0
49127.18
98
48987.33
98
P
Iron
5082.0
5039.58
99
25000.0
25120.38
100
24942.38
100
P
Magnesium
6074,0
5897.99
97
50000.0
49966.07
100
50113.79
100
P
4.0
4.06
102
5.0
5.20
104
5.20
104
CV
Potassitim
10021.0
9680.19
97
50000.0
48117.90
96
48113.06
96
p
Soditim
10097.0
10054.32
100
50000.0
50026.16
100
49855.19
100
p
Aluminum
2521.0
Calcium
Mercury
(1)
Control Limits:
Mercury 80-120;
Other Metals 90-110;
Form IIA-IN
Cyanide 85-115 ILMO5. 4
54
57
u s EPA - CLP 2A-IN INITIAL AND CONTINUING CALIBRATION VERIFICATION
L a b Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case No.:
40334
EPWO8067 SDG NO. : MY71S3
NRAS No.:
Initial Calibration Verification Source:
EPA-0307
Continuing Calibration Verification Source:
HP091809BWL
Concentration Units: ug/L i n i t i a l Calibration Verifxcation Analyte
True
Found
50000.0
49318.07
Calcitim
50000.0
Iron
25000.0
Magnesitim Potassium Sodium
True
Fotmd
Continuing Calibration %R(1)
Altimintim
Verification
S4R(1)
Fotmd
?4R(1)
M
99
P
49083.45
98
P
24959.29
100
P
50000.0
49993.65
100
P
50000.0
48069.84
96
P
50000.0
49219.27
98
P
1
1
(1)
Control Limits:
Mercury 80-120;
Other Metals 90-110;
Form IIA-IN
Cyanide 85-115 ILMO5. 4
55
58 u s EPA - CLP 2A-IN INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case No. :
40334
EPW08067 SDG NO. : MY71S3
NRAS No.:
Initial Calibration Verification Source:
EPA-0307
Continuing Calibration Verification Source:
HP091809BWL
Concentration Units; ug/L initial Calibration Verification Analyte
True
Altimintim
Found
Iron Magnesitim Mercury
S>oR(l)
True
Found
Verification
%R(1)
Found
%R(1)
M
2485.92
99
50000.0
49448.61
99
49479.18
99
P
10026.0
9839.25
98
50000.0
49547.94
99
48654.01
97
P
5082.0
5057.04
100
25000.0
25073.17
100
24937.37
100
P
6074.0
5873.15
97
50000.0
49286.18
99
49051.46
98
P
4.0
4.63
116
5.0
5.05
101
5.06
101
50000.0
48116.87
96
48314.71
97
p
50000.0
49964.34
100
49597.57
99
p
2521,0
Calcium
Continuing Calibration
Potassitim
10021.0
9781.23
98
Soditim
10097.0
9977.56
99
CV
'
(1)
Control Limits:
Mercury 80-120;
Other Metals 90-110;
Form IIA-IN
Cyanide 85-115 ILMO 5. 4
56
59
US EPA - C L P 2A-IN INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case No.
40334
EPW08067 SDG NO. : MY71S3
NRAS NO.:
Initial Calibration Verification Source:
EPA-0307
Continuing Calibration Verification Source:
HP091809BWL
Concentration Units: ug/L Initial calibration Verification Analyte
Continuing Calibration True
Found
Altimintim
50000.0
49077.81
98
48987.81
98
P
Calcium
50000.0
48472.79
97
48423.72
97
P
Iron
25000.0
24789.28
99
24774.83
99
P
Magnesium
50000.0
48738.72
97
48986.91
98
5.0
5.27
105
5.29
106
Potassitim
50000.0
47994.49
96
47662.20
95
P
Soditim
50000.0
49328.37
99
48881.25
93
p
True
Found
SiR ( 1 )
Verification
Mercury
(1)
Control
Limits:
Mercury 80-120;
Other Metals
Form
IIA-IN
90-110;
Cyanide
HR(1)
Found
%R(1)
M
P CV
85-115 ILM05.4
57
60
US EPA - CLP 2A-IN INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: COMPUCHEM
Contract; Case N o . :
Lab Code: LIBRTY Initial
Calibration Verification
NRAS N o . :
MY71S3
HP091809BWL
Source:
ug/L Initial Calibration Verification
Analyte
SDG NO. :
EPA-0307
Source;
Continuing Calibration Verification Concentration Units:
40334
EPW08067
Continuing Calibration
Verification
True
Found
50000.0
48445.18
97
P
Calcium
50000.0
47418,02
95
P
Iron
25000.0
24406.60
98
P
Magnesium
50000.0
48279.92
97
5.0
5,43
109
Potassium
50000.0
47452.44
95
Sodium
50000.0
48643.84
97
True
%R(1)
Found
Aluminum
Mercury
•
(1)
Control
Limits:
•
Mercury 80-120;
Other Metals
%R(1)
•
90-110;
Cyanide
Found
%R(1)
M
P 110
5.51
CV P p
.
•
J
85-115
58 Form
IIA-IN
ILM05.4
61
US EPA - CLP 2A-IN INITIAL AND CONTINUING CALIBRATION VERIFICATION
L a b Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case No.:
40334
EPWO8067 SDG NO. : MY71S3
NRAS No. :
Initial Calibration Verification Source:
EPA-0307
Continuing Calibration Verification Source:
HP091809BWL
Concentration Units: ug/L Initial Calibration Verification Analyte
True
Mercury
(1)
1 |
Control Limits:
Foimd
Continuing Calibration Verification
j 5iR(i)
True
j
j
'
'
Mercury 80-120;
Found
5,0
Other Metals 90-110;
Form IIA-IN
5,43
s&Rd)
Fotmd
9SR(1)
M
1
lev
109
Cyanide 85-115 ILM05.4
59
1
62 US EPA - CLP 2B-IN CRQL CHECK STANDARD
L a b Name:
COMPUCHEM
Lab Coda:
LIBRTY
Contract:
40334
Case No.
CRQL Check Standard Source:
NRAS
EPWO 8 0 6 7
No.:
SDG No.
MY71S3
HP092909BWL
Concentration Units: ug/L
CRQL Check Standard Initial
Final
Analyte True Mercury
1 0.2 J
Found* 0.18 J
Found*
9bR (1)
90
%R (1)
0,24
120
(1) Control Limits: 70-130 with the following exceptions; ICP-AES - Antimony, Lead, and Thallium: 50-150 ICP-MS - Cobalt, Manganese, and Zinc: 50-150 * if applicable, enter the concentration qualifier "J" or "U" after tho concentration in these coltrains (e.g., 0.20U for Mercury)
60 Form IIB-IN
ILM05,4
63 u s EPA - CLP 2B-IN CRQL CHECK STANDARD
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case N o . :
40334
EPWO 8 0 6 7
NRAS N o . :
SDG N o . :
MY71S3
HP092909BWL
CRQL Check Stctndard Source: Concentration Units: ug/L
CRQL Check Standard Initial
Final
Analyte Fotmd*
True Mercury
0.2 1
0.22
%R (1) 110
Fotmd*
%R (1)
0.21
105
(1) Control Limits: 70-130 with the following exceptions: ICP-AES - TVntimony, Lead, and Thallium: 50-15 0 ICP-MS - Cobalt, Manganese, and Zinc: 50-150 * if applicable, enter the concentration
61 Form IIB-IN
ILM05.4
64 u s EPA - CLP 2B-IN CRQL CHECK STANDARD
L a b Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract:
40334
Case No.
EPW08067
SDG No.:
NRAS N o . :
MY71S3
HP092909BWL
CRQL Check Standard Source: Concentration Units: ug/L
CRQL Check Standard Initial
Final
Analyte True Mercury
1
0.2 1
Fotmd*
0.20 J
%R (1) 100
Fotmd*
%R (1)
0.21
105
(1) Control Limits; 70-130 with the follovrLng exceptions: ICP-AES - Antimony, Lead, and Thallitim: 50-150 ICP-MS - Cobalt, Manganese, and Zinc: 50-150 * if applicable, enter the concentration qualifier "J" or "U" after the concentration in these columns (e.g., 0.20U for Mercury)
Form IIB-IN
ILM05.4
62
65 u s EPA - CLP 2B-IN CRQL CHECK STANDARD
L a b Name;
COMPUCHEM
Lab Code;
LIBRTY
Contract;
40334
Case No.
EPW08067
NRAS N o . :
SDG No.
MY71S3
HP0g2909BWL
CRQL Check Standard Source: Concentration Units; ug/L
CRQL Check Standard Initial
Final
Analyte True Mercury
1
Found*
%R (1)
0.2 1
Fotmd*
%R (1)
0.22
110
(1) Control Limits: 70-130 with the following exceptions: ICP-AES - Antimony, Lead, and Thallitim: 50-150 ICP-MS - Cobalt, Manganese, and Zinc; 50-150 * if applicable, enter the concentration qualifier "J" or "U" after the concentration in these coltimns (e.g., 0.20U for Mercury)
63 Form IIB-IN
ILMO5.4
66 u s EPA - CLP 2B-IN CRQL CHECK STANDARD
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: Case N o . :
40334
EPW08067
NRAS N o . :
SDG No.
MY71S3
HP092909BWL
CRQL Check Standard Source: Concentration Units: ug/L
CRQL Check Standard Initial
Final
Analyte True Mercury
Found*
'-aR (1)
0.2|
Found*
"-iR (1)
0.15 J
75
(1) Control Limits: 70-130 with the following exceptions: ICP-AES - Antimony, Lead, and Thallitim: 50-150 ICP-MS - Cobalt, Manganese, and Zinc: 50-150 * if applicable, enter the concentration qualifier "J" or "U" after the concentration in these columns (e.g., 0.20U for Mercury)
64 Form IIB-IN
ILM05.4
67
u s EPA - CLP 3-IN BLANKS
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Case No.
P r e p a r a t i o n Blank Matrix
EPW08067
Contract:
40334
(soil/water) ;
SDG NO.
NRAS N o .
WATER UG/L
Preparation Blank Concentration Units (ug/L or mg/kg) Initial Calibration Blank(ug/L) Analyte Altiminum Calcium Iron Magnesium Mercury
Continuing Calibration Blank (ug/L)
C
1
MY71S3
C
2
C
Preparation Blank C
3
C
M
p p p p
200.000
U
200.000
U
200.000 U
200.000
U
200.000
U
-203.561
J U
223.076
108.822 J 100.000 U
-317,658
J
5000.000
U
100.000
J U
100.000
U
100.000
5000.000
U
5000.000
U
5000.000 U
5000.000
U
5000.000
0.200
U
-0.074
J
0.200
U
0.200
U
1 cv
U
0.200 U 5000.000 U
5000.000
U
5000.000
U
1 p
U
5000.000 U
5000.000
U
5000.000
u 1 p
100.000
Potassium
5000.000
U
5000.000
Soditim
5000.000
U
5000.000
Form III-IN
ILM05.4
i 1 U 1 U 1
65
68
u s EPA - CLP 3-IN BLANKS
L a b Name:
COMPUCHEM
Lab Code:
LIBRTY
P r e p a r a t i o n Blank Matrix
40334
Case N o .
SDG N O .
NRAS N o .
UG/L
(ug/L o r m g / k g ) :
Initial Calibration Blank(ug/L)
Continuing Calibration Blank (ug/L) C
MY71S3
WATER
(soil/water):
P r e p a r a t i o n Blank Concentration Dnits
Analyte
EPWO 8 0 6 7
Contract:
1
1 C
C
2
Preparation Blank 3
C
C
M
35.593|
J
34,506
J
200.000
U
P
-755.211|
J
-319.201
J
-101.397
J
P
Iron
20.866J J
23.573
J
100.000
P
Magnesitim
55.703|
J
60.559
J
5000.000
Potassium
5000,000| U
5000.000
U
5000.000
Sodium
5000.000| U
5000.000
U
5000.000
u u u u
Altimintim Calcitim
Form
III-IN
P P P
ILM05.4
66
69
u s EPA - CLP 3-IN BLANKS
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Preparation Blank Matrix
Contract: Case N o . :
40334
(soil/water) :
EPW08067
NRAS N o . :
SDG NO.:
WATER UG/L
Preparation Blank Concentration Units (ug/L or mg/kg): Initial Calibration Blank(ug/L) Analyte Aluminum Calcitim Iron Magnesium
C
Continuing Calibration Blank (ug/L) 1
C
200.000
U
-653,066
J
100.000 5000.000
Potassium
5000.000
Sodium
5000.000
MY71S3
2
uI u u u
Form III-IN
C
Preparation Blank 3
c
c
1 1 1
M P P P P
1
P P
1
ILMO5.4
67
70
u s EPA - CLP 3-LN BLANKS
L a b Name:
COMPUCHEM
Lab Code:
LIBRTY
Contract: C a s e No. :
Preparation Blank Matrix
40334
(soil/water):
Preparation Blank Concentration Units
UG/L
(ug/L o r m g / k g ) :
Continuing Calibration Blank (ug/L)
Preparation Blank 3
c
U
47.256
J
P
J
448.410
J
P
100.000
U
100.000
U
P
J
5000.000
U
29.265
J
P
J
0.072
J
5000.000
U
5000.000
U
5000.000
5000.000
U
5000.000
U
5000.000
u u
C
1
C
200.000
U
58,057
Calcitim
100.392
J
438.338
Iron
100.000
U
5000.000 0.200
Potassium Soditim
Mercury
MY71S3
WATER
Altimintim
Magnesitim
SDG NO.
NRAS N O .
Initial Calibration Blank(ug/L) Analyte
EPWO 8 0 6 7
C
2
J
200.000
J
-224.962
27.763
J
U
78.124
U
0.078
5000.000
U
5000.000
u
C
M
c:v p p
68 Form I I I - I N
ILM05.4
71
u s EPA - CLP 3-IN BLANKS
L a b Name:
COMPUCHEM
Lab Code:
LIBRTY
Case No.:
Preparation Blank Matrix
40334
(soil/water):
Preparation Blank Concentration Units
NRAS N o . :
Analyte
Calcium Iron Magnesitim Mercury
UG/L
(ug/L o r mg/kg)
Continuing Calibration Blank (ug/L)
C 200.000
MY71S3
SDG NO.i
WATER
Initial Calibration Blank(ug/L)
Aluminum
EPW08067
Contract:
U
1
C
-66.949
J
u u u u u u
5000,000
U
5000.000
100,000
U
100.000
5000.000
U
5000,000
0.200
U
0.200
Potassitim
5000,000
U
5000.000
Sodium
5000,000
u
5000.000
C
2
Preparation Blank 3
C
M
200.000
U
P
J U
213.158
J
P
100.000
U
5000.000
U
25.066
J
P P
-63.156 J
-50.475
-96,010 J 100.000 U
644.669 100.000
5000.000 U
J
i
C
0.200 U
0.200
U
5000.000 U
5000.000
U
5000.000
U
p
5000.000 U
5000.000
U
5000.000
U1
p
Form I I I - I N
CV
ILM05.4
69
72
u s EPA - CLP 3-IN BLANKS
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Preparation Blank Matrix
40334
Case No.
NRAS N o .
(ug/L o r
Initial Calibration Blank(ug/L)
Altiminum
SDG NO.
UG/L
mg/kg):
Continuing Calibration Bla]nJc ( u g / L ) C
1
C
C
2
-35.588
J
5000.000
U
100.000
U
5000.000
U
5000.000 U
0.200
U
0.200 U
Potassitim
5000.000
U
5000.000 U
Soditim
5000.000
U
5000.000 U
Calcitim Iron Magnesitim Mercury
MY71S3
WATER
(soil/water);
Preparation Blank Concentration Units
Analyte
EPWO8067
Contract:
-34.965
Preparation Blank 3
C
C
J
1 1 1 1
-92.555 J 100.000
M
U
0.200
P P P P
1 CV
U
1 P 1 P
70 Form I I I - I N
ILM05.4
73
u s EPA - CLP 3-IN BLANKS
L a b Name:
COMPUCHEM
Lab c o d e :
LIBRTY
Preparation Blank Matrix
Contract: C a s e No.
40334
(soil/water) ;
EPWO8067
SDG NO.
NRAS N o .
WATER UG/L
Preparation Blank Concentration Units (ug/L or mg/kg): Initial Calibration Blank(ug/L) Analyte Mercury
|c
MY71S3
Continuing Calibration Blank (ug/L)
1 [C 1 0.200| U 1
2
C
Preparation Blank
3
1
I^C
1 11
|c
1
M
1 CV
71 Form III-IN
ILM05.4
74 u s EPA - CLP 4A-IN ICP-AES INTERFERENCE CHECK SAMPLE
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
ICP-AES I n s t r u m e n t
Contract:
Case No.;
ICS S o u r c e :
MY71S3
EPA-1206-203
ug/L
Sol.A
sol AB
Sol. A
Final Fotmd
initial Fotmd
True Analyte
SDG N O . :
NRAS N o . :
P3
ID:
Concentration Units:
40334
EPWO8067
%R
Sol AB
%R
Sol .A
%R
Sol.AB
SiR
Aluminum
244000 1
241000
257000
105
253000
105
2550001
105
255000 1
106
Calcium
235000 1
231000
254000
108
251000
109
254000 1 108
255000 1
110
95600 1
94800
102000
107
99900
105
1010001
106
101000 1
107
248000 1
251000
265000
107
261000
104
2650001
107
265000 1
106
0
1.8
4.8
2.21
3.2|
0
945
1050
9851
999 1
Iron Magnesium Potassium Soditim
° 1 ° 1
72 Form I V A - I N
ILM05.4
75 u s EPA - CLP 4A-IN ICP-AES INTERFERENCE CHECK SAMPLE
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
ICP-AES I n s t n i m e n t
Contract:
Case N o . :
ICS S o u r c e :
MY71S3
EPA-120 6-203
ug/L
Initial
True Analyte
SDG N O . :
NRAS N o . :
P3
ID:
Concentration Units:
40334
EPWO8067
S o l .A
S o l AB
Sol. A
%R
Final
Fotmd S o l AB
%R
Sol.A
Found
%R
Sol.AB
%R
Altimintim
244000
1
241000
2570001
105
257000 1
107
Calcitim
235000
1
231000
255000|
109
255000 1
110
95600
1
94800
1020001
107
103000 1
109
248000
I
251000
2700001
109
271000 1
108
°1 °1
0
3.8|
1.8|
0
9321
974 j
Iron Magnesitim Potassitim Soditim
Form IVA-IN
ILM05.4
73
76 u s EPA - CLP 4A-IN ICP-AES INTERFERENCE CHECK SAMPLE
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
ICP-AES I n s t r u m e n t
Contract; Case N o . :
40334
SDG NO.X
NRAS N o . :
P3
ID:
EPWO8067
ICS S o u r c e :
MY71S3
EPA-1206-203
Concentration U n i t s : ug/L
Analyte
Sol .A
Sol AB
Sol .A
Final Found
Initial Fotmd
True
5iR
Sol AB
°'!.R
Sol.A
%R
Sol.AB
?6R
Aluminum
244000 1
241000
2580001
106
256000 1
106
Calcium
235000 1
231000
257000 1 109
257000 1
111
95600 1
94800
1030001
108
103000 1
109
248000 1
251000
272000 1 110
271000 1
108
Iron Magnesitim Potassium Sodium
° 1 ° 1
0 0 .
1 1
Form IVA-IN
4.8|
3.2|
8741
983 1 „ ., . _ l
ILM05.4
74
77 u s EPA - CLP 4A-IN ICP-AES INTERFERENCE CHECK SAMPLE
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
ICP-AES I n s t r t i m e n t
Contract:
Case No.:
ICS S o u r c e :
MY71S3
EPA-1206-203
ug/L
Sol.A
Sol AB
Sol. A
Final Fotmd
Initial Found
True Analyte
SDG NO. :
NRAS N o . :
P3
ID:
Concentration Units:
40334
EPW08067
%R
Sol AB
?4R
Sol. A
%R
Sol.AB
%R
Altiminum
244000 1
241000
252000
103
249000
103
250000 1 102
250000 1
104
Calcitim
235000 1
231000
252000
107
248000
107
2510001
107
250000 j
108
95600 1
94800
100000
105
98800
104
1000001
105
100000 j
105
248000 1
251000
260000
105
258000
103
2630001
106
263000 1
105
0
7.9
4.8
0
1010
1060
Iron Magnesitim Potassitim Soditim
° 1 ° 1
2.41
4.3,
939 1
965 1 1
75 Form
IVA-IN
ILM05.4
78 u s EPA - CLP 4A-IN ICP-AES INTERFERENCE CHECK SAMPLE
L a b Name:
COMPUCHEM
Lab C o d e :
LIBRTY
ICP-AES I n s t r u m e n t
Contract;
Case No.:
ICS S o u r c e :
MY71S3
EPA-1206-203
ug/L
Sol.A
Sol AB
Sol. A
Final Fotmd
Initial Found
True Analyte
SDG N O . :
NRAS N o . :
P3
ID:
Concentration Units:
40334
EPWO 8 0 6 7
%R
Sol AB
%R
Sol. A
%R
Sol.AB
S-cR
Aluminum
244000 1
241000
253000
104
249000
103
256000 1 105
249000 1
103
Calcium
235000 j
231000
251000
107
245000
106
254000 1 108
245000 1
106
95600 1
94800
101000
106
99300
105
1020001
248000 1
251000
260000
105
256000
102
263000 1 106
0
7.1
14.0
8.31
14.2 1
0
1090
1120
1100 1
1020 1
Iron Magnesitim Potassitim Soditim
° 1 ° 1
107
99300 1 105 256000 1
102
1
76 Form IVA-IN
ILM05.4
79 u s EPA - CLP 4A-IN ICP-AES INTERFERENCE CHECK SAMPLE
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
ICP-AES I n s t r u m e n t Concentration
Contract:
Case No.:
ICS S o u r c e :
MY71S3
EPA-1206-203
ug/L
Sol.A
Final Fotmd
Initial Found
True Analyte
SDG NO. :
NRAS N o .
P3
ID:
Units:
40334
EPWO8067
Sol.A
Sol AB
%R
Sol AB
%R
Sol. A
%R
Sol.AB
56R
Aluminum
244000 1
241000
246000
101
248000 1
103
Calcium
235000 j
231000
244000
104
246000 1
106
95600 1
94800
98500
103
99500 1
105
248000 1
251000
255000
103
257000 1
102
0 0
4.5
14.2 1
990
980 1
Iron Magnesitim Potassium Sodium
0 1 0 1
77 Form It/A-IN
ILM05.4
80 u s EPA - CLP 5A-IN MATRIX SPIKE SAMPLE RECOVERY
EPA SAMPLE NO. MY71T5S
Lab Name: COMPUCHEM
Contract: Case No. :
Lab Code: LIBRTY Matrix (soil/water);
WATER
% Solids for Sample;
0.0
40334
Control L i m i t 5-oR
SDG HO. : MY71S3
NRAS N o . : Level
Spiked Sample R e s u l t (SSR)
( l o w / m e d ) : LQW
UG/L
C o n c e n t r a t i o n D n i t s ( u g / i , o r mg/kg d r y w e i g h t ) ; Analyte
EPW08067
C
Sample R e s u l t (SR)
Spike C Added (SA)
Q
94R
M
Altimintim
25202.8900
23480.0700
2000.00
86
P
Iron
44142.7100
43469.0400
1000.00
57
P
5.7100
4.8200
1,00
89
CV
Mercury
Comments:
78 F o r m VA-IN
ILM05.4
81
us EPA - CLP 6-IN DUPLICATES EPA SAMPLE NO. MY71T5D
Lab Name: Lab Code:
Contract;
COMPUCHEM LIBRTY
NRAS N o . ;
Case No.: 40334
Matrix (soil/water):
Level
WATER
?6 Solids for Sample:
0.0
1 1 1
Calcium Iron Magnesium Mercury Potassitim Soditun
Duplicate
5000.0000
1
0.0
(D)
C
1
Altiminum
MY71S3
UG/L
S a m p l e (S)
Control Limit
(low/med):
SDG NO. : LOW
% Solids for Duplicate:
Concentration Units:(ug/L or mg/kg dry weight): Analyte
EPWO8067
C
RPD
Q
M
23480.0700}
23284.0098
1
P
115468.8000|
114639.7031
1
P
43469.0400)
43234,0703
1
P
319136.0000}
303828.8125
5
P
4.8200}
4.7500
1
CV
11296.3400}
11193.1299
1
P
121576.2000]
120309.5000
1
P
Form VI-IN
ILMO
>9^
82 u s EPA - CLP 7-IN LABORATORY CONTROL SAMPLE
COMPUCHEM
L a b Name: Lab Code:
Contract:
LIBRTY
Case No.
40334
EPW08067
NRAS N o :
SDG NO.
MY71S3
S o l i d LCS S o u r c e : A q u e o u s LCS S o u r c e :
EPA-0307
Aqueous Analyte Altimintim Calcium Iron
True
(ug/L) Found
Solid ?tR
2482.0 }
2576.17 }
10180.0 }
9036.60 }
89
5107.0 1
5079.18 }
99 100
True
Found
(mg/kg) C
Limits
'^
104
Magnesltun
6003.0 1
6028,92 |
Potassitun
10008.0 }
8953.48 }
89
Sodium
10039.0}
10227.26}
102
1 1 1 1
80 Form V I I
IN
ILM05.4
83 u s EPA - CLP 7-IN LABORATORY CONTROL SAMPLE
L a b Name: Lab Code:
COMPUCHEM
Contract:
LIBRTY
40334
Case No.
EPWO8067 SDG NO.:
NRAS No:
MY71S3
S o l i d LCS S o u r c e : Aqueous LCS S o u r c e :
EPA-0307
Aqueous Analyte Altimintim Calcitim Iron Magnesitim Potassitim Soditim
(ug/L)
True
Fotmd
2482.0} 10180.0} 5107.0} 6003.oj 10008.0 1 10039.0 1
2481.05} 9529.76} 5018.08} 5855.86} 9005.51} 10035.97 }
Solid %R
True
Found
(mg/kg) C
Limits
100 94 98 98 90 100
^R
1 1 1
Form V I I
IN
ILM05.4
81
84 u s EPA - CLP
8-IN ICP-AES and ICP-MS SERIAL DILUTIONS EPA SAMPLE NO. MY71T5L Lab Name: COMPUCHEM
Contract:
Lab Code: LIBRTY
Case No. :
Matrix (soil/water):
40334
EPWO8067 SDG NO.: MY71S3
NRAS No.
WATER
Level (low/med):
LOW
Concentration Units: ug/L
Analyte
%' Difference
Serial Dilution R e s u l t (S)
I n i t i a l Sample Result (I)
C
C
Altiminum
}}
23480.07
1]
23844.39
Calcitim Iron Magnesium
}} }1 }}
115468.80 43469.04
]} }
121660.20 45939.56
Potassium
}}
11296.34
1} }}
308658.40 9506.61
Soditim
}}
121576.20
Li }
124462.90
1
319136.00 1
Form VIII-IN
Q
1 1 1
2
1
P
5 6
P P
3 J
16
M
E
^1
ILM05.4
P P P
82
85 US EPA - CLP 9-IN METHOD DETECTION LIMITS (ANNUALLY) Lab Name:
C0MPUC3IEM
Lab Code:
LIBRTY
Instrument Type: Preparation Method; Concentration Dnits
_ Case N o . :
EPWO 80 67
NRAS No. :
40334
Instrument ID;
P
Contract:
SDG NO. : Date:
P3
MY71S3
01/15/2010
NPl (ug/L o r m g / k g ) :
Analyte
UG/L
Wave-Length /Mass
CRQL
MDL
Altimintim
308.22
200
31.3
Calcium Iron
317.93
5000
27.3
271.44 279.08
100
13.7 28.0 29.5
Magnesium Potassitim Soditim
766.49 330.23
5000 5000 5000
454
Comment s :
83 Form IX-IN
ILM05.4
86 US EPA - CLP 9-IN METHOD DETECTION LIMITS (ANNUALLY) Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
I n s t r u m e n t Type; P r e p a r a t i o n Method: Concentration Units
Contract: Case No.
40334
NRAS N o . :
I n s t r t i m e n t ID:
P
EPW08067 SDG NO.: Date:
P3
MY71S3 01/15/2010
HWI
(ug/L o r mg/kg)
Analyte
UG/L
Wave-Length /Mass
CRQL
MDL
Altimintim Calcitim
308.22
200
56,6
317.93
5000
111.0
Iron Magnesitim Potassium Soditim
271.44 279.08
100
5000
26.0 21.5
766.49 330,23
5000 5000
26.3 346
Comments:
84 Form IX-IN
ILM05.4
87 US EPA - C L P 9-IN METHOD DETECTION LIMITS (ANNUALLY)
Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
Instrument Type; Preparation
Method:
Concentration Units
Contract: Case No.
NRAS N O . :
40334
Instrtiment
CV
EPWO 8 0 6 7
ID:
SDG N O . :
V4
Date:
MY71S3
01/15/2010
CWI ( u g / L o r mg/kg)
Analyte Mercury
UG/L
Wave-Length /Mass
CRQL
253.70
0.2
MDL
0.065
j
Comments;
85 Form
IX-IN
ILM05.4
88 US EPA - CLP lOA-lN ICP-AES INTERELEMENT CORRECTION FACTORS (QUARTERLY) Lab Name:
COMPUCHEM
Lab Code:
LIBRTY
ICP-AES I n s t r u m e n t
Analyte
Contract: Case N o . :
ID
40334
Wavelength (nm)
SDG N O . :
NRAS No Date:
P3
EPWO 8 0 6 7 MY71S3
07/15/2010
Interelement Correction Factors for: Al
Ca
Fe
0.0000000
0.0000000
Mg
Ag
0.0000000|
0.0000000
0,0000000
0.0000000
0.0000000
0,0000000
0.0000000
0.0004910
0.0000000
0,0000000
0.0000000]
0.0000000 1
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
0,0000000
0.0000000
0,0000000
0.0000000
226,50
0,0000000
0,0000000
0.0000830
0.0000000
0.0000000
317.93
-0.0005930
0,0000000
-0.0005880
0.0000000
0.0000000
Chromium
267.72
0,0000000
0,0000000
0.0000000
0.0000000
0.0000000
Cobalt
228.62
0,0000000
0.0000000
0,0000000
0.0000000
0.0000000
Copper
324.75
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Iron
271.44
0.0000000
0.0000000
0.0000000
-0.0001390
0.0000000
Lead
220.35
0,0005030
0.0000000
0.0000000
0.0000000
0.0000000
Lead
220.35
-0.0003150
0.0000000
0.0000000
0.0000000
0.0000000
Magnesitim
279.08
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Manganese
257.61
0.0000000
0.0000000
0.0000110
0.0000270
0.0000000
Nickel
231.60
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Potassitim
766.49
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Selenium
196.02
0,0000000
0.0000000
0.0000000
0.0000000
0.0014250
Selenium
196.02
0,0000000
0.0000000
-0.0002220
0.0000000
0.0000000
Silver
328.07
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Sodium
330.23
0,0000000
0.0000000
-0.0022970
0.0000000
0.0000000
Thallitim
190.86
-0,0000150
0.0000000
-0.0001380
0.0000000
0.0000000
Vanaditim
292.40
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Zinc
213.87
0.0000000
0.0000000
0.0000710
0.0000000
0.0000000
308.22
0.0000000
Antimony
206,83
0.0000000
0.0000000
Antimony
206.83
0.0000000
0.0000000
Arsenic
189.04
0.0000000
Barium
493.41
0.0000000
Beryllitim
313,04
Cadmium Calcium
Altiminum
Comments:
F o r m XA-IN
86 ILM05.4
89 US EPA - CLP lOB-IN ICP-AES INTERELEMENT CORRECTION FACTORS (QU/UiTERLY) Lab Name:
Lab Code:
Contract:
COMPUCHEM
LIBRTY
ICP-AES I n s t r t i m e n t ID:
Analyte
Case No
40334
NRAS No.
SDG NO.:
Date:
P3
length (nm)
EPWO 8 0 6 7 MY71S3
07/15/2010
Interelement Correction Factors for; As
B
Ba
Be
Cd
Altimintim
308.22
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Antimony
206.83
0.0000000
-0.0002330
0.0000000
0.0000000
-0.0001130
Antimony
206.83
0.0000000
0.0000000
0.0000000
0.0000000 1
0.0000000
Arsenic
189.04
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Barium
493.41
0.0000000
0.0000000
0.0000000
0.0000000
Beryllium
313.04
0.0000000
0.0000000
0.0000000
0.0000000
Cadmitim
226.50
0.0000000
0.0000000
0.0000000
0.0000000
Calcitim
317.93
0.0000000
0.0000000
-0.0018140
Chromitim
267.72
0.0000000
0.0000000
0.0000000
0.0000000
Cobalt
228.62
0.0000000
0.0000000
0.0001700
0.0000000
Copper
324.75
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Iron
271.44
0,0000000
0.0000000
0.0000000
0,0000000
0,0000000
Lead
220.35
0.0000000
0.0001330
0.0000000
0.0000000
0.0000000 1
Lead
220.35
0.0001720
0.0000000
0.0000000
0.0000000
0.0000000 1
Magnesium
279.08
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000 1
Manganese
257.61
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Nickel
231.60
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Potassium
766.49
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000 1
0.0000000 0.0000000 1
-0.0341570 1 -0.0114010 -0.0003480 0.0000000 1
Selenitim
196.02
0.0000000
0.0002860
0.0000000
0.0003730
0.0002570
Selenium
196.02
0.0001070
-0.0002250
0.0000000
0.0000000
0.0000000 1
Silver
328.07
0.0000000
0.0000000
0.0000000
0.0000000
Sodium
330.23
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Thallitim
190.86
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Vanadium
292.40
0.0000000
0.0000000
0.0000000
0.0000000 1
0.0000000
Zinc
213.87
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
1
0,0000000 1
Comment s :
87 Form XB-IN
ILM05.4
90
US EPA - CLP lOB-EM ICP-AES INTERELEMENT CORRECTION FACTORS (QUARTERLY) Lab Name: Lab Code:
Contract:
COMPUCHEM LIBRTY
ICP-AES I n s t r t i m e n t I D :
Analyte
Case No. :
40334
P3
length (nm)
EPWO 8 067
NRAS No.
SDG NO.:
Date:
MY71S3
07/15/2010
Interelement Correction Factors for:
Alumintun
308.22
Co -0.0038960
Cr
Cru
Mn
Mo
0,0000000
0.0000000
0.0000000
0.0000000
Antimony
206.83
0.0000000
0.0079060
0.0000000
0.0000000
-0.0015190
Antimony
206.83
0.0000000
0.0064860
0.0000000
0.0000000
-0.0078240
Arsenic
189.04
0.0000000
-0.0016360
0.0000000
0.0000000
0.0000000
Baritim
493.41
0.0000000
0.0000000
0.0000000 1
0.0000000
0.0000000
Beryllitim
313.04
0.0000000
0,0000000
0.0000000
0.0000000
0.0000000
Cadmivun
226,50
0.0000000
0,0000000
0.0000000
0.0000000
0.0000000
Calcitim
317.93
-0.0185250
-0.0154520
-0.0152030 1 -0.0307490
-0.0247540
Chromium
267.72
0,0000000
0.0000000
0.0000000
0.0000000
0.0000000
Cobalt
228,62
0.0000000
0,0000000
0.0000000
0.0000000
0.0000000
Copper
324.75
0.0000000
0.0000000
0.0000000 1
0.0000000
0.0000000
Iron
271.44
0.0820120
0.0000000
0.0000000
0.0000000
0.0000000
Lead
220.35
-0.0003320
0,0000000
0.0001270
0.0000000
-0.0007370
Lead
220.35
0.0000000
0,0000000
O.OOOOOOOJ
0.0000000
-0.0004410
Magnesium
279.08
0.0000000
0.0000000
O.OOOOOOOJ
0.0000000
0.0000000
Manganese
257.61
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Nickel
231.60
0.0000000
0.0000000
0.0000000 1
0.0000000
0.0000000
Potassitim
766.49
0.0000000
0.0000000
O.OOOOOOOJ
0.0000000
0.0000000
Selenitim
196.02
0.0003650
0,0002730
0.0001210 1
0.0011610
0.0004790
Selenitim
196.02
-0.0002710
0.0000000
0.0000000 1
0.0000980
-0.0002870
Silver
328.07
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Soditim
330.23
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Thallium
190.86
0.0024000
0.0003630
0.0000000
0.0010990
-0,0078300
Vanaditim
292.40
0.0000000
-0.0007730
0.0000000
0.0000000
-0.0062230
Zinc
213.87
0.0000000
0.0000000
0.0005740
0.0000000
0.0000000
Comments:
Form XB-IN
ILM05.4
88
91
US EPA - CLP lOB-IN ICP-AES INTERELEMENT CORRECTION FACTORS (QUARTERLY) Lab Name: Lab Code:
Contract:
COMPUCHEM LIBRTY
ICP-AES Instrument ID:
Analyte
Case No
40334
P3
length (nm)
Altunintim
308.22
EPWO 8 067 SDG NO.:
NRAS N o . : Date:
MY71S3
07/15/2010
Interelement Correction Factors for: Na
Ni
Pb
0.0000000
0.0000000
0.0000000
Sb 0.0000000
Se 0.0000000
Antimony
206.83
0.0000000
-0.0013070
-0.0001290
0.0000000
0.0000000
Antimony
206.83
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Arsenic
189.04
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Barivim
493.41
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Beryllitim
313.04
0.0000000
0.0000000
0,0000000
0.0000000
0.0000000
Cadmitim
226.50
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Calcitim
317.93
0.0000000
-0.0159200
0.0000000
0.0000000
0.0000000
Chromitim
257.72
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Cobalt
228.62
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Copper
324,75
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Iron
271.44
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Lead
220.35
0.0000000
0.0006840
0.0000000
0.0000000
0.0000000
Lead
220.35
0.0000000
0.0001020
0.0000000
0.0000000
0.0000940
Magnesium
279.08
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Manganese
257.61
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Nickel
231.60
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Potassitim
756.49
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Selenitim
196.02
0.0000000
0.0000000
0.0002520
0.0005720
0.0000000
Selenitim
196.02
0.0000000
0.0000000
-0.0001520
0.0000000
0.0000000
Silver
328.07
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Sodium
330.23
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Thallium
190.86
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Vanaditim
292.40
0.0000000
0.0000000
0.0000000
0.0000000
0.0000000
Zinc
213.87
0.0000000
0.0033600
0.0000000 1
0.0000000
0.0000000
Comment s :
89 Form XB-IN
ILM05.4
92 US EPA - CLP lOB-IN ICP-AES INTERELEMENT CORRECTION FACTORS (QUARTERLY) L a b Name:
Contract:
COMPUCHEM
Lab Code:
LIBRTY
ICP-AES I n s t r u m e n t I D :
Analyte
40334
Case No
EPWO 80 67
NRAS No,
SDG NO.:
Date:
P3
MY71S3
07/15/2010
Interelement Correction Factors for:
length (nm)
Sn
Ti
Tl
V
Zn
308.22
0.0000000
Antimony
206.83
-0.0053580
0.0007680
Antimony
206.83
0,0010120
0.0001490
0.0000000 1
0.0000000 1
0.0000000
189.04
0,0000000
0.0000000
0.0000000
0.0000000 1
0,0000000 1
493.41
0,0000000
0.0000000
O.OOOOOOOJ
0.0000000 1
0.0000000 1
313.04
0.0000000
-0.0008250
0.0000000
0.0003640 1
0.0000000 1
226.50
0,0000000
0.0000000
O.OOOOOOOJ
0.0000000 1
0.0000000
317.93
-0,0236050
-0.0603250
O.OOOOOOOJ
-0.0159670 |
0.0000000
267.72
0.0000000
0.0000000
0.0000000 1 -0.0005100 1
0.0000000
228.62
0.0000000
0.0018940
0.0000000 1
0.0000000 1
0.0000000
324.75
0.0000000
0.0000000
0.0000000
0,0000000 j
0.0000000
271.44
0.0000000
0.0000000
0.0000000
0.0104780 1
0.0000000
Altimintim
1 Arsenic
1 Baritim 1 Beryllitim 1 Cadmitim 1 Calcitim 1 Chromitim 1 Cobalt Copper
1 Iron I Lead 1 Lead I Magnesitim 1 Hanganese 1 Nickel
0.0000000 1 -0.0209750
0.0000000
-0.00012901
0.0000000
-0.0053490 | -0.0001820
220.35 1 0.0006470
0.0000000
0.00000001
-0.0001620 |
0.0001750
220.35 1-0.0001380
0.0000000
O.OOOOOOOJ
0.0000000 1
0.0000000
1 Potassitim
279.08 257.61 231.60 766.49
O.OOOOOOOJ
0.0000000 1
0.0000000
Selenium
196.02
0,0008360
0.0005590
0.0004300 1
0,0000000
0,0002870
Selenitim
196.02
0.0000000
0.0000000
O.OOOOOOOJ
Silver
328.07
0.0000000
0,0000000
O.OOOOOOOJ
-0.0025350 |
0.0000000
Soditim
330.23
0.0000000
0.0000000
O.OOOOOOOJ
0.0000000 1
0.0530470
11 11 11 11
0.0000000
0.0000000 1
0.0000000 1
0.0000000
0.0000000
0.0000000
0.0000000 1 -0.0001960 |
0.0000000
0,0000000
0.0000000
O.OOOOOOOJ
0.0000000
0.0000000
O.OOOOOOOJ
0.0000000
0.0000000 1 |
0.0000000 1 -0,0001650
Thallitim
190.86
0.0000000
0.0017100
O.OOOOOOOJ
0,0015900
|
0.0000000
Vanaditim
292.40
0.0000000
0.0000000
O.OOOOOOOJ
0.0000000 1
0.0000000
Zinc
213.87
0.0000000
0.0000000
O.OOOOOOOJ
0.0000000 1
0.0000000
Comments:
Form XB-IN
ILM05,4
90
93
US EPA - CLP ll-IN ICP-AES AND ICP-MS LINEAR RANGES (QUARTERLY) L a b Name:
COMPUCHEM
Lab Code:
LIBRTY
ICP I n s t r u m e n t
ID:
Contract: Case N o . :
40334
NRAS N o . :
P3
Date:
Analyte
EPW08067
Integ. Time (Sec.)
SDG NO.
07/15/2010
Concentration (ug/L)
M
1 Aluminum
15.00
400000.0
P
1 Calcivun
15.00
400000.0
F
15.00
700000.0
P
1 Magnesium
15.00
300000.0
P
Potassitim
15.00
400000.0
P
Soditim
15,00
700000.0
P
Iron
MY71S3
Comments;
ILM05,4 Form XI-IN
91
94
US EPA - CLP 12-IN PREPARATION LOG
L a b Name: Lab Code:
Contract:
COMPUCHEM LIBRTY
P r e p a r a t i o n Method;
EPA Sample No. LCSW MY71S3 MY71S5 MY71S7 MY71S9 MY71T1 MY71T3 MY71T7 MY71T9 MY71W1 MY71W5 MY71W9 MY71X1 MY71X3 MY71X5 MY71X6 MY71X8 MY71Y0 PBW
Case N o . :
40334
EPWO8067
NRAS No.:
SDG N O . :
MY71S3
HWI
Preparation Date
Weight (gram)
07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010
Volume(mL) 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50
Comment s :
92 Form X I I - I N
ILM05.4
95
US EPA - CLP 12-IN PREP/U^TION LOG
L a b Name:
COMPUCHEM
Lab Code:
LIBRTY
Preparation
Method:
EPA Sample No. LCSW MY71T5 MY71T5D MY71T5S PBW
Contract: Case No.:
40334
EPW08067
NRAS No.:
SDG NO.:
MY71S3
HWI
Preparation Date
Weight (gram)
08/10/2010 08/10/2010 08/10/2010 08/10/2010 08/10/2010
Volume(mL) 50 50 50 50 50
Comments:
Form XII-IN
ILM05.4
93
96
u s EPA - CLP 12-IN PREPARATION LOG
Lab Name: COMPUCHEM Lab Code:
LIBRTY
Preparation Method:
EPA Sample No. CCB CCB CCB CCB CCB CCB CCB CCV CCV CCV CCV CCV CCV CCV CRI CRI CRI CRI ICB ICB ICB ICV ICV ICV MY71S3 MY71S5 MY71S7 MY71S9 MY71T1 MY71T3 MY71T5 MY71T5D MY71T5S MY71T7 MY71T9 MY71W1
Contract: Case No.:
40334
EPWO8067 SDG NO. :
NRAS No.:
MY71S3
CWI
Preparation Date
Weight (gram)
07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010
Volume(mL) 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100
Comments:
Form X I I - I N
ILM05,4
94
97
US EPA - CLP 12-IN PREPARATION LOG
L a b Name;
_
COMPUCHEM
Lab C o d e :
LIBRTY
Preparation
Method:
EPA Sample N o .
MY71W5 MY71W9 MY71X1 MY71X3 MY71X5 MY71X6 MY71X8 MY71Y0 PBW SO SO.2 SO.5 Sl SIO S5
C a s e No.
40334
Contract:
EPWO 8 0 6 7
NRAS N o . :
SDG NO.
MY71S3
CWI
Preparation Date
weight (gram)
07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010 07/29/2010
Voltime (mL)
100 100 100 100 100 100 100 100 100 100 100 100 100 100 100
Comment s :
Form X I I - I N
ILM05,4
95
98
US E P A - C L P 13-IN ANALYSIS RUN LOG Lab Name: Lab Code;
Contract:
COMPUCHEM LIBRTY
Instrument ID:
Case No.I
40334
SDG No. : MY71S3
NRAS No.
P3
Analysis Method: End Date:
Start Date: 08/08/2010 EPA Sample NO.
EPW08067
08/08/2010 Analytes
D/F
Time
A s A L B S
B B A E
C D
C A
c c c u
R O
F B
p M M B G N
H N K S A N G I E G A
X
X
X
X
X
X
X
SO
1.0
1011
S
1.0
1018
S
1.0
1025
S
1.0
1031
s
1.0
1036
ICV
1.0
1043
X
X
X
X
X
X
1.0
1050
X
X
X
X
X
X
CRI
1.0
1057
ICSA
1.0
1104
X
X
X
X
X
X
ICSAB
1.0
llll
X
X
X
X
X
X
CCV
1.0
1118
X
X
X
X
X
X
CCB
1.0
1125
X
X
x^
X
X
X
ZZZZZZ
1.0
1136
ZZZZZZ
1.0
1143
ZZZZZZ
1.0
1150
ZZZZZZ
1.0
1157
ZZZZZZ
1.0
1204
ZZZZZZ
5.0
1211
ZZZZZZ
1.0
1213
ZZZZZZ
1.0
1225
ZZZZZZ
1.0
1232
ZZZZZZ
1.0
1239
CCV
1.0
1246
X
X
X
X
X
X
CCB
1.0
1253
X
X
X
X
X
X
ZZZZZZ
1.0
1300
ZZZZZZ
1.0
1307
ZZZZZZ
1.0
1314
ZZZZZZ
1.0
1321
PBW
1.0
1328
X
X
X
X
X
X
LCSW
1.0
1335
X
X
X
X
X
X
ZZZZZZ
1.0
1342
CRI
1.0
1349
ICSA
1.0
1356
X
X
X
X
X
X
ICSAB
1.0
1403
X
X
X
X
X
X
1.0
1410
X
X
X
X
X
X
ICB
CCV
X
X
X
X
T V L
Z C N N
X
Form XIII-IN
CLM|§.^
99
US EPA - CLP 13-IN ANALYSIS RUN LOG L a b Name:
COMPUCHEM
Lab Code:
LIBRTY
Instrtiment
Case No.:
40334
Analysis
08/08/2010
End D a t e :
EPA Sample NO.
EPWO8067 SDG N O . :
NRAS N o . :
P3
ID:
Start Date:
Contract:
MY71S3
Method: 08/08/2010 Analytes
D/F
Time
CCB
1.0
1417
ZZZZZZ
1.0
1424
ZZZZZZ
1.0
1431
ZZZZZZ
5.0
1438
ZZZZZZ
1.0
1445
My71S3
1.0
MY71S5
1.0
MY71S7
1.0
MY71S9
A L
s
A
B
s
B B A E
C D
C A
c c c R o u
F E
p M M B G N
H N K s A G I E G
N
X
X
X
X
X
X
1452
X
X
X
X
X
X
1459
X
X
X
X
X
X
1505
X
X
X
X
X
X
1.0
1513
X
X
X
X
X
X
MY71T1
1.0
1520
X
X
X
X
X
X
MY71T3
1.0
1527
X
X
X
X
X
X
CCV
1.0
1534
X
X
X
X
X
X
CCB
1.0
1541
X
X
X
X
MY71T7
1.0
1548
X
X
X
X X
X X
X
MY71T9
1.0
1555
X
X
X
X
X
X
MY71W1
1.0
1602
X
X
X
X
X
My71W5
1.0
1609
X
X
X
X
X
My71W9
1.0
1616
X
X
X
X
X
MY? 1X1
1.0
1623
X
X
X
X
X
MY? 1X3
1.0
1630
X
X
X
X
X
X
CRI
1.0
1637
ICSA
1.0
1644
X
X
X
X
X
X
ICSAB
1.0
1651
X
X
X
X
X
X
CCV
1.0
1658
X
X
X
X
X
X
CCB
1.0
1705
X
X
X
X
X
X
MY71X5
1.0
1712
X
X
X
X
X
X
MY71X6
1.0
1719
X
X
X
X
X
X
MY71X8
1.0
1726
X
X
X
X
X
X
MY71Y0
1.0
1733
X
X
X
X
X
X
ZZZZZZ
1.0
1740
ZZZZZZ
1.0
1747
ZZZZZZ
1.0
1754
ZZZZZZ
1.0
1801
ZZZZZZ
1.0
1808
ZZZZZZ
5.0
1815
Form X I I I - I N
X
T V L
z c N
N
^"^f-
100
US EPA - CLP 13-IN ANALYSIS RUN LOG Lab Name: Lab Code:
COIPUCHEM LIBRTY
Instrument ID:
Contract: 40334
Case No.
SDG No. : MY71S3
NRAS No.
P3
Analysis Method: End Date:
Start Date: 08/08/2010 EPA Sample NO.
EPWO8067
08/08/2010 Analytes
Time
D/F
A s A L B S
B B A E
C D
C A
c c c R 0 u
F E
p M M B G N
H N K s A N T V G X E G A L
CCV
1.0
1822
X
X
X
X
X
X
CCB
1.0
1829
X
X
X
X
X
X
ZZZZZZ
1.0
1836
ZZZZZZ
1.0
1843
ZZZZZZ
1.0
1850
ZZZZZZ
1.0
1857
ZZZZZZ
1.0
1904
ZZZZZZ
1.0
1911
ZZZZZZ
1.0
1918
CRI
1.0
1925
ICSA
1.0
1932
X
X
X
X
X
X
ICSAB
1.0
1939
^
X
X
X
X
X
CCV
1.0
1946
X
X
X
X
X
X
CCB
1.0
1953
X
X
X
X
X
X
Form XIII-IN
Z C N N
CLMQ^ .4
101
US EPA - CLP 13-IN ANALYSIS RUN LOG Lab Name:
COMPUCHEM LIBRTY
Lab Code: Instrtiment Start
Case No.:
40334
Analysis
08/10/2010
End D a t e :
EPA Sample NO.
EPW08067 SDG N o . :
NRAS N o . ;
P3
ID:
Date:
Contract:
MY71S3
Method: 08/10/2010 Analytes
D/F
Time
A s A L B s
B B A E
C D
C A
c c c R o D
F E
p M M B G N
H N K s A G I E G
X
X
X
X
X
X
X
N T V A L
SO
1.0
1035
S
1.0
1042
S
1.0
1049
S
1.0
1055
S
1.0
1100
ICV
1.0
1107
X
X
X
X
X
X
ICB
1.0
1114
X
X
X
X
X
X
CRI
1.0
1121
ICSA
1.0
1128
X
X
X
X
X
X
ICSAB
1.0
1135
X
X
X
X
X
X
CCV
1.0
1142
X
X
X
X
X
X
CCB
1.0
1149
X
X
X
X
X
X
ZZZZZZ
1.0
1159
ZZZZZZ
1.0
1206
ZZZZZZ
1.0
1214
ZZZZZZ
1.0
1221
ZZZZZZ
1.0
1228
ZZZZZZ
5.0
1238
ZZZZZZ
1.0
1245
ZZZZZZ
1.0
1252
ZZZZZZ
1.0
1259
MY71W1
2.0
1306
CCV
1.0
1313
X
X
X
X
X
X
CCB
1.0
1320
X
X
X
X
X
X
My71W9
2.0
1328
X
MY71X1
2.0
1335
X
CRI
1.0
1342
ICSA
1.0
1349
X
X
X
X
X
X
ICSAB
1.0
1355
X
X
X
X
X
X
CCV
1.0
1403
X
X
X
X
X
X
CCB
1.0
1410
X
X
X
X
X
X
X
X
X
X
Z C N N
X
X
Form
XIII-IN
CLMg^.
102
US EPA - CLP 13-IN ANALYSIS RUN L O G L a b Name:
COMPUCHEH LIBRTY
Lab Code: Instrument
40334
Case No.
SDG N o . :
Analysis
08/12/2010
End D a t e :
EPA Sample NO.
EPWO8067
NRAS N o .
P3
ID:
Start Date:
Contract:
MY71S3
Method: 08/12/2010 Analytes
Time
D/F
SO
1.0
1054
S
1.0
1101
S
1.0
1108
S
1.0
1113
S
1.0
1119
ICV
1.0
1126
ICB
1.0
1133
CRI
1.0
1140
ICSA
1.0
1147
ICSAB
1.0
1154
CCV
1.0
CCB ZZZZZZ
A s A L B s
B B A E
C D
C A
X
X
X
X
c c c R o u
H N K s A N G I E G A
F E
p M M B G N
X
X
X
X
X
X
X
T V L
z C N N
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
1201
X
X
X
X
X
X
1.0
1208
X
X
X
X
X
X
1.0
1218
ZZZZZZ
1.0
1225
ZZZZZZ
1.0
1232
ZZZZZZ
1.0
1239
ZZZZZZ
1.0
1257
ZZZZZZ
1.0
1304
ZZZZZZ
1.0
1311
ZZZZZZ
1.0
1318
ZZZZZZ
1.0
1325
ZZZZZZ
1.0
1335
CCV
1.0
1342
X
X
X
X
X
X
CCB
1.0
1349
X
X
X
X
X
X
ZZZZZZ
1.0
1357
CRI
1.0
1404
ICSA
1.0
1411
X
X
X
X
X
X
ICSAB
1.0
1413
X
X
X
X
X
X
CCV
1.0
1425
X
X
X
X
X
X
CCB
1.0
1432
X
X
X
X
X
X
PBW
1.0
1440
X
X
X
X
X
X
LCSW
1.0
1447
X
X
X
X
X
X
MY71T5
1.0
1454
X
X
X
X
X
X
X
X
X
MY71T5D
1.0
1501
X
MY71T5S
1.0
1508
X
X Form X I I I - I N
^^5-
103
US EPA - CLP 13-IN /yV/a.YSIS RUN LOG COMPUCHEM
L a b Name: Lab Code:
LIBRTY
Instrtiment
ID:
Start Date:
Contract:
40334
Case No.
SDG N o . :
NRAS N o .
P3
Analysis
08/12/2010
Analytes D/F
Time
A s A L B S
B B A E
C C D A
c C C F R O u E
p M M B G N
5.0
1515
ZZZZZZ
1.0
1522
ZZZZZZ
1.0
1600
CCV
1.0
CCB
1.0
MY71T5
2.0
1624
X
MY71T5D
2.0
1631
X
MY71T5L
10.0
1638
X
ZZZZZZ
1.0
1648
CRI
1.0
1655
ICSA
1.0
1702
X
X
ICSAB
1.0
1709
X
CCV
1.0
1716
X
CCB
1.0
1723
X
MY71T5L
MY71S3
Method:
End D a t e :
08/12/2010
EPA Sample NO.
EPWO8067
X
X
X
1607
X
X
X
1614
X
X
X
H N K s A N G I E G A X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
Form X I I I - I N
T V L
z N
C N
, 1 ^ ^ .
104
US EPA - C L P 13-IN ANALYSIS RUN LOG Lab Name:
COMPUCHEM LIBRTY
Lab Code:
I n s t r t i m e n t ID: S t a r t Date:
Contract; Case N o . :
40334
SDG No. : MY71S3
NRAS N o . :
V4
A n a l y s i s Method: End D a t e :
08/02/2010
EPA Sample NO.
EPW08067
CV
08/02/2010 Analytes
D/F
Time
A S A L B S
B B A E
C D
C A
C C R O
c u
F E
P M M B G N
H N K s A N T V E G A L G I
|so
1.0
0948
X
{so.2
1.0
0950
X
|S0.5
1.0
0952
X
|si
1.0
0954
X
|S5
1.0
0956
X
1 SIO 1 ICV
1.0
0958
X
1.0
1000
X
|lCB
1.0
1002
X
CRI
1.0
1004
X
CCV
1.0
1006
X
CCB
1.0
1007
X
PBW
1.0
1009
X
MY71T5
1.0
1011
X
MY71T5D
1.0
1014
X
MY71T5S
1.0
1016
X
MY71S3
1.0
1018
X
MY71S5
1.0
1020
X
MY71S7
1.0
1022
X
My71S9
1.0
1024
X
MY71T1
1.0
1026
MY71T3
1.0
1028
X
CCV
1.0
1030
X
CCB
1.0
1032
X
MY71T7
1.0
1034
X
MY71T9
1.0
1035
X
MY71W1
1.0
1037
X
MY71W5
1.0
1039
X
MY71W9
1.0
1041
X
MY71X1
1.0
1043
X
MY71X3
1.0
1045
MY71X5
1.0
1048
X
MY71X6
1.0
1050
X
CHI
1.0
1051
X
CCV
1.0
1053
X
CCB
1.0
1055
X
Form X I I I - I N
Z C N N
CL^|.
105
US EPA - CLP 13-IN ANALYSIS RUN LOG Lab Name:
Lab Code:
COMPUCHEH
LIBRTY
Instrtiment ID:
Contract; 40334
Case No.
NRAS No. :
V4
SDG NO.
Analysis Method: End D a t e :
Start Date: 08/02/2010 EPA Sample NO.
EPWO8067 MY71S3
CV
08/02/2010 Analytes
D/F
Time
A S A L B S
B B A E
C D
C A
C C C F R 0 D Z
P M M B G N
H N K S A N E G A G I
SO
1.0
1617
X
SO.2
1.0
1619
X
SO.5
1.0
1621
X
Sl
1.0
1622
X
S5
1.0
1625
X
SIO
1.0
1627
X
ICV
1.0
1629
X
ICB
1.0
1631
X
CRI
1.0
1632
X
CCV
1.0
1634
X
CCB
1.0
1636
X
MY71X8
1.0
1638
X
MY71Y0
1.0
1642
X
ZZZZZZ
1.0
1644
CRI
1.0
1646
X
CCV
1.0
1647
X
CCB
1.0
1649
X
Form X I I I - I N
T V L
Z C N N
^H^§ . 4
106
US EPA - C L P 13-IN ANALYSIS RUN LOG Lab Name:
COMPUCHEM LIBRTY
Lab Code: Instrument
ID:
Start Date:
Contract: Case N o . ;
40334
SDG N o . :
NRAS N o .
V4
A n a l y s i s Method: End D a t e :
08/02/2010
EPA Sample NO.
EPW08067
CTV
08/02/2010
Analytes D/F
Time
A S A L B S
B B A E
C D
C A
C C C F R O u E
P M M B G N
H N K S A N E G A G I
SO
1.0
1803
X
so.2
1.0
1805
X
SO.5
1.0
1807
X
Sl
1.0
1810
X
S5
1.0
1811
X
SIO
1.0
1813
X
ICV
1.0
1816
X
ICB
1.0
1818
X
CRI
1.0
1820
X
CCV
1.0
1821
X
1 CCB
1.0
1823
X
IZZZZZZ
1.0
1825
ZZZZZZ
1.0
1827
ZZZZZZ
1.0
1829
ZZZZZZ
1.0
1832
ZZZZZZ
1.0
1834
ZZZZZZ
1.0
1836
ZZZZZZ
1.0
1838
ZZZZZZ
1.0
1840
ZZZZZZ
1.0
1842
ZZZZZZ
5.0
1844
CCV
1.0
1846
X
CCB
1.0
1848
X
ZZZZZZ
1.0
1850
ZZZZZZ
1.0
1852
ZZZZZZ
1.0
1854
ZZZZZZ
1.0
1856
ZZZZZZ
1.0
1858
ZZZZZZ
1.0
1901
ZZZZZZ
5.0
1903
ZZZZZZ
1.0
1905
CRI
1.0
1906
X
CCV
1.0
1908
X
CCB
1.0
1911
X
1.0
1912
ZZZZZZ
MY71S3
Form X I I I - I N
T V L
Z C N N
[L^^^.^
107
US EPA - C L P 13-IN ANALYSIS RUN LOG L a b Name:
COMPUCHEM
Lab Code:
LIBRTY
Instrument
ID:
S t a r t Date:
Contract: Case No.t
40334
SDG N o . : M Y 7 1 S 3
NRAS N o . :
V4
A n a l y s i s Method: End D a t e :
08/02/2010
EPA Sample NO.
EPWO 8 0 6 7
CV
08/02/2010 Analytes
Time
D/F
A Ii
S A B S
B A E
C D
C A
C C C P R O U E
P M M B G
H N K S A G I E G
ZZZZZZ
1.0
1914
ZZZZZZ
1.0
1916
ZZZZZZ
1.0
1919
ZZZZZZ
1.0
1920
ZZZZZZ
1.0
1923
ZZZZZZ
1.0
1925
ZZZZZZ
1.0
1926
ZZZZZZ
1.0
1923
CCV
1.0
1930
X
CCB
1.0
1932
X
ZZZZZZ
1.0
1934
ZZZZZZ
1.0
1936
ZZZZZZ
1.0
1939
ZZZZZZ
1.0
1941
ZZZZZZ
1.0
1943
ZZZZZZ
1.0
1945
ZZZZZZ
1.0
1947
ZZZZZZ
1.0
1948
CRI
1.0
1950
X
CCV
1.0
1952
X
CCB
1.0
1954
X
ZZZZZZ
1.0
1956
ZZZZZZ
1.0
1958
ZZZZZZ
1.0
2000
ZZZZZZ
1.0
2002
ZZZZZZ
1.0
2004
MY71T1
3.0
2006
X
MY71X3
3.0
2008
X
ZZZZZZ
1.0
2010
ZZZZZZ
1.0
2012
ZZZZZZ
1.0
2014
CCV
1.0
2016
X
CCB
1.0
2018
X
ZZZZZZ
1.0
2020
ZZZZZZ
1.0
2022
Form X I I I - I N
N A
T V L
Z C N N
[LIfg§.
108
US E P A - C L P 13-IN ANALYSIS RUN L O G L a b Name:
COMPUCHEM
Lab Code:
LIBRTY
Instrtiment Start
C a s e NO.
40334
SDG N o . :
Analysis
08/02/2010
End D a t e :
EPA Sample NO.
EPWO8067
NRAS N o .
V4
ID:
Date:
Contract:
Method:
MY71S3
CV
08/02/2010 Analytes
Time
D/F
A S A L B S
B B A E
C C D A
C C R 0
c u
F E
P M M B G N
H N K S A N E G A G I
ZZZZZZ
1.0
2024
ZZZZZZ
1.0
2026
ZZZZZZ
1.0
2028
ZZZZZZ
1.0
2030
ZZZZZZ
1.0
2032
ZZZZZZ
1.0
2034
CRI
1.0
2036
X
CCV
1.0
2033
X
CCB
1.0
2040
X
Form X I I I - I N
T V L
Z C N N
^^1-
109
3. Raw Data For each reported value, the laboratory shall include in the data package all raw data used to obtain that value. This applies to all required QA/QC measurements, instrument standardization, as well as all sample analysis results. This does not apply to the quarterly verification of method and instrument parameters submitted as a part of each data package. The order of the raw data in the data package shall be: ICP-AES, Graphite Furnace AA (if used), ICP-MS, mercury, and cyanide (if a target analyte). Raw data shall be labeled with EPA sample numbers and appropriate codes in order to identify: - calibration standards, including source and preparation date - initial and continuing calibration blanks and preparation blanks - initial and continuing calibration verification standards, interference check samples, serial dilution samples, CRQL check standard, Laboratory Control Sample, and post digestion spike - diluted and undiluted samples (by EPA sample number) and all weights, dilutions, and volumes used to obtain the reported values - duplicates - spikes (indicating standard solutions used, final spike concentrations, and volumes involved). - instrument used, any instrument adjustments, data corrections or other apparent anomalies on the measurement record, including all data voided or data not used and a brief written explanation - time and date of each analysis (instrument run logs can be submitted if they contain this information)
107
110
Maintenance:
Daily Instrument Profile
\\o^f.
Nebulizer pressure: 3 ^ Peak position: "^ O y O Peak intensity: 2 Vernier position: _
Printed: 8/10/2010 11:26:51 AM Method(s)
(circle one): (^ ILM05.4
Operator(s):
)6010B
6010C
j\Qyy CyZ
Other
Date/Time Oft, oft |ft |e)- l(
to
Oft-Og^P
Specified element(s) fail(s) high Specified element(s) fait(s) low COPY RR Re-run sample(s) neat ^jBQBIJtepCWaEWTS WCLUWcD RR#X Re-run at a iV-fold dilution #X Sample run at a #-fold dilution (aliquot of sample diluteci with acidified water) Matrix = leachate JSeMlSi W Matrix = water Matrix = solid Matrix = bioloqical tissue
SDG MC0021 MY71S3
Matrix
^(
• ^ J 3
IN CSF-JllLL'' T-
Comments
H
<2/A^\^n^''^r[^
|g>U
A\> < ^
-J^ li ICP Run Log (P3) MY71S4
Y^
^ /^\/A^lf^.
\\o^
3^ KB
^
V l L ^ - r . o r J ^ P l L o - ) I '^T^^
File Name: P30808 Seq
Sample ID
Client ID
Sample Type
DF
Date
Time
SDG
1
CALI
so BLANK
CALIB STD
08/08/10
10:11:45
2
CAL2
S RSTD-1
CALIB STD
08/08/10
10:18:46
3
CAL4
S RSTD-3
CALIB STD
08/08/10
10:25:47
4
CAL3
S RSTD-2
CALIB STD
08/08/10
10:31:14
5
CAL5
S RSTD-4
CALIB STD
08/08/10
10:36:42
6
ICVl
ICV1
ICV
08/08/10
10:43:43
7
ICBI
ICB
ICB
08/08/10
10:50:44
8
CRL1
CRI
CRI
08/08/10
10:57:44
9
IPAI
ICSA
ICS
08/08/10
11:04:44
10
IFB1
ICSAB
ICS
08/08/10
11:11:44
11
CCVl
CCV
CCV
08/08/10
11:18:45
12
CCB1
CCB
CCB
08/08/10
11:25:47
13
0080340-BLK1
PBW
PBW
08/08/10
11:36:22
MC0021
14
0080340-BSI
LCSW
LCS
08/08/10
11:43:22
MC0021
15
1008010-04
MC0031
SAMPLE
08/08/10
11:50:22
MC0021
16
0080340-DUP1
MC0031D
SAMPLE
08/08/10
11:57:22
MC0021
Action Needed
The presence of the Chemist's/Analyst's employee ID number, or signature, on this njn log attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials of the lab supervisor and a QA department representative, signifying approval of the deviation.
Reviewed By
.y
'ZyZir^
Date:
t-lb-JO
Page 1 of 4
108
111 ICP Run Log (P3) File Name: P30808 Seq
Sample ID
Sample Type
DF
Date
Time
SDG
17
0080340-MS1
MC0031S
SAMPLE
1
08/08/10
12:04:22
MC0021
18
SRD1
MC0031L
SAMPLE
5
08/08/10
12:11:22
MC0021
19
0080340-PS1
MC0031A
SAMPLE
08/08/10
12:18:22
MC0021
20
1008010-01
MC0021
SAMPLE
08/08/10
12:25:22
MC0021
21
1008010-02
MC0029
SAMPLE
08/08/10
12:32:22
MC0021
22
1008010-03
MC0030
SAMPLE
08/08/10
12:39:22
MC0021
23
CCV2
CCV
CCV
08/08/10
12:46:23
24
CCB2
CCB
CCB
08/08/10
12:53:25
25
1008010-05
MC0032
SAMPLE
08/08/10
13:00:25
MC0021
26
1008010-06
MC0033
SAMPLE
08/08/10
13:07:25
MC0021
27
1008010-07
MC0034
SAMPLE
08/08/10
13:14:25
MC0021
28
1008010-08
MC0035
SAMPLE
08/08/10
13:21:26
MC0021
29
0072821-BLKl
PBW
PBW
08/08/10
13:28:27
MY71S3
30
0072821-BS1
LCSW
LCS
08/08/10
13:35:27
MY71S3
31
1007157-07
MY71T5
SAMPLE
08/08/10
13:42:28
MY71S3
32
CRL2
CRI
CRI
08/08/10
13:49:28
33
IFA2
ICSA
ICS
08/08/10
13:56:28
34
IFB2
ICSAB
ICS
08/08/10
14:03:29
35
CCV3
CCV
CCV
08/08/10
14:10:30
36
CCB3
CCB
CCB
08/08/10
14:17:31
37
0072821-DUPI
MY71T5D
SAMPLE
08/08/10
14:24:32
MY71S3
38
0072821-MS1
MY71T5S
SAMPLE
08/08/10
14:31:32
MY71S3
39
SRD2
MY71T5L
SAMPLE
08/08/10
14:38:32
MY71S3
40
0072821-PS1
MY71T5A
SAMPLE
08/08/10
14:45:32
MY71S3
41
1007157-01
MY71S3
SAMPLE
08/08/10
14:52:32
MY71S3
42
1007157-02
MY71S5
SAMPLE
08/08/10
14:59:33
MY71S3
43
1007157-03
MY71S7
SAMPLE
08/08/10
15:06:32
MY71S3
44
1007157-04
MY71S9
SAMPLE
08/08/10
15:13:32
MY71S3
45
1007157-05
MY71T1
SAMPLE
08/08/10
15:20:32
MY71S3
46
1007157-06
MY71T3
SAMPLE
08/08/10
15:27:33
MY71S3
47
CCV4
CCV
CCV
08/08/10
15:34:34
48
CCB4
CCB
CCB
08/08/10
15:41:35
Client ID
Action Needed
M
c^.,0^1
Z%
AtiAh?r ».Kib!4-4Z->A. Vi^T-9ri
f^'
yy ^
^ ^ l ^ ^ 4 •
iuZU J '
The presence of the Chemist's/Analyst's employee ID number, or signalure, on this run log attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials of the lab supervisor and a QA department representative, signifying approval of the deviation.
Reviewed By;
y^^y^^
Date:
"S-16-/0
Page 2 of 4
109
112 ICP Run Log (P3) File Name: P30808 Date
Time
SDG
08/08/10
15:48:36
MY71S3
SAMPLE
08/08/10
15:55:36
MY71S3
MY71W1
SAMPLE
08/08/10
16:02:36
MY71S3
1007157-11
MY71W5
SAMPLE
08/08/10
16:09:37
MY71S3
53
1007157-12
MY71W9
SAMPLE
08/08/10
16:16:37
MY71S3
54
1007157-13
MY71X1
SAMPLE
08/08/10
16:23:38
MY71S3
55
1007157-14
MY71X3
SAMPLE
08/08/10
16:30:38
MY71S3
56
CRL3
CRI
CRI
08/08/10
16:37:38
57
IF A3
ICSA
ICS
08/08/10
16:44:38
58
IFB3
ICSAB
ICS
08/08/10
16:51:38
59
CCV5
CCV
CCV
08/08/10
16:58:40
60
CCB5
CCB
CCB
08/08/10
17:05:41
61
1007157-15
MY71X5
SAMPLE
08/08/10
17:12:42
MY71S3
62
1007157-16
MY71X6
SAMPLE
08/08/10
17:19:42
MY71S3
63
1007157-17
MY71X8
SAMPLE
08/08/10
17:26:42
MY71S3
64
1007157-18
MY71Y0
SAMPLE
08/08/10
17:33:42
MY71S3
65
0080607-BLK1
PBW
PBW
08/08/10
17:40:42
MY71S4
66
0080607-BS1
LCSW
LCS
08/08/10
17:47:43
MY71S4
67
1007159-07
MY71T6
SAMPLE
08/08/10
17:54:43
MY71S4
UK-^-Z^
68
0080607-DUPl
MY71T6D
SAMPLE
08/08/10
18:01:43
MY71S4
M^-f^vL
69
0080607-MS1
MY71T6S
SAMPLE
08/08/10
18:08:43
MY71S4
70
SRD3
SAMPLE
08/08/10
18:15:44
MY71S4
M ^ ^
MY71T6L
CCV6
CCVl
CCV
08/08/10
18:22:44
CCB6
CCB1
CCB
08/08/10
18:29:45
0080607-PS1
MY71T6A
SAMPLE
08/08/10
18:36:46
MY71S4
1007159-01
MY71S4
SAMPLE
08/08/10
18:43:47
MY71S4
75
1007159-02
MY71S6
SAMPLE
08/08/10
18:50:47
MY71S4
76
1007159-03
MY71S8
SAMPLE
08/08/10
18:57:47
MY71S4
77
1007159-04
MY71T0
SAMPLE
08/08/10
19:04:48
MY71S4
78
1007159-05
MY71T2
SAMPLE
08/08/10
19:11:48
MY71S4
79
1007159-06
MY71T4
SAMPLE
08/08/10
19:18:49
MY71S4
80
CRL4
CRI
CRI
08/08/10
19:25:49
Seq
Sampie ID
49
1007157-08
MY71T7
SAMPLE
50
1007157-09
MY71T9
51
1007157-10
[52
1 '^ 1 ^^ 1 ^^ 73
Client ID
Sample Type
DF
Action Needed
My H 1 Ma 2x
Miffv _y
'
The presence of the Chemist's/Analyst's employee ID number, or signature, on this njn log attests that strict compliance with the method's SOP has occuned. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemisf s/analysts initials and the initials of the lab supervisor and a QA department representative, signifying approval of the deviation.
Reviewed By: ^
• vCHMxua^'>(:^t^
Date:
?-M-/(^
Page 3 of 4
110
113 ICP Run L o g (P3) File Name: P30808 Seq
Sampie ID
Client ID
Sampie Type
DF
Date
Time
SDG
81
IFA4
ICSA
ICS
08/08/10
19:32:49
82
IFB4
ICSAB
ICS
08/08/10
19:39:49
83
CCV7
CCV1
CCV
08/08/10
19:46:50
84
CCB 7
CCBl
CCB
08/08/10
19:53:51
85
1007159-08
MY71T8
SAMPLE
08/08/10
20:00:52
MY71S4
86
1007159-09
MY71W0
SAMPLE
08/08/10
20:07:52
MY71S4
87
1007159-10
MY71W2
SAMPLE
08/08/10
20:14:52
MY71S4
20:21:53
MY71S4
88
1007159-11
MY71W6
SAMPLE
08/08/10
89
1007159-12
MY71X0
SAMPLE
08/08/10
20:28:53
MY71S4
90
1007159-13
MY71X2
SAMPLE
08/08/10
20:35:53
MY71S4
91
1007159-14
MY71X7
SAMPLE
08/08/10
20:42:54
MY71S4
92
1007159-15
MY71X9
SAMPLE
08/08/10
20:49:54
MY71S4
93
1007159-16
MY71Y1
SAMPLE
08/08/10
20:56:55
MY71S4
94
IBLI
IBL
SAMPLE
08/08/10
21:03:56
95
CCV8
CCVl
CCV
08/08/10
21:10:57
96
CCB8
CCB1
CCB
08/08/10
21:17:57
97
CRL5
CRI
CRI
08/08/10
21:24:58
98
IFA5
ICSA
ICS
08/08/10
21:31:58
99
IFB5
ICSAB
ICS
08/08/10
21:38:58
100
CCV9
CCV1
CCV
08/08/10
21:45:59
101
CCB9
CCBl
CCB
08/08/10
21:53:00
J
Action Needed
^Kt7_y 0 7^ M(x4^y. '
^
^
J
^
The presence of the Chemist's/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials of the lab supervisor and a QA department representative, signifying approval of the deviation.
Reviewed By: < g ^ ' yTQi^aiJ^^Hsor
Date:
^-/oyp
Page 4 of 4
111
114 CM
D a i l y S t a n d a r d s / Q C P r e p a r a t i o n L o g f o r T r a c e I C P ( P 3 & P4) 1 of 3 compuchem a division ofLiberty Analytical corp. worksheet 1 p(6) 2 S T A N D A R D S and R E A G E N T S TRACEABILITY
Seq. File Name:
Refr HNO3 [Baker Instra-analyzed Trace-Metals grade] HCI [Baker instra-analyzed Trace-Metals grade] SM-770-027 multi-element standard mix (RSTD-1) SM-770-028 partA multi-element standard mix (RSTD-2A) SM-770-028 pail B multi-element standard mix {RSTD-2B) SM-770-029 part A multi-element standard mix {RSTD-3A) SM-770-029 part B multi-element standard mix (RSTD-3B) SM-770-030 multi-element standard mix (RSTD-4) SPEX-R multi-element standard mix ICP-AES-CRQL-R multi-element standard mix ICV1 multi-element standard mix ICSA multi-element standard mix \CSB multi-element standard mix SM-770-031 multi-element standard mix (PDS-R) ARSENIC (As) 1,000 PPM single-element standard Intemal Mix SM-770-040 multi-element CCV mix (Soln A) SM-770-040 multi-element CCV mix (Soln B) SM-770-042 (LRS 6010B)
0 <3^ I Z 0 \ 0 0F12002 9J22002 9J22001 GDI4008 9G08005 0F12003 0F12001 9104002 0B04003 0BO4002 0B04001 9122001 9F17001 0B04004 0E03001 0E03001 0B23007
?3^g?C?e>
Manufacturer JT Baker Caledon Hlgti Purity High Purity Hlqh Puritv High Puritv High Purity High Purity Hlqh Purity High Purity EPA EPA EPA High Purity High Purity High Puritv High Purity High Puritv High Purity
Lot# -:?-Zo3--^ 1015827 0928011 0928012 0925430 0906204 1015830 1015828 0923808 0307 1206 0203 0926418 0911221 0934101 1010910 1010911 1004021
Expiration Date m i<2..\*506/09/11 10/12/2010 10/12/2010 04/09/11 10/16/10 06/09/11 06/09/11 08/28/10 02/04/11 02/04/11 02/04/11 09/17/10 12/05/10 12/10/10 04/21/11 04/21/11 02/10/11
Multi-Element Stock Standar(d Concentrations: rjraSi^v^S RSTD-1 multi-element standard mix RSTD-2A/2B multi-element standard mix RSTD-3A/3B multi-element standard mix RSTD-4 multi-element standard mix SPEX-R multi-element standard mix ICP-AES-CRQL-R multi-element standard mix PDS-R multi-element standard mix Intemal Mix LRS 6010B multi-element standanJ mix
Entered By: ^ . f f l f e ^ x > u | ^ ^ ^ ^ Revlewecd By:
CdM.OOO Crrl.OOO Cuil.OOO Pb:1.000 Nhl.OOO Se:1.000 Ag:100 Tlil.OOO Znrl.OOO PartA:As:1,000 Barl.OOO Berl.OOO Corl.OOO Mnrl.OOO Morl.OOO Vrl.OOO Part Br Fer25.000 PartArCarlO.OOO MgrlO.OOO KrlO.OOO NarlO.OOO Part Br AlrlO.OOO Sbrl.OOO BIrl.OOO BrI.OOO Snrl.OOO Tlrl.OOO Morl.OOO Snrl.OOO Birl.OOO Tlrl.OOO BrI.OOO Agr10 Ber5 CdrS Cor50 CrIO Cur25 Mnr15 Nlr40 Tlr25 VrSO Znr60 PbrlO Ser35 AsrIO Sbr60 Alr400 Bar400 Agr20 BerlO CdrlO CorlOO Crr20 CurSO Fer200 Mnr30 NirSO Tlr20 VrlOO Znr40 PbrS SerlO Asr20 Sbr120 LIrSO.OOO Yr250 Al; 20 Sb;1 Asr1 Bar20 BerO.5 Bir2 Br2 CdrO.5 CarSOO Crr1 CorO.S CurO.S FerlO PbrO.3 MgrSOO Mnr1 Mor2 NIrO.S KrSOO SerO.5 TlrO.5 Vr2 Znr2 /A-/KJL^
n
•Ref# = Logbook ID, Page number, and Item number frora fror]^Materials Materii Receipt Log "High Purity Is abbreviated "HP* on reporting fonns
Date:
^^67/0 03/25/10: Jcf
115 CO
Daily S t a n d a r d s / Q C Preparation Log for Trace ICP (P3 & P4) 2 of 3 compuChem a division of Liberty Analytical corp worksheet 1 p(6) 2
SO/ICB/CCB- O f e . o s - : i c f i O i H
RSTD-1-
c»e>.o9.|o-'5G,r
RSTD-2- o a . o«r. 10- -S^^i-l RSTD-3- O 2 > , c > < . i o -
^^r-\
U Ot« 0 0
\
0 H 0 O 0 0 2 I
Uc»C^ C> O 3 <:aH<=> «o
^
Place In a 500 mL volumetric flask: 100 mL deionized water, 20 mL concentrated HNO3, and 100 mL concentrated HCI. Bring up to volume with deionized water. Transfer to a 2L Teflon bottle and add 1.5L deionized water. Final volume 2 L. Prepare as needed.
N/A
In a 200 mL volumetric flask, combine 150 mL deionized water, 2 mL concentrated HNO3. and 10 mL concentrated HCI. Pipet 0.4 mL RSTD-1 Into flask. Bring up to 200 mL volume with deionized water. Prepare as needed.
Cd:2,000 Cr:2,000 Cu:2,000 Pb:2,000 Nlr2,000 Se:2,000 Ag:200 Tl:2,000 Zn:2,000
In a 200 mL volumetric flask, combine 150 mL deionized water, 2 mL concentrated HNO3, and 10 mL concentrated HCI. Pipet 0.4 mL each RSTD-2A and RSTD-2B Into flask. Bring up to 200 mL volume with deionized water. Prepare as needed. In a 200 mL volumetric flask, combine 150 mL deionized water. 2 mL concentrated HNO3, and 10 mL concentrated HCI. Pipet 2.0 mL each RSTD-3A and RSTD-3B Into flask. Bring up to 200 mL volume with delonlzed water. Prepare as needed, In a 200 mL volumetric flask, combine 150 mL deionized water, 2 mL concentrated HNO3, and 10 mL concentrated HCI. Pipet 0.4 mL RSTD-4 Into flask. Bring up to 200 mL volume with deionized water. Prepare as needed.
RSTD-4- tf>g, . o ^ . \ 0 ' ' S > a , y i
^i<^/A ICV1-
0£>.6 3 . l o - e a j M
CCV/CVS1-
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O HO-^ ( O 0 2 .
Place in a 500-mL volumetric flask: 300 mL deionized water, 20 mL concentrated HNOs.and 100 mL concentrated HCI. Add 50 ml of SM-770-40 Soln A and Soln B. Bring up to volume with deionized water. Transfer to a 2000mL Teflon bottle and add 1.5 L of deionized water. Prepare as needed.
In a 500 mL volumetric flask, combine 200 mL deionized water, 5 mL concentrated HNOsand 25 mL concentrated HCI. Pipet S.OmL of LRS 601 OB. Bring up to volume with deionized water and transfer to a SOOmL Teflon bottle. Final volume 500 mL. Prepare as needed.
KilOO.OOO NarlOO.OOO Al:100,000 Mg: 100.000 Ca: 100,000
Sn:2,000 Bl:2,000 Tl:2,000 Sb:2,000 B:2,000 Al:2,521 Bar497 K:10,021 Mg:6,074 Narl0,097 Ca:10,026 Agr501 Be:495 Cdr496 Co:499 Cr;490 Cur492 Fe:5.082 Mn:499 Nl:503 Tl;1,028 V:501 Zn: 1,025 Pb:1002 Sell,029 Asi999 Sbi994 Moi1,100 Smi,100 Bill,100 Till,100 Bll,100 Al:50,000 Bail,000 K;50,000 Mgi50,000 Nai50,000 Cai50,000 AgilOO Bei1,000 Cdil.OOO Coi1,000 Cnl.OOO Cuil.OOO Fei25,000 Mn:1,000 Nil1,000 Tlil.OOO Vll,000 2ni1,100 Pbi1,000 Sell,000 Asil,000 Moil,000 Smi,000 Bill,000 Tin.OOO Sbil.OOO Bil.OOO AI12OO Bai200 KiS.OOO MgiS,000 Nai5,000 CaiS.OOO Agi5 BeiS Cd:5 Cono Cri10 Cui5 FeilOO MmlO NiiS Tl:10 Vi20 2n:20 Pb:3 SeiS AsilO M012O Srii20 BI12O Tii20 SbilO B:20
^^M
Standard Solutions Prepared By: Entered By:
Place In a 500 mL volumetric flask; 300 mL deionized water, 5 mL concentrated HN03,and 25 mL concentrated HCI. PIpet 50.0 mL ICVl Into flask and 0.55 mL Compuchem SPEX-R. Bring up to volume with deionized water. Transfer to a SOOmL Teflon bottle. Final volume 500 mL. Prepare as needed.
As:2.000 Ba:2,000 Be;2.000 Co:2,000 FerSO.OOO Mn:2.000 Mo:2,000 V:2,000
yr)l^X>vtwyv .
U
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Reviewed By: •Standard Lot Number consists of standard ID, date pre
Date: d initials of preparer.
O^ O'i lb 03/25/10: Jcf
116
Daily S t a n d a r d s / Q C Preparation Log f o r Trace ICP (P3 & P4) 3 of 3 compuChem a division ofLiberty Analytical corp. worksheet 1 p(6) 2
As-
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ICSAB-
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In a 100 mL volumetric flask, combine 50 mL deionized water. 1 mL concentrated HNO3, 5 mL concentrated HCI, and 0.1 mL 1000-ppm As standard. Bring to flnal 100 mL volume In a 500-mL volumetric flask, combine 350 mL delonlzed water, 5 mL concentrated HNO3, and 25 mL concentrated HCI. Plpet 50.0 mL ICSA Into flask. Bring up to volume with deionized water and transfer to a SOOmL Teflon bottle. Final volume 500 mL.
Asn.OOO Ali244,100 Bai2 Cai234,900 Coi4 Cr;43 Cui23 Fei95,600 Mgi247,500 Mni19 Nii21 Zni28 PbilO
In a SOO-mL volumetric flask, combine 350 mL deionized water. 5 mL concentrated HNO3, and 25 mL concentrated HCI. Plpet 50.0 mL ICSA and 50.0 mL ICSB Into flask. Add 0.5 mL Compuchem SPEX-R. Bring up to volume with deionized water and transfer to a SOOmL Teflon bottle. Final volume 500 mL.
Agi206 Ali241,100 Bai495 Bei475 Cai231,100 Cdi940 Coi461 CriSII CuiS48 Fei94,800 Mgi251,100 Mni502 Nli984 TI1IO3 Vi494 Zni1028 Pbi61 Sei53 Sbi589 AsilOI Snil.OOO Blil.OOO M01I.OOO Tlil.OOO B1I1OOO
In a 500 mL volumetric flask, combine 300 mL deionized water, 5 mL concentrated HNOs.and 25 mL concentrated HCI. Plpet 0.50 mL ICP-AESCRQL-R and 25 pL Compuchem SPEX-R into flask. Bring up to volume with deionized water and transfer to a SOOmL Teflon bottle. Final volume 500 mL, Prepare as needed.
AgilO MnilS Sei35 BiiSO
Bei5 CdiS CoiSO Cri10 Cui25 Nli40 Tli25 ViSO Zni60 PbilO AsilO Sbi60 Sm50 Bi50 MoiSO TliSO
In a 10 L container, combine 8 L deionized water and 400 mL concentrated HNOa Fill with deionized water. Final volume 10 L.
N/A
In a 10 L container, combine 8 L deionized water and 400 mL concentrated HNO3 Fill with deionized water. Final volume 10 L.
N/A
In a 10 L container, combine 8 L deionized water and 400 mL concentrated HNO3 Fill with deionized water. Final volume 10 L.
N/A
In a 10 L container, combine 8 L deionized water, 400 mL concentrated HNO3, and 200 mL Internal Mix. Fill with deionized water. Final volume 10 L.
Llll,000.000
YiS.OOO
In a 10 L container, combine 8 L deionized vwiter, 400 mL concentrated HNO3, and 200 mL Intemal Mix. Fill with delonlzed vrater. Final volume 10 L.
Lill.OOO.OOO
YlS.OOO
In a 10 L container, combine 8 L delonlzed water, 400 mL concentrated HNO3, and 200 mL Intemal Mix. Fill with deionized water. Final volume 10 L.
LI11,000,000
YiS.OOO
Standard Solutions Prepared By: Entered By:.
f PA'T..^.^.^ Date:
Reviewed By: •standard Lot Number consists of standard ID, dat
d. and initials of preparer.
0 'dO^/a 03/25/101 Jcf
117 STANDARDIZATION RPT.
08/08/10 10:18:42 AM
PAGE 1
METHOD: ALT-P3Q3 STANDARD: SO BLANK RUN TIME: 08/08/10 10:11:45 ELEM AVGE SDEV %RSD
AG3280 -.25499 .07192 28.205
AL3082 9.0187 .0696 .77180
BA4934 .39068 .01247 3.1932
BE3130 1.8909 .0146 .77448
CA3179 .00042 .00041 98.396
CD2265 -.16354 .03468 21.204
C02286 -.01769 .01182 66.844
#1 #2 #3
-.17899 -.26399 -.32198
9.0990 8.9757 8.9814
.40473 .38641 .38089
1.8752 1.8934 1.9042
.00000 .00043 .00083
-.15728 -.13241 -.20091
-.01037 -.01137 -.03133
ELEM AVGE SDEV %RSD
CR2677 -.00275 .00539 196.28
CU3247 .66797 .01852 2.7725
FE2714 .01303 .00728 55.846
K_7 664 .48220 .07429 15.406
MG2790 .01237 .00522 42.172
MN2576 .01304 .00468 35.868
NA3302 -.32397 .02026 6.2544
ftl #2 #3
.00251 -.00249 -.00826
.68197 .67497 .64697
.01506 .01908 .00496
.56743 .44804 .43115
.01575 .01501 .00636
.01841 .01079 .00991
-.30380 -.34432 -.32377
ELEM AVGE SDEV %RSD
NI2316 .02638 .02440 92.502
TL1908 -.02605 .00981 37.642
V_2924 -.02421 .00107 4.4090
ZN2138 .01220 .00263 21.524
AS1890 -.04845 .01769 36.514
22031 .33241 .14127 42.498
22032 -.04281 .02846 66.486
#1 #2 03
.05430 .01565 .00918
-.03348 -.01493 -.02973
-.02429 -.02310 -.02523
.01506 .01162 .00991
-.03766 -.06886 -.03882
.48374 .30948 .20401
-.01004 -.06140 -.05699
ELEM AVGE SDEV %RSD
20681 -.01131 .02123 187.71
20682 .00656 .04208 641.16
19601 -.18513 .03314 17.900
19602 .20934 .06013 28.725
SNI899 -.00871 .03831 439.65
BI2230 -.02001 .03943 197.05
MO2020 .01257 .04168 331.67
#1 #2 #3
-.00837 .00830 -.03386
.00084 -.03236 .05121
-.21341 -.19332 -.14867
.27869 .17175 .17758
-.03013 -.03153 .03552
-.02260 -.05808 .02065
.05896 .00043 -.02170
ELEM AVGE SDEV %RSD
TI3349 .20151 .31883 158.22
B_2496 .19471 .00972 4.9940
ffl #2 ft3
.35653 .41319 -.16519
.20337 .18419 .19658
115
118 0 8 / 0 8 / 1 0 1 0 : 2 5 : 4 3 AM
STANDARDIZATION R P T .
PAGE 1
METHOD: ALT-P303 STANDARD: S RSTD-1 RUN TIME: 08/08/10 10:18: 46 ELEM AVGE SDEV %RSD
AG3280 24.501 .057 .23253
CD2265 661.61 .61 .09238
CR2677 35.928 .011 .02974
CU3247 169.09 .43 .25210
NI2316 32.308 .032 .09806
TLI 908 13.502 .023 .17299
ZN2138 30.537 .050 .16350
#1 #2 #3
24.436 24.538 24.531
661.75 660.94 662.13
35.927 35.918 35.939
168.79 168.91 169.58
32.329 32.271 32.324
13.505 13.478 13.524
30.479 30.565 30.566
ELEM AVGE SDEV %RSD
22031 202.23 .33 .16488
22032 183.04 .29 .15638
19601 44.417 .131 .29391
19602 79.342 .401 .50545
ffl ff2 ff3
202.20 202.57 201.91
182.78 183.35 182.98
44.522 44.458 44.271
79.002 79.785 79.240
116
119 STANDARDIZATION R P T . METHOD: ALT-P3Q3 Rtw T I M E : 0 8 / 0 8 / 1 0
0 8 / 0 8 / 1 0 1 0 : 3 1 : 1 1 AM
PAGE 1
STANDARD: S RSTD-3 10:25:47
ELEM AVGE SDEV %RSD
AL3082 1865.0 1.0 .05234
CA3179 .12391 .00070 .56451
K_7664 691.42 .74 .10741
MG2790 279.96 .03 .00912
NA33 02 41.232 .017 .04011
#1 #2 #3
1865.6 1865.6 1863.9
.12452 .12407 .12315
692.01 691.66 690.59
279.98 279.96 279.93
41.239 41.244 41.213
117
120 STANDARDIZATION R P T . METHOD: ALT-P3Q3 RUN TIME: 0 8 / 0 8 / 1 0
08/08/10
1 0 : 3 6 : 3 8 AM
PAGE 1
STANDARD: S RSTD-2 10:31:14
ELEM AVGE SDEV %RSD
BA4934 365.42 .28 .07617
BE3130 1732.7 3.3 .19016
C02286 115.03 .10 .08656
FE2714 62.445 .051 .08211
MN2576 58.193 .026 .04550
V_2924 17.213 .015 .08487
ASI890 175.30 .13 .07409
ftl #2 #3
365.11 365.50 365.65
1729.1 1733.6 1735.5
114.94 115.14 115.03
62.388 62.486 62.462
58.162 58.211 58.204
17.198 17.216 17.227
175.17 175.32 175.43
ELEM AVGE SDEV %RSD
MO2020 138.07 .43 .30811
ffl #2 ff3
137.62 138.46 138.14
118
121 STANDARDIZATION RPT.
08/08/10 10:43:39 AM
PAGE 1
METHOD: ALT-P3Q3 STANDARD: S RSTD-4 RUN TIME: 08/08/10 10:36:42 ELEM AVGE SDEV %RSD
20681 18.667 .032 .17304
20682 74.750 .032 .04343
SN1899 26.991 .015 .05531
BI2230 165.23 .20 .12296
TI3349 248.14 .32 .12801
B 2496 151.46 .16 .10416
#1 S2 ff3
18.634 18.667 18.699
74.783 74.749 74.718
27.006 26.976 26.989
165.02 165.43 165.25
247.84 248.09 248.47
151.30 151.62 151.45
119
122 ANALYSIS REPORT
QC STANDARD
08/08/10 10:50:40 AM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICVl RUN TIME: 08/08/10 10:43:43 COMMENT: ICVl MODE: CONC CORR:. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 508.0343 .9123 .1795674
AL3082 UG/LITER 2599.331 33.551 1.290764
BA4934 UG/LITER 514.4148 5.2566 1.021855
BE3130 UG/LITER 500.8891 4.6942 .9371687
CA3179 UG/LITER 9925.322 66.474 .6697422
CD2265 UG/LITER 507.7703 5.5684 1.096640
C02286 UG/LITER 513.0485 4.5062 .8783186
ftl #2 ff3
507.2229 507.8582 509.0217
2583.754 2576.400 2637.839
512.6104 510.2981 520.3359
499.3048 497.1921 506.1705
9917.165 9863.303 9995.498
505.4497 503.7375 514.1237
511.2484 509.7206 518.1765
ERRORS VALUE RANGE
QC PASS 501.0000 10.40000
QC PASS 2521.000 10.40000
QC PASS 497.0000 10.40000
QC PASS 495.0000 10.40000
QC PASS 10026.00 10.40000
QC PASS 496.0000 10.40000
QC PASS 499.0000 10.40000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 507.7907 5.3339 1.050418
CU3247 UG/LITER 507.9954 1.6592 .3266095
FE2714 UG/LITER 5100.922 55.062 1.079453
K_7664 UG/LITER 9772.557 93.001 .9516597
MG2790 UG/LITER 6018.626 62.256 1.034385
MN2576 UG/LITER 500.1302 4.9486 .9894569
NA3302 UG/LITER 10193.45 83.69 .8210525
ftl #2 ft3
506.3929 503.2949 513.6844
506.8317 507.2592 509.8953
5078.736 5060.414 5163.616
9734.269 9704.810 9878.590
5993.765 5972.642 6089.470
498.3297 496.3339 505.7269
10161.69 10130.28 10288.37
ERRORS VALUE RANGE
QC PASS 490.0000 10.40000
QC PASS 492.0000 10.40000
QC PASS 5082.000 10.40000
QC PASS 10021.00 10.40000
QC PASS 6074.000 10.40000
QC PASS 499.0000 10.40000
QC PASS 10097.00 10.40000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 511.9742 4.9736 .9714486
TL1908 UG/LITER 1051.612 8.686 .8260128
V_2924 UG/LITER 513.2126 5.2831 1.029423
ZN2138 UG/LITER 998.9412 10.3535 1.036445
PB2203 UG/LITER 1019.172 9.640 .9459057
SE1960 UG/LITER 1018.501 10.489 1.029814
SB2068 UG/LITER 1018.140 9.247 .9082008
ftl ft2 #3
509.8737 508.3955 517.6534
1052.338 1042.585 1059.912
510.7438 509.6158 519.2781
994.3883 991.6443 1010.791
1013.627 1013.585 1030.304
1015.608 1009.762 1030.132
1014.527 1011.246 1028.648
ERRORS VALUE RANGE
QC PASS 503.0000 10.40000
QC PASS 1028.000 10.40000
QC PASS 501.0000 10.40000
QC PASS 1025.000 10.40000
QC PASS 1002.000 10.40000
QC PASS 1029.000 10.40000
QC PASS 994.0000 10.40000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1020.082 8.113 .7953607
22031 UG/LITER 1019.473 7.896 .7745610
22032 UG/LITER 1019.007 10.638 1.043992
20681 UG/LITER 1018.122 7.640 .7503988
20682 UG/LITER 1018.145 10.352 1.016727
19601 UG/LITER 1011.901 11.197 1.106564
19602 UG/LITER 1021.785 10.345 1.012464
#1 #2 ft3
1016.451 1014.418 1029.377
1016.754 1013.296 1028.370
1012.054 1013.714 1031.254
1012.515 1015.027 1026.824
1015.527 1009.354 1029.555
1006.126 1004.770 1024.807
1020.332 1012.244 1032.781
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
999.0000 10.40000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1110.931 7.541 .6788148
BI2230 UG/LITER 1103.127 11.935 1.081926
MO2020 UG/LITER 1104.586 13.346 1.208251
TI3349 UG/LITER 1111.245 7.901 .7110303
B_2496 UG/LITER 1108.033 12.506 1.128672
Y_3710 PPM 1212.289 7.569 .6243349
ftl tf2 #3
1108.485 1104.916 1119.391
1095.827 1096.653 1116.900
1099.014 1094.928 1119.815
1107.528 1105.888 1120.320
1101.150 1100.481 1122.469
1213.133 1219.400 1204.333
ERRORS VMJUE RANGE
QC PASS 1100.000 10.40000
QC PASS 1100.000 10.40000
QC PASS 1100.000 10.40000
QC PASS 1100.000 10.40000
QC PASS 1100.000 10.40000
NOCHECK
120
123 ANALYSIS REPORT
QC STANDARD
08/08/10 10:57:41 AM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICB RUN TIME: 08/08/10 10:50:44 COMMENT: ICB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.153955 .194647 126.4314
AL3082 UG/LITER -8.16591 7.61243 93.22199
BA4934 UG/LITER -.460642 .058644 12.73083
BE3130 UG/LITER -.017248 .051796 300.3025
CA3179 UG/LITER -203.561 379.759 186.5583
CD2265 UG/LITER .3112062 .0988379 31.75960
C02286 UG/LITER .0700174 .1279893 182.7964
ftl ff2 ff3
.0481706 -.340144 -.169891
.2764470 -10.2672 -14.5070
-.403963 -.521070 -.456894
.0415230 -.037027 -.056239
17.26399 -642.065 14.11923
.2366403 .2736637 .4233148
.1705840 .1135214 -.074053
ERRORS VALtJE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM tmiTS AVGE SDEV %RSD
CR2677 UG/LITER .1220468 .0265615 21.76337
CU3247 UG/LITER .3285231 .1077450 32.79677
FE2714 UG/LITER .6063982 4.256603 701.9485
K_7664 UG/LITER 2.017506 5.538057 274.5002
MG2790 UG/LITER 7.409300 1.631397 22.01824
MN2576 UG/LITER .1534580 .0186387 12.14581
NA3302 UG/LITER -78.9403 32.4258 41.07638
#1 #2 #3
.1064618 .1527160 .1069625
.2137380 .4274759 .3443554
-1.11734 -2.51799 5.454520
8.236740 -2.38088 .1966550
7.553880 5.710424 8.963594
.1674977 .1605650 .1323113
-64.5044 -116.077 -56.2394
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS •OOOOOOO 5000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 2.831744 .481155 16.99147
TL1908 UG/LITER -.619662 1.985380 320.3972
V_2924 UG/LITER -.184132 .133056 72.26122
ZN2138 UG/LITER .0098486 .0819716 832.3153
PB2203 UG/LITER .5699637 .7030097 123.3429
SE1960 UG/LITER .4513531 .3434802 76.10010
SB2068 UG/LITER .1331468 1.787798 1342.727
#1 ft2 ff3
3.304781 2.847588 2.342863
-1.04361 -2.35883 1.543449
-.117953 -.337301 -.097141
-.055964 .1016689 -.016159
-.163509 .6354763 1.237924
.5505180 .0691998 .7343416
1.327454 .9942263 -1.92224
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5^000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1.22383 1.25671 102.6863
22031 UG/LITER 1.138354 .246866 21.68624
22032 UG/LITER .2762627 1.090393 394.6944
20681 UG/LITER .5336365 .5571590 104.4080
20682 UG/LITER -.076726 2.402841 3131.701
19601 UG/LITER 1.295503 .941929 72.70759
19602 UG/LITER .0199803 .9736581 4873.102
#1 #2 #3
-.634536 -.370063 -2.66690
1.082076 1.408501 .9244868
-.795356 .2396364 1.384508
.9395999 .7628833 -.101574
1.511102 1.099827 -2.84111
.7182134 2.382449 .7858485
.4568076 -1.09559 .6987268
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.420083 1.770018 421.3492
BI2230 UG/LITER -.673298 3.151397 468.0536
MO2020 UG/LITER 2.656359 1.645838 61.95841
TI3349 UG/LITER .9028678 2.325461 257.5638
B_2496 UG/LITER 2.145153 .416938 19.43629
Y_3710 PPM 1230.800 6.123 .4974947
#1 #3
-1.45196 -1.43202 1.623725
1.452190 -4.29398 .8218912
4.554810 1.782600 1.631667
2.677715 -1.72961 1.760496
2.600272 2.053562 1.781625
1223.733 1234.133 1234.533
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50-00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
ff2
121
124 ANALYSIS REPORT
QC STANDARD
08/08/10 11:04:41 AM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CRI RUN TIME: 08/08/10 10:57:44 COMMENT: CRI MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 8.210563 .077625 .9454339
AL3082 UG/LITER -21.3066 7.1401 33.51151
BA4934 UG/LITER -.506656 .028521 5.629302
BE3130 UG/LITER 4.931883 .147578 2.992319
CA3179 UG/LITER -648.420 330.358 50.94812
CD2265 UG/LITER 5.381334 .260716 4.844819
C02286 UG/LITER 51.48237 1.01527 1.972077
ffl ff2 tf3
8.157838 8.299701 8.174150
-23.0763 -13.4480 -27.3954
-.527396 -.474131 -.518441
4.860144 5.101616 4.833890
-319.721 -645.127 -980.412
5.288573 5.675746 5.179684
50.88356 52.65462 50.90894
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS .OOOOOOO 400.0000
QC PASS .OOOOOOO 400.0000
QC PASS 5.000000 1.500000
QC PASS .OOOOOOO 2000.000
QC PASS 5.000000 1.500000
QC PASS 50.00000 15.00000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 9.767212 .315537 3.230579
CU3247 UG/LITER 25.46251 .05858 .2300459
FE2714 UG/LITER 4.749906 7.916994 166.6769
K_7 664 UG/LITER .0789447 2.123442 2689.785
MG2790 UG/LITER 4.200665 1.173162 27.92801
MN2576 UG/LITER 14.61832 .35161 2.405287
NA3302 UG/LITER -7.74033 26.64983 344.2983
#1 tl2 ft3
9.647121 10.12516 9.529351
25.42292 25.52980 25.43480
4.262265 -2.91200 12.89945
2.508720 -.851080 -1.42081
5.308861 2.971855 4.321279
14.45043 15.02241 14.38213
-6.35249 -35.0570 18.18846
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS 25.00000 7.500000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 2000.000
QC PASS .OOOOOOO 2000.000
QC PASS 15.00000 4.500000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 38.64836 .82086 2.123908
TL1908 UG/LITER 23.94283 3.27078 13.66078
V_2924 UG/LITER 51.11009 1.01497 1.985848
ZN2138 UG/LITER 54.26129 1.35819 2.503063
PB2203 UG/LITER 10.75821 .68298 6.348493
SE1960 UG/LITER 36.84832 1.37174 3.722675
SB2068 UG/LITER 63.66555 1.87235 2.940912
•38.56349 39.50835 37.87324
21.95995 27.71800 22.15055
50.49396 52.28155 50.55476
53.52669 55.82858 53.42861
10.08471 10.73961 11.45030
38.21642 36.85556 35.47297
63.83615 65.44677 61.71375
ERRORS VALUE RANGE
QC PASS 40.00000 12,00000
QC PASS 25.00000 12.50000
QC PASS 50.00000 15.00000
QC PASS 60.00000 18.00000
QC PASS 10.00000 5.000000
QC PASS 35.00000 10.50000
QC PASS 60.00000 30.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 9.962957 .376118 3.775167
22031 UG/LITER 10.95524 .98005 8.945987
22032 UG/LITER 10.64470 .73160 6.872873
20681 UG/LITER 64.38620 2.37184 3.683769
20682 UG/LITER 63.29568 2.25816 3.567631
19601 UG/LITER 33.77822 .82641 2.446571
19602 UG/LITER 38.37097 2.26754 5.909516
ttl ft2 ff3
9.528744 10.17238 10.18775
10.61822 10.18817 12.05934
9.803358 10.99946 11.13128
62.39991 67.01232 63.74638
64.54319 64.65486 60.68898
33.85024 32.91816 34.56626
40.38624 38.81101 35.91566
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
10.00000 3.000000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 52.88937 2.61086 4.936462
BI2230 UG/LITER 52.81129 2.16331 4.096297
MO2020 UG/LITER 52.96273 1.46840 2.772523
TI3349 UG/LITER 53.34990 .83812 1.570992
B_2496 UG/LITER 52.87781 .94023 1.778114
Y_3710 PPM 1211.444 21.290 1.757406
#1 ft2 tt3
51.11839 55.88776 51.66197
53.84895 54.26029 50.32464
52.53383 54.59782 51.75653
52.38212 53.83199 53.83559
52.60244 53.92498 52.10602
1222,066 1186.933 1225.333
ERRORS VALUE RANGE
NOCHECK
QC PASS 50.00000 15.00000
NOCHECK
NOCHECK
QC PASS 50.00000 15.00000
NOCHECK
ffl tf2 ft3
122
125 ANALYSIS REPORT
QC STANDARD
08/08/10 11:11:41 AM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSA RUN TIME: 08/08/10 11:04:44 COMMENT: ICSA MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.134411 .077064 57.33496
AL3082 UG/LITER 256955.5 7806.2 3.037975
BA4934 IX3/LITER 2.591143 .127010 4.901688
BE3130 UG/LITER .8448806 .1139302 13.48477
CA3179 UG/LITER 254062.6 8101.6 3.188816
CD2265 UG/LITER 1.836557 .096227 5.239535
C02286 UG/LITER 5.152932 .199663 3.874754
ftl ff2 ft3
-.093860 -.086088 -.223284
250143.5 255249.3 265473.8
2.484989 2.556584 2.731856
.7406622 .8274630 .9665167
247162.2 252042.4 262983.1
1.809297 1.943474 1.756902
5.291951 4.924141 5.242704
ERRORS VALUE RANGE
QC PASS .OOOOOOO 10.00000
QC PASS 244100.0 48820.00
QC PASS 2.000000 400.0000
QC PASS .OOOOOOO 10.00000
QC PASS 234900.0 46980.00
QC PASS .OOOOOOO 10.00000
OC PASS 4.000000 10.00000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 46.12806 1.42337 3.085687
CU3247 UG/LITER 23.82385 .32656 1.370735
FE2714 UG/LITER 101689.9 3495.3 3.437263
K_7 664 UG/LITER 1.765374 4.556477 258.1026
MG2790 UG/LITER 265018.7 8766.5 3.307876
MN2576 UG/LITER 18.32423 .65139 3.554816
NA3302 UG/LITER 945.2046 88.2406 9.335604
#1 #2 #3
44.69146 46.15491 47.53782
23.81989 23.49929 24.15237
98661.77 100893.1 105514.9
1.902753 -2.85824 6.251609
257457.1 262971.1 274627.7
17.74898 18.19218 19.03153
1040.459 866.2514 928.9031
ERRORS VALUE RANGE
QC PASS 43.00000 20.00000
QC PASS 23.00000 10.00000
QC PASS 95600.00 19120.00
QC PASS .OOOOOOO 2000.000
QC PASS 247500.0 49500.00
QC PASS 19.00000 20.00000
OC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 20.19973 .79204 3.921018
TL1908 UG/LITER -2.61503 4.22573 161.5938
V_2924 UG/LITER 1.152097 .060537 5.254531
ZN2138 UG/LITER 28.76387 .97898 3.403524
PB2203 UG/LITER 12.29067 1.75809 14.30426
SE1960 UG/LITER -3.74447 3.38983 90.52897
SB2068 UG/LITER 4.437019 2.048345 46.16489
#1 #2 #3
20.14924 19.43416 21.01581
-4.43019 -5.62991 2.215008
1.214827 1.094021 1.147445
27.94948 28.49209 29.85002
10.26286 13.22172 13.38742
-7.10992 -.330785 -3.79269
3.543049 2.987605 6.780404
ERRORS VALUE RANGE
QC PASS 21.00000 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS 1.000000 40.00000
QC PASS 28.00000 40.00000
QC PASS 10.00000 6.000000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .2671385 .6598956 247.0238
22031 UG/LITER -4.02292 .94812 23.56806
22032 UG/LITER 20.42067 2.60600 12.76158
20681 UG/LITER 7.880219 3.739679 47.45653
20682 UG/LITER 2.707470 1.256839 46.42117
19601 UG/LITER -5.98815 4.88898 81.64416
19602 UG/LITER -2.63484 2.90866 110.3922
#1 #2 tt3
-.013007 -.206467 1.020890
-4.23991 -2.98511 -4.84373
17.48909 21.29854 22.47437
5.664874 5.777847 12.19793
2.473391 1.584126 4.064892
-9.56957 -.418265 -7.97663
-5.89229 -.297558 -1.71467
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 20.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -1.05942 2.03996 192.5544
BI2230 UG/LITER 6.034118 2.448335 40.57485
MO2020 UG/LITER .9755909 .6588103 67.52935
TI3349 UG/LITER 3.936684 6.428777 163.3044
B_2496 UG/LITER -2.35536 .32278 13.70409
Y_3710 PPM 1166.355 26.416 2.264817
#1 ft2 #3
-.426230 -3.34090 .5888624
7.604281 3.213040 7.285033
.9196654 .3465261 1.660581
-1.73981 2.632198 10.91766
-2.03813 -2.68342 -2.34453
1187.467 1174.867 1136.733
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO IOO.OOOO
QC PASS .OOOOOOO 100.0000
NOCHECK
123
126 ANALYSIS REPORT
QC STANDARD
08/08/10 11:18:41 AM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSAB RUN TIME: 08/08/10 11:11:44 COMMENT: ICSAB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 203.0975 .5986 .2947483
AL3082 UG/LITER 252557.1 1091.4 .4321493
BA4934 UG/LITER 515.9972 2.5514 .4944595
BE3130 UG/LITER 495.4320 .8243 .1663870
CA3179 UG/LITER 250712.6 604.9 .2412898
CD2265 UG/LITER 996.7107 3.5335 .3545126
C02286 UG/LITER 506.9432 1.1177 .2204878
tfl ff2 #3
202.4257 203.5745 203.2923
253800.9 251759.3 252111.2
518.9383 514.3784 514.6749
496.2251 494.5797 495.4912
251408.4 250311.3 250418.0
1000.528 993.5547 996.0493
508.1826 506.0116 506.6354
ERRORS VALUE RANGE
QC PASS 206.0000 41.20000
QC PASS 241100.0 48220.00
QC PASS 495.0000 400.0000
QC PASS 475.0000 95.00000
QC PASS 231100.0 46220.00
QC PASS 940.0000 188.0000
QC PASS 461.0000 92.20000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 544.8165 1.2601 .2312928
CU3247 UG/LITER 533.4500 .2539 .0476009
FE2714 UG/LITER 99944.05 312.04 .3122167
K_7664 UG/LITER 4.809013 4.175657 86.82982
MG2790 UG/LITER 261245.7 783.6 .2999469
MN2576 UG/LITER 520.6754 1.5618 .2999577
NA3302 UG/LITER 1048.146 61.320 5.850344
#1 #3
546.2643 543.9669 544.2184
533.1571 533.6083 533.5845
100288.6 99680.38 99863.23
1.692824 9.553507 3.180709
262062.0 260499.5 261175.4
522.4714 519.6359 519.9189
987.3677 1047.076 1109.994
ERRORS VALUE RANGE
QC PASS 511.0000 102.2000
QC PASS 548.0000 109.6000
QC PASS 94800.00 18960.00
QC PASS .OOOOOOO 2000.000
QC PASS 251100.0 50220.00
QC PASS 502.0000 100.4000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1039.573 2.723 .2619084
TL1908 UG/LITER 102.8079 3.3478 3.256397
V_2924 UG/LITER 511.2561 1.4125 .2762872
ZN2138 UG/LITER 1035.045 3.925 .3792265
PB2203 UG/LITER 62.77451 1.48936 2.372551
SE1960 UG/LITER 46.33338 3.16708 6.835424
SB2068 UG/LITER 619.0722 1.7188 .2776332
ftl
#2 #3
1042.687 1037.640 1038.393
104.9325 104.5425 98.94875
512.8819 510.3297 510.5567
1039.418 1031.827 1033.891
63.45359 61.06664 63.80330
42.91007 46.93096 49.15910
620.9673 617.6142 618.6351
ERRORS VALUE RANGE
QC PASS 984.0000 196.8000
QC PASS 103.0000 20.60000
QC PASS 494.0000 98.80000
QC PASS 1028.000 205.6000
QC PASS 61.00000 12.20000
QC PASS 53.00000 10.60000
QC PASS 589.0000 117.8000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 99.33100 .80520 .8106269
22031 UG/LITER 45.40299 2.52244 5.555679
22032 UG/LITER 71.43113 .97413 1.363732
20681 UG/LITER 619.5472 .5476 .0883913
20682 UG/LITER 618.8286 2.3359 .3774774
19601 UG/LITER 38.12394 2.43160 6.378138
19602 UG/LITER 50.42147 3.58906 7.118113
#1 #2 ff3
98.44430 99.53210 100.0166
46.60678 42.50416 47.09801
71.84814 70.31791 72.12734
620.0018 618.9393 619.7007
621.4429 616.9463 618.0967
35.83918 37.85296 40.67968
46.42968 51.45272 53.38200
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
101.0000 20.20000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 993.0305 5.6512 .5690832
BI2230 UG/LITER 1026.518 5.340 .5202432
MO2020 UG/LITER 995.1958 2.1305 .2140814
TI3349 UG/LITER 1010.278 2.955 .2924984
B_2496 UG/LITER 1013.340 3.735 .3685869
Y_3710 PPM 1173.600 6.025 .5133562
ffl tf2 #3
998.8274 987.5373 992.7269
1031.907 1021.227 1026.420
996.3055 992.7395 996.5424
1013.343 1007.447 1010.042
1017.167 1009.704 1013.148
1166.733 1178.000 1176.067
ERRORS VALUE RANGE
QC PASS 1000.000 200.0000
QC PASS 1000.000 200.0000
QC PASS 1000.000 200.0000
QC PASS 1000.000 200.0000
QC PASS 1000.000 200.0000
ff2
NOCHECK
124
127 ANALYSIS REPORT
QC STANDARD
08/08/10 11:25: 43 AM
METHOD:; ALT-P3Q3 SAMPLE NAME: CCV RUN TIME: 08/08/10 11:18:45 COMMENT: CCV CVSl MODE: CONC CORR. FACTOR: 1
PAGE
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 101.5322 .2867 .2823737
AL3082 UG/LITER 50339.57 9.54 .0189595
BA4934 UG/LITER 1009.222 .578 .0573025
BE3130 UG/LITER 1010.709 1.634 .1617004
CA3179 UG/LITER 49663.38 752.29 1.514787
CD2265 UG/LITER 998.5710 1.0513 .1052812
C02286 UG/LITER 999.9536 1.0985 .1098549
ffl ff2 ff3
101.5185 101.8256 101.2527
50350.22 50336.70 50331.79
1009.737 1008.596 1009.334
1011.737 1011.566 1008.825
50286.22 48827.56 49876.37
998.8159 999.4783 997.4189
999.8789 1001.088 998.8944
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1007.406 1.028 .1020403
CU3247 UG/LITER 1008.486 3.363 .3334845
FE2714 UG/LITER 25106.37 25.87 .1030308
K_7664 UG/LITER 48408.31 36.18 .0747474
MG2790 UG/LITER 50277.04 21.01 .0417833
MN2576 UG/LITER 995.3319 1.0239 .1028738
NA3302 UG/LITER 50731.84 193.64 .3816958
ftl ft2 #3
1008.262 1007.689 1006.266
1006.598 1006.491 1012.369
25076.70 25118.22 25124.19
48398.35 48378.15 48448.43
50268.56 50300.96 50261.61
995.8037 996.0349 994.1571
50898.40 50777.77 50519.37
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1006.758 .531 .0527558
TL1908 UG/LITER 1010.932 5.898 .5833803
V_2924 UG/LITER 1016.054 .159 .0156844
ZN2138 UG/LITER 1085.379 1.545 .1423104
PB2203 UG/LITER 1001.778 .867 .0865399
SE1960 UG/LITER 1007.554 4.077 .4046849
SB2068 UG/LITER 1031.400 1.847 .1790752
#1 ft2 ft3
1006.161 1007.138 1006.985
1014.264 1004.122 1014.408
1015.944 1015.981 1016.237
1086.285 1086.257 1083.596
1001.656 1002.699 1000.978
1002.941 1010.676 1009.044
1030.965 1033.427 1029.811
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1015.110 .629 .0619267
22031 UG/LITER 998.5329 2.4150 .2418579
22032 UG/LITER 1003.383 1.117 .1113581
20681 UG/LITER 1029.972 1.798 .1745267
20682 UG/LITER 1032.110 1.920 .1860047
19601 UG/LITER 996.5284 9.3291 .9361550
19602 UG/LITER 1013.048 1.456 .1437246
#1 #2 ff3
1015.733 1015.119 1014.476
1000.535 999.2126 995.8508
1002.203 1004.424 1003.523
1029.017 1032.045 1028.853
1031.933 1034.112 1030.285
985.9886 1003.726 999.8705
1011.394 1014.136 1013.614
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1010.941 2.123 .2099828
BI2230 UG/LITER 1013.264 4.543 .4483574
MO2020 UG/LITER 1021.326 3.326 .3256897
TI3349 UG/LITER 1016.596 4.462 .4388674
B_2496 UG/LITER 1021.437 2.173 .2127817
Y_3710 PPM 1211.489 5.103 .4211864
ftl #2 #3
1012.726 1008.593 1011.502
1018.301 1009.475 1012.018
1017.542 1023.786 1022.651
1014.815 1021.673 1013.300
1019.292 1021.382 1023.638
1207.600 1209.600 1217.267
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
125
128 ANALYSIS REPORT
QC STANDARD
08/08/10 11:32:44 AM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCB RUN TIME: 08/08/10 11:25:47 COMMENT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .2775698 .1035893 37.32010
AL3082 UG/LITER -6.90150 11.25259 163.0456
BA4934 UG/LITER -.426758 .113182 26.52124
BE3130 UG/LITER .0053605 .0483594 902.1444
CA3179 UG/LITER 223.0762 180.9889 81.13323
CD2265 UG/LITER .2752552 .1615277 58.68287
C02286 UG/LITER .1373227 .4123259 300.2606
#1 #2 #3
.2022352 .2347742 .3957000
-18.7573 3.630836 -5.57804
-.555994 -.345299 -.378982
-.039297 .0567222 -.001344
327.6007 14.08818 327.5397
.1490736 .4572991 .2193929
-.260256 .5629624 .1092617
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.199409 .253258 127.0042
CU3247 UG/LITER .4156014 .2018635 48.57143
FE2714 UG/LITER 9.869743 3.311300 33.55001
K_7664 UG/LITER 1.510309 2.532018 167.6491
MG2790 UG/LITER 22.66477 13.36701 58.97704
MN2576 UG/LITER -.248629 .105022 42.24039
NA3302 UG/LITER 36.61965 27.13084 74.08818
ftl #2 tf3
-.490658 -.076587 -.030982
.2137380 .6174650 .4156011
9.465911 13.36444 6.778880
-.073974 4.430513 .1743867
7.816597 33.73931 26.43841
-.368864 -.174827 -.202196
42.18262 60.53784 7.138503
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -1.70651 .87249 51.12717
TL1908 UG/LITER -.155209 .236339 152.2708
V_2924 UG/LITER .0847478 .1281297 151.1894
ZN2138 UG/LITER -.086657 .042369 48.89290
PB2203 UG/LITER -.739664 .203076 27.45512
SE1960 UG/LITER -.236427 2.300399 972.9871
SB2068 UG/LITER .9177429 .3549018 38.67115
ftl #2 «3
-2.68584 -1.42158 -1.01210
-.392257 -.153785 .0804138
.1095758 .1986464 -.053979
-.083019 -.046224 -.130727
-.921995 -.776196 -.520802
-.801142 -2.20188 2.293743
.5668920 .9097753 1.276561
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -2.00028 .94497 47.24178
22031 UG/LITER .5878605 1.576507 268.1771
22032 UG/LITER -1.41234 1.00076 70.85825
20681 UG/LITER 1.142978 .884040 77.34532
20682 UG/LITER .7953893 .5465232 68.71141
19601 UG/LITER -1.44202 2.80681 194.6447
19602 UG/LITER .3555574 2.234747 628.5194
ttl ff2 ft3
-2.79320 -2.25297 -.954651
2.354927 -.674464 .0831187
-2.56791 -.836885 -.832216
.3219144 2.078788 1.028231
.6792885 .3162451 1.390634
-3.33661 -2.77201 1.782572
.4547808 -1.92715 2.539040
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -1.31016 .84852 64.76420
BI2230 UG/LITER 1.375485 2.573183 187.0746
MO2020 UG/LITER 3.196275 .888232 27.78961
TI3349 UG/LITER 1.981448 .723113 36.49420
B_2496 UG/LITER 2.032334 .271839 13.37569
Y_3710 PPM 1233.955 .518 .0419644
ftl ft2 #3
-1.80238 -1.79773 -.330384
-1.43719 3.611234 1.952411
4.025209 3.304883 2.258733
1.146979 2.423976 2.373387
1.972446 2.329122 1.795432
1233.533 1234.533 1233.800
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
126
129 08/08/10 11:43:19 AM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0080340-BLKl RUN TIME: 08/08/10 11:36:22 COMMENT: SDG:MC0021 CLIENTID:PBW 1:1 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0645875 .2123246 328.7395
AL3082 UG/LITER 102.9102 9.7412 9.465752
BA4934 UG/LITER -.062809 .089275 142.1383
BE3130 UG/LITER .0622552 .0354046 56.87006
CA3179 UG/LITER 13.33080 1.27505 9.564698
CD2265 UG/LITER .0969418 .1351931 139.4581
C02286 UG/LITER .0248461 .1450942 583.9713
ftl It2 ft3
-.162205 .2586410 .0973267
98.88618 95.82568 114.0187
-.147569 -.071239 .0303824
.0661464 .0250658 .0955534
14.56456 13.40972 12.01813
-.015814 .0598216 .2468173
-.125377 .0357155 .1642000
ERRORS HIGH LOW
LC PASS 5.000000 -5.00000
LC PASS 200.0000 -200.000
LC PASS 200.0000 -200.000
LC PASS 5.000000 -5.OOOOO
LC PASS 5000.000 -5000.00
LC PASS 5.000000 -5.00000
LC PASS 50.00000 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .0462442 .2058393 445.1135
CU3247 UG/LITER .2929000 .1526823 52.12781
FE2714 UG/LITER 7.809946 11.00027 140.8495
K_7664 UG/LITER 2.223038 2.827061 127.1711
MG2790 UG/LITER 23.87562 16.51473 69.16987
MN2576 UG/LITER -.203578 .071367 35.05654
NA3302 UG/LITER -17.0309 131.7211 773.4229
#1 #2 #3
.0606356 .2445102 -.166413
.1187434 .4037271 .3562295
.8369776 2.101910 20.49095
.4093198 .7793446 5.480449
12.56401 16.23586 42.82699
-.229162 -.258626 -.122945
-150.724 112.6248 -12.9932
ERRORS HIGH LOW
LC PASS 10.00000 -10.0000
LC PASS 26.00000 -25.0000
LC PASS 100.0000 -100.000
LC PASS 5000.000 -5000.00
LC PASS 5000.000 -5000.00
LC PASS 15.00000 -15.0000
LC PASS 5000.000 -5000.00
ELEM UNITS AVGE SDEV. %RSD
NI2316 UG/LITER -1.78947 .64322 35.94466
TL1908 UG/LITER -3.20091 1.36593 42.67302
V_2924 UG/LITER -.015255 .210915 1382.565
ZN2138 UG/LITER 1.669636 .172168 10.31174
PB2203 UG/LITER -.139563 .829000 593.9990
SE1960 UG/LITER .9822023 1.643174 167.2949
SB2068 UG/LITER .7230222 .2563707 35.45820
#1 #2 ft3
-2.28979 -2.01470 -1.06393
-1.64122 -4.18389 -3.77762
-.251953 .0534331 .1527533
1.623124 1.526502 1.860282
-1.07851 .1685713 .4912472
.3420137 -.244519 2.849112
.8425925 .8977645 .4287096
ERRORS HIGH LOW
LC PASS 40.00000 -40.0000
LC PASS 10.00000 -10.0000
LC PASS 50.00000 -60.0000
LC PASS 60.00000 -60.0000
LC PASS 10.00000 -10.0000
LC PASS 35.00000 -35.0000
LC PASS 60.00000 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.849958 1.203844 141.6358
22031 UG/LITER 1.762431 .924350 62.44745
22032 UG/LITER -1.09942 1.68078 162.8781
20681 UG/LITER 1.081285 1.046350 96.67667
20682 UG/LITER .5342855 .9037659 169.1541
19601 UG/LITER -.605791 2.054361 339.1186
19602 UG/LITER 1.765130 1.465383 82.46185
#1 #2 #3
-.050922 -.264388 -2.23466
2.657048 1.819274 .8109714
-2.95464 -.665422 .3217902
.7631988 .2319269 2.248730
.8723172 1.220310 -.489770
-1.08326 -2.37936 1.645250
1.043665 .8114220 3.440303
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
10.00000 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.630478 .614332 97.43910
BI2230 UG/LITER .9179550 1.953946 212.8584
MO2020 UG/LITER 1.221560 .497462 40.72350
TI3349 UG/LITER 2.720254 2.436473 89.56784
B_2496 UG/LITER 6.793041 .617129 9.084717
Y_3710 PPM 1237.200 5.175 .4182577
#1 tf2 #3
.0363691 -.754402 -1.17340
-.018351 3.163859 -.391643
.9385474 .9301726 1.795959
.1762382 2.951884 5.032641
7.473638 6.269879 6.635607
1232.200 1236.867 1242.533
ERRORS HIGH LOW
LC PASS 100.0000 -100.000
LC PASS 50.00000 -60.0000
LC PASS 10.00000 -10.0000
LC PASS 40.00000 -40.0000
LC PASS 10.00000 -10.0000
NOCHECK
127
130 08/08/10 11:50:19 AM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0080340-BSl RUN TIME: 08/08/10 11:43:22 COMMENT: SDG:MC0021 CLIENTID:LCSW MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM tmiTS AVGE SDEV %RSD
AG3280 UG/LITER 508.9652 1.0583 .2079309
AL3082 UG/LITER 2614.910 3.816 .1459187
BA4934 UG/LITER 512.3502 .3554 .0693636
BE3130 UG/LITER 496.3783 .2473 .0498127
CA3179 UG/LITER 9286.478 377.510 4.065161
CD2265 UG/LITER 502.7268 .9033 .1796899
C02286 UG/LITER 509.2860 .3901 .0766902
ftl ff2 ft3
507.7838 509.2856 509.8263
2619.155 2613.806 2611.768
512.7311 512.0276 512.2919
496.1078 496.4343 496.5928
9078.020 9059.162 9722.254
503.1624 503.3299 501.6882
509.7364 509.0686 509.0631
ERRORS HIGH LOW
LC PASS 594.0000 396.0000
LC PASS 2978.000 1986.000
LC PASS 602.0000 402.0000
LC PASS 591.0000 395.0000
LC PASS 12216.00 8144.000
LC PASS 592.0000 395.0000
LC PASS 696.0000 397.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 502.3164 .4426 .0881035
CU3247 UG/LITER 511.3163 .8189 .1601625
FE2714 UG/LITER 6069.055 6.148 .1212842
K_7664 UG/LITER 8967.292 4.411 .0491848
MG2790 UG/LITER 6013.426 4.700 .0781515
MN2576 UG/LITER 495.9204 .2393 .0482460
NA3302 UG/LITER 10309.16 57.00 .5628853
ftl ft2 #3
502.8016 501.9349 502.2126
510.4178 511.5102 512.0208
5062.238 5074.181 5070.745
8972.037 8966.622 8963.317
6012.208 6009.456 6018.615
495.9337 496.1527 495.6747
10321.16 10369.20 10247.12
ERRORS HIGH LOW
LC PASS 588.0000 392.0000
LC PASS 588.0000 392.0000
LC PASS 6128.000 4086.000
LC PASS 12009.00 8007.000
LC PASS 7203.000 4803.000
LC PASS 594.0000 396.0000
LC PASS 12046.00 8031.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 506.7024 .7006 .1382743
TL1908 UG/LITER 1034.944 4.543 .4389145
V_2924 UG/LITER 508.6749 .2473 .0486131
ZN2138 UG/LITER 990.8723 .5126 .0517354
PB2203 UG/LITER 1012.566 .533 .0526762
SE1960 UG/LITER 995.7698 4.4456 .4464371
SB2068 UG/LITER 1010.371 1.058 .1046977
tfl #2 #3
507.0574 505.8953 507.1544
1029.704 1037.766 1037.361
508.9366 508.6433 508.4450
990.3810 991.4039 990.8320
1012.364 1012.162 1013.170
993.0218 1000.899 993.3890
1010.988 1010.976 1009.149
ERRORS HIGH LOW
LC PASS 590.0000 394.0000
LC PASS 1232.000 822.0000
LC PASS 601.0000 401.0000
LC PASS 1200.000 800.0000
LC PASS 1196.000 797.0000
LC PASS 1206.000 804.0000
LC PASS 1190.000 794.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1007.335 1.458 .1447639
22031 UG/LITER 1014.365 1.045 .1029976
22032 UG/LITER 1011.652 1 .246 .1232056
20681 UG/LITER 1009.604 2.664 .2539271
20682 UG/LITER 1010.760 2.707 .2677766
19601 UG/LITER 994.6143 5.7009 .5731755
19602 UG/LITER 996.0636 6.8161 .6843071
ftl #2 ft3
1006.680 1009.006 1006.318
1016.396 1014.391 1013.307
1010.836 1011.034 1013.087
1006.840 1010.066 1011.904
1013.066 1011.424 1007.770
988.6627 996.3962 999.8838
994.9645 1003.362 989.8636
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
1195.000 797.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.426182 2.479181 581.7186
BI2230 UG/LITER 3.760575 1.626156 43.35748
MO2020 UG/LITER .7141961 .2861863 39.93109
B_2496 TI3349 UG/LITER UG/LITER 3.862216 L3.261340 .110181 2.041960 52.87016 3.378406
Y_3710 PPM 1220.733 1.514 .1240564
#1 #2 ft3
1.942576 -.218414 -3.00271
4.624824 1.874303 4.752598
1.027090 .4688433 .6466549
6.564164 L3.379993 4.424440 L3.241774 1.598044 L3.162252
1219.000 1221.400 1221.800
ERRORS HIGH LOW
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
LC LOW 1200.000 800.0000
128
131 08/08/10 11:67:19 AM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1008010-04 RUN TIME: 08/08/10 11:50:22 COMMENT: SDG:MC0021 CLIENTID:MC0031 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .3398977 .0503963 14.82691
AL3082 UG/LITER 41.62212 4.87665 11.71649
BA4934 UG/LITER 38.19165 .19798 .5183991
BE3130 UG/LITER .0232459 .0353068 151.8840
CA3179 UG/LITER 11091.84 410.06 3.696989
CD2265 UG/LITER .0414384 .1482648 357.7969
C02286 UG/LITER .4460603 .3347688 75.05013
ftl ft2
#3
.3964000 .3237055 .2995878
36.50025 42.15659 46.20953
38.02331 38.40972 38.14162
-.017358 .0403730 .0467226
10870.63 11665.01 10839.89
.0785419 .1676276 -.121854
.6581872 .6198572 .0601365
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -6.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .1827228 .4603709 251.9505
CU3247 UG/LITER .9776525 .2091813 21.39629
FE2714 UG/LITER 152.0992 3.4556 2.271866
K_7664 UG/LITER 702.3480 3.7641 .5359297
MG2790 UG/LITER 2320.076 8.191 .3530583
MN2576 UG/LITER 270.1612 1.2016 .4447594
NA3302 UG/LITER 4087.916 75.665 1.850946
#1 ft2 ft3
.1529334 -.262030 .6572649
1.199307 .7837053 .9499457
148.5353 152.3273 155.4349
706.2950 698.7984 701.9506
2312.431 2328.721 2319.071
268.9300 271.3307 270.2229
4173.987 4031.878 4057.885
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.813195 .211322 25.98661
TL1908 UG/LITER .7595536 .6824941 89.85464
V_2924 UG/LITER .2402799 .0279263 11.62197
ZN2138 UG/LITER 2.638821 .132610 5.025341
PB2203 UG/LITER .2915104 .2517013 86.34388
SE1960 UG/LITER -.224611 1.035326 460.9423
SB2068 UG/LITER 1.001333 .470019 46.93932
#1
#2 ft3
-1.05717 -.694967 -.687458
.1513804 .6295985 1.497682
.2221558 .2262453 .2724387
2.491070 2.677875 2.747518
.4541578 .4187842 .0015891
-.086386 .7346591 -1.32211
1.544060 .7281775 .7317612
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.129919 .728401 560.6593
22031 UG/LITER 1.936351 .904106 46.69122
22032 UG/LITER -.540415 .100626 18.60156
20681 UG/LITER .9980550 1.609894 161.2836
20682 UG/LITER .9930596 .2933489 29.53991
19601 UG/LITER -1.89362 1.95918 103.4677
19602 UG/LITER .5986806 2.261627 377.7686
#1 #2 #3
.4020400 -.960109 .1683124
2.372408 2.539783 .8968615
-.514679 -.651307 -.455260
2.606874 .7765020 -.388211
1.003539 .6946114 1.281028
-3.88109 -1.83546 .0359847
1.798208 2.007849 -2.01002
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM in^ITS AVGE SDEV %RSD
SN1899 UG/LITER -.221910 1.664978 750.2952
BI2230 UG/LITER 1.520478 4.594008 302.1424
MO2020 UG/LITER .7047260 .2028386 28.78261
TI3349 UG/LITER 5.775430 .725519 12.56216
B_2496 UG/LITER 9.499209 .392125 4.127980
Y_3710 PPM 1233.333 3.367 .2730157
ftl ft2 If3
-1.06018 1.695601 -1.30115
6.006232 -3.17463 1.729829
.9053696 .7090470 .4997615
5.744509 5.065866 6.515914
9.376696 9.937964 9.182967
1233.400 1229.933 1236.667
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -60.0000
NOCHECK
129
132 08/08/10 12:04:19 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0080340-DUPl RUN TIME: 08/08/10 11:57:22 COMMENT: SDG:MC0021 CLIENTID:MC0031D 1:1 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0298623 .1447244 484.6382
AL3082 UG/LITER 23.24791 3.02557 13.01439
BA4934 UG/LITER 37.94909 .06634 .1748002
BE3130 UG/LITER -.075479 .022220 29.43879
CA3179 UG/LITER 10946.34 29.06 .2654763
CD2265 UG/LITER .1010227 .0941421 93.18908
C02286 UG/LITER .4324315 .1501334 34.71843
ftl ft2 #3
-.079684 -.024657 .1939279
26.05936 23.63827 20.04611
38.02086 37.89003 37.93639
-.057090 -.069179 -.100169
10979.21 10924.04 10935.78
.1129493 .1886332 .0014856
.5301386 .2696617 .5075943
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -6.00000
LC PASS 50000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .2607108 .1926233 73.84653
CU3247 UG/LITER 3.328768 .168487 5.061550
FE2714 UG/LITER 140.2717 5.6033 3.994571
K_7664 UG/LITER 697.7688 6.0213 .8629429
MG2790 UG/LITER 2307.109 2.999 .1299984
MN2576 UG/LITER 268.8859 .5108 .1899684
NA3302 UG/LITER 4173.576 58.675 1.405871
ftl #2 #3
.1066295 .1989730 .4765298
3.479177 3.146695 3.360433
144.7146 133.9769 142.1237
703.7394 697.8690 691.6980
2310.347 2304.427 2306.561
269.3415 268.3337 268.9826
4241.324 4139.070 4140.333
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.643958 .157444 28.94413
TL1908 UG/LITER -.239826 2.660812 1109.477
V_2924 UG/LITER .0955212 .3070557 321.4529
ZN2138 UG/LITER 1.766285 .109687 6.210014
PB2203 UG/LITER .4514701 .3744013 82.92937
SE1960 UG/LITER -.252109 .690644 273.9068
SB2068 UG/LITER .3661337 .8326594 227.4195
ftl ft2 ft3
-.668613 -.367025 -.596236
1.104323 -3.30457 1.480770
.4335208 -.166217 .0192600
1.768595 1.879614 1.660645
.3966789 .8602479 .1074834
.4736418 -.901017 -.328952
.4624460 -.510494 1.146449
ERRORS HIGH LOW
LC PASS 60000.00 -4 0 . 0 0 0 0
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1.12937 .11514 10.19506
22031 UG/LITER 2.224637 1.853032 83.29594
22032 UG/LITER -.444179 1.483970 334.0928
20681 UG/LITER .9650472 1.566090 162.2812
20682 UG/LITER .0671481 1.484116 2596.964
19601 UG/LITER -2.45064 2.34265 95.69339
19602 UG/LITER .8355312 .8312112 99.48296
ftl ft2 ft3
-1.00783 -1.23681 -1.14345
2.753856 .1645686 3.755488
-.791399 1.182616 -1.72375
-.837021 1.735505 1.996658
1.101199 -1.64177 .7120129
-1.44776 -5.12778 -.776377
1.422897 1.199240 -.115543
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER .1781388 .4682257 262.8431
BI2230 UG/LITER .2140484 .9837502 459.5924
MO2020 UG/LITER .4162942 .3018505 72.50893
TI3349 UG/LITER 4.227284 1.072718 25.37605
B_2496 UG/LITER 9.219868 .217400 2.357950
Y_3710 PPM 1225.311 3.099 .2529438
ftl ft2 #3
.2801675 .5869374 -.332688
1.219620 -.746322 .1688467
.5857203 .5953705 .0677918
4.213208 5.306971 3.161674
8.983506 9.264817 9.411279
1221.800 1227.667 1226.467
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
130
133 08/08/10 12:11:19 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0080340-MSl RUN TIME: 08/08/10 12:04:22 COMMENT: SDG:MC0021 CLIENTID:MC0031S MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 50.57632 .13269 .2623517
AL3082 UG/LITER 2055.082 1.756 .0854592
BA4934 UG/LITER 2044.752 2.805 .1371897
BE3130 UG/LITER 50.22501 .05337 .1062555
CA3179 UG/LITER 10738.74 386.16 3.595919
CD2265 UG/LITER 50.46558 .23786 .4713222
C02286 UG/LITER 507.9315 .3481 .0685287
#1 #2 #3
50.44331 50.70868 50.57697
2053.263 2055.213 2056.769
2047.443 2044.968 2041.845
50.26166 50.24959 50.16378
11007.26 10296.19 10912.76
50.46823 50.70211 50.22642
507.7362 508.3334 507.7250
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM in^ITS AVGE SDEV %RSD
CR2677 UG/LITER 201.9889 .4100 .2029579
CU3247 UG/LITER 255.2821 .3189 .1249273
FE2714 UG/LITER 1143.945 6.059 .5296695
K_7664 UG/LITER 684.9399 3.7579 .5486499
MG2790 UG/LITER 2271.792 2.321 .1021464
MN2576 UG/LITER 762.0220 .3741 .0490923
NA3302 UG/LITER 4106.508 32.660 .7953112
ftl #2 »3
201.6475 201.8757 202.4436
254.9179 255.4167 255.5117
1137.057 1148.453 1146.324
688.9569 684.3527 681.5101
2273.613 2272.710 2269.153
762.3597 762.0865 761.6199
4141.600 4100.923 4077.001
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -16.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 507.6399 1.0436 .2055872
TL1908 UG/LITER 48.49835 3.20759 6.613804
V_2924 UG/LITER 506.9780 .7366 .1452880
ZN2138 UG/LITER 482.9044 .9009 .1865535
PB2203 UG/LITER 20.98798 1.16788 5.564509
SE1960 UG/LITER 50.56374 1.39899 2.766777
SB2068 UG/LITER 102.4081 .9506 .9282468
#1 ft2 ft3
507.0443 508.8450 507.0304
52.05740 45.83086 47.60679
607.6193 507.1411 506.1735
483.6690 483.2662 481.8791
22.33147 20.41726 20.21521
60.39043 49.25948 62.04131
103.3814 102.3610 101.4819
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 39.22328 1.44239 3.677376
22031 UG/LITER 22.28020 1.25396 5.628136
22032 UG/LITER 20.33289 1.69318 8.327315
20681 UG/LITER 102.7009 1.1644 1.133744
20682 UG/LITER 102.2519 1.9792 1.935586
19601 UG/LITER 51.22356 .99370 1.939930
19602 UG/LITER 50.22438 1.60139 3.188463
ftl ft2 ft3
37.76104 39.26385 40.64496
22.78950 20.85172 23.19938
22.09282 20.19041 18.71545
101.3665 103.2334 103.5038
104.3778 101.9155 100.4626
51.11308 50.28972 52.26788
50.01967 48.73520 51.91828
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM ITOITS AVGE SDEV %RSD
SN1899 UG/LITER .8418167 1.761624 209.2645
BI2230 UG/LITER 2.265418 1.992298 87.94396
MO2020 UG/LITER .6393013 .1629035 25.48149
TI3349 UG/LITER 5.030106 .942569 18.73866
B_2496 UG/LITER 9.003758 .173783 1.930116
Y_3710 PPM 1229.911 5.035 .4093895
ftl ft2 ft3
1.435809 2.229664 -1.14002
4.036695 .1084864 2.651072
.5369842 .5537632 .8271564
4.329552 4.659026 6.101739
9.183105 8.992036 8.836132
1224.800 1230.066 1234.867
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
131
134 08/08/10 12:18:19 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: SDI1008010-04 RUN TIME: 08/08/10 12:11:22 COMMENT: SDG:MC0021 CLIENTID :MC0031L 1:5 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.050860 .604480 1188.524
AL3082 UG/LITER -9.20594 3.35165 36.40750
BA4934 UG/LITER 7.308163 .028259 .3866791
BE3130 UG/LITER -.082618 .039496 47.80431
CA3179 UG/LITER 1865.980 377.077 20.20800
CD2265 UG/LITER .0505258 .1177938 233.1362
C02286 UG/LITER .0387817 .2246380 579.2371
#1 #2 #3
.2180339 .3725176 -.743131
-7.28196 -7.25980 -13.0761
7.306378 7.337272 7.280838
-.043910 -.081088 -.122856
1647.312 1649.237 2301.390
-.066244 .1693172 .0485046
.1372193 .1973963 -.218271
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -6.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.384185 .465781 121.2390
CU3247 UG/LITER 5.315738 .233394 4.390624
FE2714 UG/LITER 29.06826 7.68269 26.42981
K_7 664 UG/LITER 119.1555 4.7310 3.970420
MG2790 UG/LITER 467.2021 1.9263 .4123115
MN2576 UG/LITER 53.69938 .03158 .0588178
NA3302 UG/LITER 761.7738 30.5419 4.009315
ftl ft2 #3
-.630480 .1530359 -.676110
5.046587 5.462189 5.438439
28.84538 36.85997 21.49944
122.7690 120.8968 113.8006
467.4057 469.0186 465.1821
53.73398 53.69206 53.67209
795.5820 753.5625 736.1769
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -26.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -1.35937 .27542 20.26076
TL1908 UG/LITER -1.42420 .60604 42.48275
V_2924 UG/LITER .1203263 .2109681 175.3300
ZN2138 UG/LITER .9178882 .1554999 16.94106
PB2203 UG/LITER -.021895 .254731 1163.439
SE1960 UG/LITER -.786847 1.975157 251.0218
SB2068 UG/LITER 1.610056 1.561099 96.95930
ftl #2 ft3
-1.40675 -1.06371 -1.60866
-.731137 -1.84702 -1.69445
-.031613 .3612001 .0313917
.7456388 1.047920 .9601066
.2608504 -.233477 -.093068
.2914477 .4144675 -3.06646
-.036515 3.068663 1.798019
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.848233 .635432 74.91241
22031 UG/LITER .8515848 2.168655 254.6611
22032 UG/LITER -.467907 1.108011 236.8015
20681 UG/LITER 2.270771 2.198599 96.82169
20682 UG/LITER 1.270266 2.703859 212.8678
19601 UG/LITER -5.35670 .53238 9.938665
19602 UG/LITER 1.484725 3.098502 208.6919
#1 #2 tf3
-.137847 -1.04441 -1.36245
.4286018 -1.07442 3.200570
.1671712 .1764246 -1.74732
3.579718 3.600131 -.267536
-1.85186 2.843313 2.819334
-5.02306 -5.97067 -5.07637
2.934787 3.592309 -2.07292
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER .6256939 2.698557 513.3323
BI2230 UG/LITER 1.054904 2.378036 226.4268
MO2020 UG/LITER .4189477 .0712104 16.99744
TI3349 UG/LITER .8300332 4.717987 568.4094
B_2496 UG/LITER 1.866867 .609132 32.62867
Y_3710 PPM 1231.044 1.535 .1247122
ftl ft2 #3
-2.17532 .5306087 3.221790
-1.37074 3.382281 1.153176
.4689605 .3374173 .4604652
.6543652 5.633400 -3.79767
1.659588 2.552588 1.388426
1230.667 1229.733 1232.733
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
132
135 ANALYSIS REPORT
08/08/10 12:25:19 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 00a0340-PSl RUN TIME: 08/08/10 12:18:22 COMMENT: SDG:MC0021 CLIENTID:MC0031A MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 15.56181 .18741 1.204289
AL3082 UG/LITER 27.70718 2.66469 9.617319
BA4934 UG/LITER 38.30045 .24434 .6379466
BE3130 UG/LITER 9.184540 .093963 1.023052
CA3179 UG/LITER 11393.94 432.02 3.791699
CD2265 UG/LITER 9.592500 .131818 1.374178
C02286 UG/LITER 94.55142 .67784 .7169019
#1 #2 #3
15.43384 15.77692 15.47466
25.46047 30.65119 27.00988
38.14378 38.58199 38.17558
9.098054 9.284520 9.171046
10900.64 11704.91 11576.26
9.709868 9.617747 9.449884
94.20271 95.33263 94.11892
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -6.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 18.85449 .39417 2.090602
CU3247 UG/LITER 48.58577 .30328 .6242199
FE2714 UG/LITER 148.2406 5.8239 3.928682
K_7664 UG/LITER 698.6733 5.9356 .8495568
MG2790 UG/LITER 2320.293 20.667 .8907173
MN2576 UG/LITER 298.1476 2.2867 .7669537
NA3302 UG/LITER 4189.636 66.340 1.344748
#1 ft2 #3
18.40382 19.13502 19.02461
48.29287 48.89846 48.66698
141.5431 152.1143 151.0645
699.3978 704.2134 692.4087
2305.595 2343.924 2311.360
296.2094 300.6695 297.5638
4239.202 4128.362 4201.344
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 73.70753 .61853 .8391724
TL1908 UG/LITER 44.44568 1.90129 4.277778
V_2924 UG/LITER 94.65622 .81940 .8656606
ZN2138 UG/LITER 104.7757 1.0081 .9621396
PB2203 UG/LITER 19.13894 .56448 2.897145
SE1960 UG/LITER 64.29308 1.14089 1.774517
SB2068 UG/LITER 113.0203 .6387 .5651498
#1 ft2 #3
73.61327 74.39987 73.20944
45.77977 45.28862 42.26865
94.09938 95.69711 94.27216
103.8498 105.8496 104.6276
18.89193 19.77400 18.75089
63.01228 65.20052 64.66643
112.7161 113.7543 112.5905
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 17.16225 .85988 5.010292
22031 UG/LITER 20.72089 1.47980 7.141591
22032 UG/LITER 18.33668 1.29549 7.065014
20681 UG/LITER 114.4192 1.7669 1.543350
20682 UG/LITER 112.3119 .4135 .3681687
19601 UG/LITER 59.99972 1.63286 2.721441
19602 UG/LITER 66.42656 .98603 1.482882
ftl #2 #3
16.18474 17.50022 17.80181
22.42893 19.90878 19.82496
17.11367 19.69416 18.20223
112.8591 116.3363 114.0621
112.6348 112.4561 111.8459
58.12640 60.75141 61.12136
66.44163 67.41168 66.42636
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI 899 UG/LITER -.164602 2.103848 1278.139
BI2230 UG/LITER .5738621 .6147137 107.1187
MO2020 UG/LITER .4751469 .2204154 46.38890
TI3349 UG/LITER 3.567009 1.047062 29.35405
B_2496 UG/LITER 9.452869 .294247 3.112784
Y_3710 PPM 1226.689 7.842 .6397892
#1 #2 #3
-1.54806 -1.20224 2.256493
.3302296 .1183090 1.273048
.4370979 .7121098 .2762330
2.383297 3.945667 4.372074
9.200743 9.776172 9.381662
1230.867 1216.667 1229.533
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
133
136 08/08/10 12:32:19 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1008010-01 RUN TIME: 08/08/10 12:25:22 COMMENT: SDG:MC0021 CLIENTID:MC0021 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.181104 .171591 94.74706
AL3082 UG/LITER -18.3648 4.1408 22.54722
BA4934 UG/LITER -.534408 .019643 3.675747
BE3130 UG/LITER -.079412 .032868 41.38876
CA3179 UG/LITER 1.626190 560.1961 34448.38
CD2265 UG/LITER .1255497 .2078116 165.5214
C02286 UG/LITER .0542091 .1123661 207.2826
#1 #2 #3
-.153773 -.024819 -.364720
-14.8007 -22.9071 -17.3867
-.546864 -.511726 -.545634
-.041656 -.094953 -.101627
326.7865 323.3216 -645.229
.0519829 -.035471 .3601375
-.053100 .0446990 .1710280
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -6.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.308497 .246197 79.80519
CU3247 UG/LITER 1.072647 .125853 11.73292
FE2714 UG/LITER -1.81702 4.86682 267.8469
K_7664 UG/LITER .1278379 1.442977 1128.766
MG2790 UG/LITER 6.653633 1.424384 21.40761
MN2676 UG/LITER -.340774 .026508 7.778770
NA3302 UG/LITER -23.7714 33.7416 141.9420
#1 #2 ft3
-.398261 -.030014 -.497217
1.092438 1.187432 .9380716
-6.82774 -3.22069 3.597371
1.767566 -.987313 -.386739
5.809691 5.863029 8.298179
-.313288 -.342852 -.366181
-34.1123 -51.1324 13.93052
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LG PASS 40000.00 -16.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.768101 .177136 23.06153
TL1908 UG/LITER -1.07714 1.19295 110.7515
V_2924 UG/LITER -.271537 .183309 67.50822
ZN2138 UG/LITER 1.441272 .017732 1.230292
PB2203 UG/LITER .0964210 1.210751 1268.851
SE1960 UG/LITER 1.115893 1.850297 165.8131
SB2068 UG/LITER 1.038767 .526522 50.68716
ffl «2 ft3
-.595465 -.759420 -.949417
-2.37446 -.027438 -.829511
-.112271 -.230429 -.471909
1.437071 1.426018 1.460727
-.923874 -.223602 1.433739
2.189456 2.178860 -1.02064
.6738617 1.642359 .8000810
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -2.16863 1.59589 73.59291
22031 UG/LITER 1.237204 .653101 52.78846
22032 UG/LITER -.485011 1.631390 336.3614
20681 UG/LITER 1.969579 1.113883 56.55437
20682 UG/LITER .5641445 .9002016 159.5693
19601 UG/LITER -2.72836 3.95069 144.8011
19602 UG/LITER 3.025220 1.218653 40.28313
ftl #2 ft3
-3.45763 -.383680 -2.66439
1.294998 .5571271 1.859488
-2.04278 -.623429 1.211178
.8433962 1.994600 3.070740
.5793278 1.456658 -.343563
.9048399 -2.15584 -6.93407
2.820903 4.333117 1.921639
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.619837 1.352561 218.2125
BI2230 UG/LITER 1.565627 1.132283 72.78629
MO2020 UG/LITER .5187331 .5806115 111.9287
TI3349 UG/LITER .8860503 .1997850 22.64781
B_2496 UG/LITER -.859261 .124493 14.48841
Y_3710 PPM 1232.400 10.038 .8145226
ftl #2 ft3
-2.04305 .6487820 -.465238
2.811129 .6118839 1.243867
-.144006 .7623962 .9378092
.7364337 .8087890 1.112928
-.721258 -.893407 -.963119
1234.533 1241.200 1221.467
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -60.0000
NOCHECK
134
137 08/08/10 12:39:19 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1008010-02 RUN TIME: 08/08/10 12:32:22 COMMENT: SDG:MC0021 CLIENTID:MC0029 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .1807987 .1713879 94.79492
AL3082 UG/LITER 23.20883 1.35331 5.830993
BA4934 UG/LITER 109.2918 .1548 .1416153
BE3130 UG/LITER -.112387 .012906 11.48366
CA3179 UG/LITER 135343.3 919.5 .6793737
CD2265 UG/LITER .2037188 .1427107 70.05280
C02286 UG/LITER 1.187696 .040415 3.402803
ftl ft2 #3
.1540745 .0243427 .3639789
24.66176 23.22936 21.84538
109.4316 109.1255 109.3184
-.098275 -.123592 -.115293
135035.7 136377.1 134617.0
.0986759 .1462819 .3661986
1.166904 1.234274 1.161909
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -6.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.049701 .188971 380.2196
CU3247 UG/LITER 2.505482 .134867 5.382856
FE2714 UG/LITER 2718.361 5.906 .2172729
K_7664 UG/LITER 2184.067 6.321 .2894295
MG2790 UG/LITER 10370.31 .33 .0031656
MN2576 UG/LITER 1883.213 .028 .0014770
NA3302 UG/LITER 50778.76 87.13 .1715830
ftl #2 #3
.1529462 -.080944 -.221103
2.669849 2.410488 2.446111
2711.548 2722.027 2721.508
2190.690 2178.098 2183.415
10369.93 10370.54 10370.45
1883.228 1883.181 1883.230
60708.55 50751.46 50876.27
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -16.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 2.707116 .092632 3.421780
TLI908 UG/LITER -6.13640 .79495 12.95461
V_2924 UG/LITER .1612231 .0976075 64.54538
ZN2138 UG/LITER 11.46864 .28240 2.464485
PB2203 UG/LITER 1.004886 .455533 45.33192
SE1960 UG/LITER -.169884 1.071770 670.3408
SB2068 UG/LITER 1.157277 1.553937 134.2753
ftl #2 #3
2.623586 2.806740 2.691021
-6.80469 -7.04348 -5.66103
.2314875 .0425676 .1796142
11.19543 11.42354 11.75694
1.461986 .5509353 1.001733
.7652672 -1.33433 .0894114
2.395231 1.663164 -.586566
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .1276710 1.571478 1230.880
22031 UG/LITER 1.860373 .481700 25.89266
22032 UG/LITER .5664539 .4754698 83.93796
20681 UG/LITER 1.078519 1.788270 165.8080
20682 UG/LITER 1.186515 2.704941 227.9737
19601 UG/LITER -2.72631 3.22234 118.1941
19602 UG/LITER 1.111322 .327367 29.45747
ftl ft2 #3
1.281750 .7633226 -1.66206
2.183652 1.306747 2.090719
1.090347 .1622986 .4467157
-.737774 2.837382 1.135948
3.949300 1.066855 -1.45661
-.503031 -6.42179 -1.25411
1.388380 1.195501 .7500855
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1.554 982 .802926 51.63572
BI2230 UG/LITER 2.526393 1.842018 72.93986
MO2020 UG/LITER .6828426 .1913768 28.02648
TI3349 UG/LITER 5.473481 2.491775 45.52451
B_2496 UG/LITER 48.91423 .36338 .7428871
Y_3710 PPM 1215.156 .482 .0396847
#1 #2 #3
2.471366 .9748402 1.218741
4.503842 2.212437 .8599015
.8586791 .7108391 .4790097
3.647279 4.461048 8.312117
49.30643 48.58898 48.84729
1214.600 1215.467 1215.400
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -60.0000
NOCHECK
135
138 08/08/10 12:46:19 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1008010-03 RUN TIME: 08/08/10 12:39:22 COMMENT: SDG:MC0021 CLIENTID:MC0030 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.355768 .077178 21.69344
AL3 082 UG/LITER 24.25072 3.77796 15.57874
BA4934 UG/LITER 38.02803 .18385 .4834679
BE3130 UG/LITER -.026058 .055310 212.2606
CA3179 UG/LITER 11287.05 448.00 3.969156
CD2265 UG/LITER .1039890 .0762843 73.35799
C02286 UG/LITER .1613843 .2383830 147.7113
ftl ft2 #3
-.266793 -.395876 -.404633
26.51996 26.34268 19.88951
38.22493 37.99831 37.86084
.0017152 .0098626 -.089751
11578.10 11511.90 10771.16
.0197762 .1684659 .1237250
-.047441 .4211047 .1104889
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -6.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.305835 .089931 29.40516
CU3247 UG/LITER 6.891065 .611537 8.874350
FE2714 UG/LITER 133.4569 6.64 82 4.157298
K_7664 UG/LITER 707.7744 8.3137 1.174629
MG2790 UG/LITER 2316.452 9.610 .4148691
MN2676 UG/LITER 257.8173 .8720 .3382281
NA3302 UG/LITER 4238.945 117.872 2.780689
ftl ft2 ft3
-.308885 -.214417 -.394202
6.222145 7.421452 7.029599
134.5669 138.3662 127.4376
715.6703 708.5550 699.0980
2321.707 2322.289 2306.360
258.1219 258.4961 256.8338
4369.357 4140.001 4207.477
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.200966 .345291 171.8160
TL1908 UG/LITER .0935926 2.122291 2267.584
V_2924 UG/LITER -.125684 .141002 112.1883
ZN2138 UG/LITER 10.68430 .34229 3.203646
PB2203 UG/LITER 1.475774 1.842382 124.8418
SE1960 UG/LITER .5342820 1.115828 208.8462
SB2068 UG/LITER .4929233 .4428355 89.83861
ftl #2 ft3
-.536156 .1536097 -.220351
-2.29470 1.763305 .8121732
-.082513 -.011313 -.283224
10.44654 11.07661 10.52975
2.942732 -.592021 2.076610
1.409191 -.722302 .9159570
.9837073 .3718358 .1232269
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.841318 .356759 42.40471
22031 UG/LITER 2.970105 2.257499 76.00739
22032 UG/LITER .7186021 1.671370 232.5863
20681 UG/LITER 1.337570 .615684 46.03002
20682 UG/LITER .0613429 .9154665 1492.375
19601 UG/LITER -2.89151 2.28001 78.86186
19602 UG/LITER 2.234718 .574792 26.72100
ftl ft2 ft3
-1.19851 -.840455 -.484992
5.101585 .6047895 3-203939
1.853729 -1.20066 1.502739
.6974212 1.925457 1.389833
1.116685 -.413706 -.518950
-1.41967 -5.51785 -1.73701
2.811544 1.661983 2.230626
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM iraiTS AVGE SDEV %RSD
SN1899 UG/LITER 1.552242 1.324665 85.33882
BI2230 UG/LITER -1.07947 2.04422 189.3722
MO2020 UG/LITER .5946605 .0922403 15.51143
TI3349 UG/LITER -1.84107 1.01711 55.24577
B_2496 UG/LITER 8.790343 .515438 5.863684
Y_3710 PPM 1236.111 7.891 .6383495
ftl ft2 #3
2.802891 1.689572 .1642614
-2.37649 -2.13894 1.277005
.4907381 .6668301 .6264134
-1.72906 -.884595 -2.90955
8.861813 8.242900 9.266316
1228.600 1235.400 1244.333
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
136
139 ANALYSIS REPORT
QC STANDARD
08/08/10 12:53:21 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCV RUN TIME: 08/08/10 12:46:23 COMMENT: CCV CVSl MODE: CONC CORR- FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 102.0482 .1003 .0983124
AL3082 UG/LITER 50658-27 32.53 .0642231
BA4934 UG/LITER 1014.750 .507 .0499715
BE3130 UG/LITER 1014.611 .741 .0730132
CA3179 UG/LITER 49172.43 589.29 1.198421
CD2265 UG/LITER 1001.220 .398 .0397368
C02286 UG/LITER 1002.454 1.430 .1426143
#1 «2 #3
102.1326 102.0747 101.9373
50634.05 50695.25 50645.50
1014.579 1015.320 1014.351
1013.848 1015.328 1014.656
49063.44 49808.62 48645.25
1001.092 1001.666 1000.901
1002.258 1003.972 1001.133
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1009.235 .760 .0752641
CU3247 UG/LITER 1015.116 1.208 .1190159
FE2714 tX3/LITER 25090.79 30.12 .1200449
K_7664 UG/LITER 48695.32 62.40 .1281370
MG2790 UG/LITER 50365.39 31.41 .0623563
MN2576 UG/LITER 997.1746 .5402 .0541773
NA33 02 UG/LITER 51131.05 41.61 .0813866
ftl ft2 ft3
1009.388 1009.907 1008.411
1014.281 1014.566 1016.501
25076.80 25125.36 25070.21
48706.18 48761.57 48628.21
50362.84 50401.12 50342.19
997.1004 997.7481 996.6753
51088.96 51172.17 51132.01
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 60000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1008.640 1.997 .1979517
TLI908 UG/LITER 1009.246 3.093 .3064880
V..2924 UG/LITER 1018.818 .319 .0312912
ZN2138 UG/LITER 1087.358 .507 .0465349
PB2203 UG/LITER 1001-715 .392 .0391597
SE1960 UG/LITER 1008.820 2.954 .2928175
SB2068 UG/LITER 1030.768 2.871 .2785168
ftl #2 #3
1007.060 1010.884 1007.975
1008.587 1006-536 1012-616
1019.105 1018.653 1018.615
1086.774 1087.622 1087.679
1001.796 1002.061 1001.289
1005.599 1011.402 1009.460
1027.892 1033.634 1030.778
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104-0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
OC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1019.313 1.039 .1019101
22031 UG/LITER 1001.027 3.934 .3929973
22032 UG/LITER 1002.043 1.395 .1392342
20681 UG/LITER 1031.440 5.494 .5326808
20682 UG/LITER 1030.429 1.698 .1648245
19601 UG/LITER 1001.079 .490 .0489114
19602 UG/LITER 1012.675 4.670 .4611431
#1 ft2 #3
1018.173 1020.205 1019.562
1002.769 1003.789 996.5228
1001.294 1001.183 1003.653
1025.429 1036.203 1032.688
1029.118 1032.348 1029.821
1001.636 1000.720 1000.880
1007.567 1016.725 1013.734
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1013.677 3.012 .2971776
BI2230 UG/LITER 1011.612 2.716 .2684406
MO2020 UG/LITER 1020.797 2.019 .1978331
TI3349 UG/LITER 1020.463 2.499 .2448448
B_2496 UG/LITER 1020.654 .757 .0741631
Y„3710 PPM 1212.267 1.538 .1268386
#1 #2 #3
1016.081 1010.298 1014.653
1008.488 1013.399 1012.951
1019.165 1020.172 1023.056
1019.347 1023.326 1018.717
1021.244 1019.800 1020.917
1211.733 1211.067 1214.000
ERRORS VALUE IRANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
137
140 ANALYSIS REPORT
QC STANDARD
08/08/10 01:00:22 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCB RUN TIME: 08/08/10 12:53:25 COMMENT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .2904124 .1274687 43.89232
AL3082 UG/LITER -9.17420 4.56082 49.71355
BA4934 UG/LITER -.449396 .028356 6.309825
BE3130 UG/LITER -.001475 .046087 3124.716
CA3179 UG/LITER 108.8216 379.1143 348.3815
CD2265 UG/LITER .2658786 .1816125 68.30655
C02286 UG/LITER .0825445 .1106034 133.9924
ffl
ft2 #3
.4364471 .2014678 .2333223
-12.2815 -11.3029 -3.93822
-.442534 -.480553 -.425100
-.037008 -.018017 .0505998
330.8960 -328.926 324.4951
.4607514 .1013485 .2355361
.2060687 -.007314 .0488792
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 6000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .1683610 .0957168 56.85213
CU3247 UG/LITER .2097799 .2508640 119.5844
FE2714 UG/LITER 8.561737 9.400273 109.7940
K_7 664 UG/LITER .3201985 3.593491 1122.270
MG2790 UG/LITER 19.99554 2.15949 10.79987
MN2576 UG/LITER -.313789 .029341 9.350584
NA3302 UG/LITER 2.953495 41.68069 1407.847
#1 it2 #3
.2453461 .1985466 .0611904
.4987217 .0474976 .0831205
17.52377 9.384182 -1.22274
4.038189 .0566952 -3.13429
22.42672 18.29992 19.25998
-.284079 -.314542 -.342747
47.36453 -3.45016 -35.0539
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.OOOOOO
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -1.82862 .18019 9.853903
TL1908 UG/LITER -2.23194 2.06032 92.31077
V^2924 UG/LITER -.160320 .231959 144.6846
ZN2138 UG/LITER -.058536 .022134 37.81327
PB2203 UG/LITER .1116803 .8670744 776.3894
SE1960 UG/LITER .6607555 .3279628 49.63461
SB2068 UG/LITER .8582087 .2106284 24.54279
#1 ft2 ft3
-1.91470 -1.94963 -1.62153
-.546790 -1.62016 -4.52885
.0863006 -.193141 -.374121
-.084085 -.046159 -.046364
-.461165 1.109232 -.313026
.6091493 1.011462 .3616552
.8123481 1.087989 .6742890
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
OC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.287793 .927618 322.3210
22031 UG/LITER .8347444 1.369808 164.0990
22032 UG/LITER -.259206 1.466999 565.9579
20681 UG/LITER .6005952 1.059818 176.4612
20682 UG/LITER .9769273 .7621450 78.01450
19601 UG/LITER -.189450 2.827586 1492.524
19602 UG/LITER 1.075324 1.213963 112.8927
#1 «2 S3
-1.33996 .0645521 .4120274
2.129119 .9748426 -.599728
-1.76432 1.166450 -.179751
-.219970 .2246098 1.797146
1.317785 1.509155 -1038413
2.271907 .4377013 -3.27796
-.230936 1.288036 2.168873
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -2.20352 .87944 39.91089
BI2230 UG/LITER .6792975 1.972846 290.4245
MO2020 UG/LITER 2.080542 1.306495 62.79590
TI3349 UG/LITER 3.571040 2.434020 68.15997
B_24 96 UG/LITER 1.329826 .055928 4.205653
Y_3710 PPM 1234.844 6.053 .4901434
ftl #2 ft3
-1.38090 -2.09918 -3.13048
1.820205 1.S16436 -1.59875
3.539706 1.019209 1.682711
6.182626 1.365710 3.164783
1.281604 1.391138 1.316737
1227.933 1237.400 1239.200
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
138
141 08/08/10
ANALYSIS REPORT METHOD: A L T - P 3 Q 3 SAMPLE NAME: 1 0 0 8 0 1 0 - 0 5 RUN T I M E : 0 8 / 0 8 / 1 0 1 3 : 0 0 : 2 5 COMMENT: SDG;MC0021 CLIENTID:MC0032 MODE: CONC CORR. FACTOR: 1
0 1 : 0 7 : 2 2 PM
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.089117 .218058 244.6859
AL3082 UG/LITER 33.23375 6.66051 20.04142
BA4934 UG/LITER 38.41580 .27819 .7241639
BE3130 UG/LITER -.081954 .016823 20.52699
CA3179 UG/LITER 11113.38 430.08 3.869932
CD2265 UG/LITER .0758684 .1526503 201.2042
C02286 UG/LITER .3168516 .1538937 48.56964
#1
ft2 #3
.1615940 -.194299 -.234647
39.27821 34.32988 26.09317
38.52262 38.62475 38.10003
-.062616 -.090032 -.093214
11602.48 10943.35 10794.30
-.039779 .0184904 .2488936
.4836516 .1803801 .2865232
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.368953 .066363 17.98420
CU3247 UG/LITER 2.034467 .285066 14.01183
FE2714 UG/LITER 162.1631 3.3968 2-094681
K_7664 UG/LITER 691.8695 6.2665 .9057305
MG2790 UG/LITER 2294.662 18.706 .8152283
MN2576 UG/LITER 292.5922 2.3842 .8148680
NA3302 UG/LITER 4082.140 105.446 2.583112
ftl ft2 ft3
-.356004 -.310029 -.440826
1.888017 2.362990 1.852394
158.8564 165.6425 161.9913
698.9440 687.0162 689.6482
2303.575 2307.055 2273.056
293.7724 294.1562 289.8481
4096.633 3970.196 4179.589
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -1.09421 .29868 27.29645
TLI908 UG/LITER 1.603830 1.467494 91.49938
V_2924 UG/LITER -.100899 .097375 96.50713
ZN2138 UG/LITER 5.466443 .159750 2.922376
PB2203 UG/LITER .6353753 .7685998 120.9678
SE1960 UG/LITER 1.227199 1.350688 110.0627
SB2068 UG/LITER ,8672045 .6951540 80.16032
ftl ft2 #3
-1.41071 -1.05463 -.817293
3.181794 1.349695 .2800004
.0111074 -.165433 -.148372
5.600409 5.509279 5.289642
-.249734 1.134332 1.021529
1.935827 -.330337 2.076107
1.339156 .0689250 1.193634
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1.97069 .29831 15.13748
22031 UG/LITER 2.313065 1.489063 64.37619
22032 UG/LITER -.213379 .415511 194.7291
20681 UG/LITER .5422688 .9118341 168.1517
20682 UG/LITER 1.019505 -886027 86.90756
19601 UG/LITER 1.254425 1.474217 117.5213
19602 UG/LITER 1.203675 1.728328 143.5876
#1 #2 ft3
-1.91305 -1.70540 -2.29361
.6137009 3.389529 2.935965
-.692021 -.002788 .0546723
.1548287 -.111867 1.583844
1.920468 .1492107 .9888358
.4228278 .3838913 2.956556
2.681219 -.696891 1.626696
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.401547 1.759789 73.27730
BI2230 UG/LITER .1175302 .8073575 686.9362
MO2020 UG/LITER .6778300 .7851199 115.8285
TI3349 UG/LITER .8540127 .7999466 93.66916
B_2496 UG/LITER 9.335383 .524707 6.620624
Y_3710 PPM 1231.244 9.203 .7474514
#1 #2 ft3
1.577212 1.205234 4.422195
1.011683 -.558006 -.101087
.3349482 1.576070 .1224715
1.722166 .6931512 .1467208
9.879723 9.293624 8.832805
1226.200 1225.667 1241.867
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
139
142 08/08/10 01:14:22 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1008010-06 RUN TIME: 08/08/10 13:07:25 COMMENT: SDG:MC0021 CLIENTID:MC0033 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.142592 .101195 70.96828
AL3082 UG/LITER 157.7484 5.6874 3.605333
BA4934 UG/LITER 39.76035 .07176 .1804791
BE3130 UG/LITER -.035778 .040208 112.3829
CA3179 UG/LITER 10947.06 39.18 .3579194
CD2265 UG/LITER .0001754 .0431711 24620.47
C02286 UG/LITER .5274994 .2996487 56.80551
ftl »2 ft3
-.250060 -.049128 -.128589
151.9732 157.9284 163.3436
39.68275 39.77399 39.82431
-.075764 -.036217 .0046481
10992.02 10928.96 10920.20
.0203320 -.049387 .0295815
.8005358 .5750400 .2069222
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -6.OOOOO
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.140065 .162071 115.7109
CU3247 UG/LITER 1.120145 .197747 17.65370
FE2714 UG/LITER 341.3200 3.7288 1.092467
K_7664 UG/LITER 704.1166 5.2213 .7415414
MG2790 UG/LITER 2305.359 3.795 .1646323
MN2576 UG/LITER 287.6046 .4318 .1501373
NA3302 UG/LITER 4085.787 85.130 2.083566
ftl #2 «3
.0134555 -.309511 -.124141
1.341799 1.056815 .9618204
345.5933 339.6396 338.7272
708.5015 698.3406 705.5076
2304.552 2302.032 2309.493
287.2263 287.6125 288.0750
4172.189 4001.988 4083.184
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.322101 .184770 57.36391
TL1908 UG/LITER -2.40781 1.25917 52.29550
V_2924 UG/LITER .0491567 .2736806 556.7514
ZN2138 UG/LITER 3.608704 .081763 2.265729
PB2203 UG/LITER .8144145 1.210141 148.5903
SE1960 UG/LITER 2.415241 1.275418 52.80705
SB2068 UG/LITER .6464453 .2872400 44.43377
.415925 .109244 .441134
-3.83322 -1.94343 -1.44677
.1450020 -.259556 .2620238
3.686544 3.616054 3.523514
1.925432 -.475037 .9928485
2.569505 3.606611 1.069708
.9454702 .6212104 .3726552
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1.43526 .77308 53.86314
22031 UG/LITER 1.303875 1.924302 147.5833
22032 UG/LITER .5592462 1.828015 326.8713
20681 UG/LITER 1.121756 1.786677 159.2752
20682 UG/LITER .3991703 .5039682 126.2539
19601 UG/LITER 1.157927 2.402031 207.4424
19602 UG/LITER 3.032978 2.653774 84.20023
ftl ft2 »3
-.590497 -1.60779 -2.10760
.4431370 -.039816 3.508303
2.655451 -.703529 -.274184
3.170275 .3093657 -.114376
-.175282 .7669411 .6058518
-1.65387 2.009461 3.018187
4.618081 4.393877 .0869758
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.169926 2.016800 1261.089
BI2230 UG/LITER 1.736320 1.195504 68.85277
MO2020 UG/LITER .4360829 .0897558 20.58227
TI3349 UG/LITER 3.146620 2.247473 71.42497
B_2496 UG/LITER 8.941387 .302613 3.384404
Y_3710 PPM 1226.333 4.130 .3370148
ftl ft2 #3
1.463874 -2.41749 .4738374
.3678094 2.577466 2.263683
.3569203 .5335957 .4177326
5.533429 2.835537 1.070895
9.274208 8.867155 8.682797
1220.600 1227.200 1228.200
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
#1 ft2 »3
140
143 08/08/10 01:21:22 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1008010-07 RUN TIME: 08/08/10 13:14:25 COMMENT: SDG:MC0021 CLIENTID:MC0034 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.010895 .268475 2464.108
AL3082 UG/LITER 10.29324 6.69716 65.06364
BA4934 UG/LITER 37.48475 .18114 .4832317
BE3130 UG/LITER -.083788 .046906 55.98128
CA3179 UG/LITER 10898.33 50.43 .4627170
CD2265 UG/LITER .1472174 .1323093 89.87344
C02286 UG/LITER .4077965 .2673923 65.57002
#1 #2 #3
-.152996 .2987639 -.178455
16.40899 11.33416 3.136570
37.63014 37.54229 37.28183
-.040085 -.077933 -.133346
10953.69 10886.29 10855.01
.2976122 .0483136 .0958264
.7149926 .2810698 .2273371
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.015734 .418158 2657.611
CU3247 UG/LITER 2.901293 .076341 2.631270
FE2714 UG/LITER 139.4236 6.6362 4.759746
K_7664 UG/LITER 686.3826 14.1595 2.062910
MG2790 UG/LITER 2284.563 9.628 .4214277
MN2576 UG/LITER 254.6668 1.0192 .4002138
NA3302 UG/LITER 4122.367 61.598 1.494241
ftl ft2 #3
.2919571 -.491839 .1526789
2.932957 2.956706 2.814215
143.6865 142.8066 131.7776
702.6834 679.3290 677.1353
2293.305 2286.140 2274.244
255.6494 254.7363 253.6146
4180.907 4058.109 4128.086
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.900041 .056492 6.276621
TLI908 UG/LITER -2.21214 .49680 22.45768
V_2924 UG/LITER -.048964 .241456 493.1263
ZN2138 UG/LITER 1.463839 .059551 4.068150
PB2203 UG/LITER .4966221 .3346351 67.38223
SE1960 UG/LITER -1.06502 .90694 85.16738
SB2068 UG/LITER .5718395 .8923387 156.0471
ftl ft2 #3
-.834856 -.930501 -.934765
-1.83688 -2.77553 -2.02403
:1942592 -.052538 -.288614
1.532545 1.431924 1.427047
.2318416 .8727317 .3852932
-.884073 -2.04880 -.262191
.1383168 1.598114 -.020913
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.291731 1.077167 369.2330
22031 UG/LITER 1.630144 .698098 42.82433
22032 UG/LITER -.079222 .413126 521.4802
20681 UG/LITER 1.261420 .280917 22.26991
20682 UG/LITER .2176336 1.211696 556.7696
19601 UG/LITER -5.01260 3.08475 61.53994
19602 UG/LITER .8958707 .6942558 77.49509
ftl #2 #3
.9423416 -1.04326 -.774277
1.788838 2.235233 .8663600
-.555474 .1825775 .1352316
1.014965 1.567293 1.202002
-.309334 1.603586 -.641351
-6.04451 -7.44910 -1.54418
1.682291 .6373788 .3679426
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.108840 1.479709 1359.530
BI2230 UG/LITER 1.942826 1.669503 85.93165
MO2020 UG/LITER .2587514 .3564019 137.7391
TI3349 UG/LITER 4.036745 2.875997 71.24546
B_2496 UG/LITER 8.995997 .590336 6.562211
Y_3710 PPM 1230.422 5.376 .4369078
ftl #2 #3
-1.56988 1.388859 -.145500
2.707514 3.093023 .0279425
.1835839 .6467417 -.054071
6.236079 5.091970 .7821862
9.122612 9.512754 8.352627
1224.533 1231.667 1236.066
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
141
144 ANALYSIS REPORT
08/08/10 01:28:23 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 1008010-08 RUN TIME: 08/08/10 13:21:26 COMMENT: SDG:MC0021 CLIENTID:MC0035 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .1515195 .1741245 114.9189
AL3082 UG/LITER -.019335 4.762176 24629.37
BA4934 UG/LITER 77.90741 .06302 .0808971
BE3130 UG/LITER -.057582 .042603 73.98690
CA3179 UG/LITER 117448.5 609.2 .5186933
CD2265 UG/LITER .0940030 .0392245 41.72689
C02286 UG/LITER .3036761 .1098007 36.15718
#1 #2 #3
.3155051 -.031226 .1702783
-4.08009 -1.20004 5.222121
77.95813 77.92725 77.83685
-.089212 -.074397 -.009137
116933.9 117290.4 118121.1
.0560010 .1343453 .0916629
.3363215 .3934519 .1812548
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.344763 .135016 39.16184
CU3247 UG/LITER 1.579285 .148785 9.421038
FE2714 UG/LITER 66.32104 5.19446 9.222938
K_7664 UG/LITER 2145.916 5.917 .2757176
MG2790 UG/LITER 8898.081 2.008 .0225707
MN2576 UG/LITER 69.43782 .11520 .1659063
NA3302 UG/LITER 42884.86 209.08 .4875478
ftl «2 #3
-.268449 -.500654 -.265186
1.591160 1.721777 1.424918
51.59925 56.47867 61.88520
2152.733 2142.899 2142.117
8900.398 8896.853 8896.990
69.35778 69.56986 69.38583
43068.94 42928.10 42657.54
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -1.13380 .06410 5.653238
TL1908 UG/LITER -3.11832 2.99760 96.12888
V_2924 UG/LITER .2868522 .1294079 45.27090
ZN2138 UG/LITER 3.090020 .091361 2.956651
PB2203 UG/LITER 1.090094 .489709 44.92353
SE1960 UG/LITER 2.102116 1.690690 80.42803
SB2068 UG/LITER 1.697510 1.367827 79.98932
ftl #2 ft3
-1.20777 -1.09900 -1.09463
.0516903 -5.90703 -3.49961
.1780514 .4293664 .2601388
3.194928 3.047189 3.027944
.8842638 .7368946 1.649123
3.920441 1.808340 .6775650
2.195846 .1609262 2.735768
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -60.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -6.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.958970 1.478481 154.1739
22031 UG/LITER 2.955386 1.547346 52.35683
22032 UG/LITER .1475330 .0621283 42.11149
20681 UG/LITER 1.099691 1.252657 113.9099
20682 UG/LITER 1.985914 1.744806 87.85906
19601 UG/LITER .7878882 4.349742 652.0760
19602 UG/LITER 2.748187 4.136942 150.5335
ftl #2 #3
-2.04848 .7240446 -1.55248
2.414418 1.751160 4.700587
.1089808 .2192040 .1144142
2.480614 .0364848 .7819741
2.043584 .2129887 3.701170
-.214892 -2.97289 5.561446
6.974916 4.185307 -1.91566
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER -.178811 2.892786 1617.790
BI2230 UG/LITER 1.455251 1.734032 119.1569
MO2020 UG/LITER .8293368 .6809289 82.10523
TI3349 UG/LITER 4.682877 1.124932 24.02224
B_2496 UG/LITER 50.87295 .48005 .9436185
Y_3710 PPM 1217.911 4.634 .3805138
ftl #2 #3
1.399768 -3.51747 1.581268
.6434398 3.446271 .2760424
1.413023 .0812626 .9937246
5.019989 5.600709 3.427933
51.35082 50.87728 50.39076
1213.800 1217.000 1222.933
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
142
145 08/08/10 01:35:24 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0072821-BLKl RUN TIME: 08/08/10 13:28:27 COMMENT: SDG:MY71S3 CLIENTID:PBW 1:1 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0563608 .0793008 140.7021
AL3082 UG/LITER -21.2272 3.7960 17.87780
BA4934 UG/LITER -.475337 .035272 7.420423
BE3130 UG/LITER -.079654 .031489 39.53243
CA3179 UG/LITER 3.867506 327.7412 8474.227
CD2265 UG/LITER .1767346 .0431700 24.56544
C02286 UG/LITER -.037272 .217554 583.6901
ftl'
#2 #3
.1451211 .0314693 -.007508
-17.3635 -21.3900 -24.9382
-.516296 -.462185 -.448532
-.045975 -.084624 -.108362
326.7703 13.33891 -328.507
.1376816 .1668752 .2226470
-.127143 -.195492 .2108188
ERRORS HIGH LOW
LC PASS 5.000000 -5.00000
LC PASS 200.0000 -200.000
LC PASS 200.0000 -200.000
LC PASS 5.000000 -5.00000
LC PASS 5000.000 -5000.00
LC PASS 5.000000 -5.00000
LC PASS 50.00000 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .1220538 .3819885 312.9672
CU3247 UG/LITER 5.561141 .090692 1.630810
FE2714 UG/LITER 4.772304 4.030384 84.45364
K_7664 UG/LITER 2.173583 2.541303 116.9407
MG2790 UG/LITER 5.458312 .765737 13.84562
MN2576 UG/LITER -.378665 .031839 8.408618
NA3302 UG/LITER -41.9199 66.4376 158.4870
#1 #2 #3
-.306218 .4275836 .2447956
6.462189 5.580932 6.640304
6.775108 .1328284 7.408974
2.216807 -.389557 4.693498
5.677589 4.650030 6.147318
-.397073 -.341890 -.397001
5.961876 -117.769 -13.9526
ERRORS HIGH LOW
LC PASS 10.00000 -10.0000
LC PASS 25.00000 -25.0000
LC PASS 100.0000 -100.000
LC PASS 5000.000 -5000.00
LC PASS 5000.000 -5000.00
LC PASS 15.00000 -15.0000
LC PASS 5000.000 -6000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 3.272936 .219834 6.716708
TL1908 UG/LITER -1.35299 1.23891 91.56821
V_2924 UG/LITER -.073862 .281043 380.5477
ZN2138 UG/LITER .1503601 .0632081 42.03778
PB2203 UG/LITER .3103591 .8066439 259.9066
SE1960 UG/LITER .1652093 .8976220 643.3242
SB2068 UG/LITER 1.120062 1.163956 103.9189
ftl #2 #3
3.078026 3.511226 3.229555
.0631284 -2.23669 -1.88540
-.113665 -.332866 .2249740
.1374336 .0946146 .2190322
-.541236 1.062904 .4094086
-.267104 1.197181 -.434449
-.212988 1.935003 1.638171
ERRORS HIGH LOW
LC PASS 40.00000 -40.0000
LC PASS 10.00000 -10.0000
LC PASS 50.00000 -50.0000
LC PASS 60.00000 -60.0000
LC PASS 10.00000 -10.0000
LC PASS 35.00000 -35.0000
LC PASS 60.00000 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.990545 1.860356 187.8113
22031 UG/LITER .9334108 .2678129 28.69186
22032 UG/LITER -.010588 1.292824 12210.80
20681 UG/LITER .8485058 1.582118 186.4594
20682 UG/LITER 1.245752 1.819969 146.0940
19601 UG/LITER .4992574 2.023152 406.2324
19602 UG/LITER -.011453 .765201 6681.426
#1 #2 #3
-2.69385 .9946808 -1.27247
1.201446 .9329649 .6658211
-1.42116 1.117902 .2715000
.8449237 2.432412 -.731819
-.761044 1.676796 2.811504
-1.60223 2.643403 .4665953
.3396368 .5152029 -.889198
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
10.00000 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER -.879383 1.182713 134.4935
BI2230 UG/LITER -2.50436 .33271 13.28530
MO2020 UG/LITER .1701768 .6495676 381.6957
TI3349 UG/LITER 3.445016 1.485810 43.12926
B_24 96 UG/LITER -.955999 .265241 27.74496
Y_3710 PPM 1235.822 1.309 .1058966
#1 #2 #3
-2.16543 .1616020 -.634322
-2.52284 -2.82745 -2.16279
-.559012 .3826614 .6868814
2.726021 2.455471 5.153557
-.707382 -1.23521 -.925402
1235.066 1237.333 1236.066
ERRORS HIGH LOW
LC PASS 100.0000 -100.000
LC PASS 50.00000 -50.0000
LC PASS 10.00000 -10.0000
LC PASS 40.00000 -40.0000
LC PASS 10.00000 -10.0000
NOCHECK
143
146 0 8 / 0 8 / 1 0 0 1 : 4 2 : 2 4 PM
ANALYSIS REPORT
METHOD: A L T - P 3 Q 3 SAMPLE NAME: 0 0 7 2 8 2 1 - B S l RUN T I M E : 0 8 / 0 8 / 1 0 1 3 : 3 5 : 2 7 COMMENT: SDG:MY71S3 CLIENTID:LCSW MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 513.3624 1.1391 .2218983
/U.3082 UG/LITER 2576.171 2.332 .0905260
BA4934 UG/LITER 514.3608 .5583 .1085482
BE3130 UG/LITER 500.8013 .2572 .0513583
CA3179 UG/LITER 9036.599 19.716 .2181714
CD2265 UG/LITER 505.3303 .6832 .1352018
C02286 UG/LITER 511.4505 .4588 .0897052
ftl ft2 ft3
512.1034 513.6621 514.3218
2578.816 2574.410 2575.288
514.9950 514.0068 514.0518
500.7229 500.5925 501.0886
9058.861 9021.348 9029.587
505.9866 505.3812 504.6230
511.9488 511.3572 511.0455
ERRORS HIGH LOW
LC PASS 594.0000 396.0000
LC PASS 2978.000 1986.000
LC PASS 602.0000 402.0000
LC PASS 591.0000 395.0000
LC PASS 12216.00 8144.000
LC PASS 592.0000 395.0000
LC PASS 595.0000 397.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 504.5630 .3777 .0748602
CU3247 UG/LITER 515.8562 1.0618 .2058291
FE2714 UG/LITER 5079.178 4.810 .0947097
K_7664 UG/LITER 8953.476 23.869 .2665915
MG2790 UG/LITER 6028.917 2.366 .0392428
MN2576 UG/LITER 497.3537 .2865 .0575999
NA3302 UG/LITER 10227.26 37.63 .3679475
ftl ft2 #3
504.3702 504.3206 504.9982
514.7400 515.9749 616.8636
5073.633 5081.658 5082.242
8975.772 8956.357 8928.295
6030.717 6029.796 6026.237
497.6802 497.2370 497.1441
10266.50 10191.48 10223.81
ERRORS HIGH LOW
LC PASS 588.0000 392.0000
LC PASS 588.0000 392.0000
LC PASS 6128.000 4086.000
LC PASS 12009.00 8007.000
LC PASS 7203.000 4803.000
LC PASS 594.0000 396.0000
LC PASS 12046.00 8031.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 512.2457 .9243 .1804376
TL1908 UG/LITER 1041.970 4.677 .4488615
V_2924 UG/LITER 510.7552 .6698 .1311438
ZN2138 UG/LITER 995.4979 .6638 .0666786
PB2203 UG/LITER 1017.284 1.625 .1498827
SE1960 UG/LITER 1016.875 3.264 .3199911
SB2068 UG/LITER 1016.773 2.444 .2404130
ftl ft2 #3
513.2282 512.1158 511.3933
1036.589 1046.060 1044.259
511.2492 511.0234 509.9928
995.1339 996.2640 995.0957
1019.027 1016.626 1016.198
1019.217 1018.248 1013.159
1019.484 1014.736 1016.099
ERRORS HIGH LOW
LC PASS 690.0000 394.0000
LC PASS 1232.000 822.0000
LC PASS 601.0000 401.0000
LC PASS 1200.000 800.0000
LC PASS 1196.000 797.0000
LC PASS 1206.000 804.0000
LC PASS 1190.000 794.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1016.165 5.383 .5297033
22031 UG/LITER 1018.021 .944 .0927308
22032 UG/LITER 1016.901 1.818 .1787369
20681 UG/LITER 1016.667 4.489 .4414947
20682 UG/LITER 1016.823 1.643 .1615472
19601 UG/LITER 1009.384 3.761 .3726134
19602 UG/LITER 1020.330 4.005 .3925212
ftl ft2 ft3
1022.192 1011.835 1014.469
1019.080 1017.716 1017.267
1018.986 1016.067 1015.660
1021.850 1014.094 1014.066
1018.299 1015.053 1017.115
1013.727 1007.177 1007.248
1021.672 1023.491 1015.826
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
1195.000 797.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.402579 3.482677 865.0919
BI2230 UG/LITER 1.001376 1.936112 193.3452
MO2020 UG/LITER -.080626 .165598 205.3898
B_2496 TI3349 UG/LITER UG/LITER 2.555986 L-l.05514 .20593 3.045315 119.1445 19.51724
Y_3710 PPM 1224.355 2.509 .2049225
#1 #2 #3
.7895371 2.327499 -4.32477
3.209902 -.403455 .1976809
.0339027 -.005282 -.270500
-.575355 L-.831981 2.736024 L-l.09560 5.507288 L-l.23784
1221.533 1226.333 1225.200
ERRORS HIGH LOW
NOCHECK
NOCHECK
NOCHECK
NOCHECK
LC LOW 1200.000 800.0000
NOCHECK
144
147 ANALYSIS REPORT
0 8 / 0 8 / 1 0 0 1 : 4 9 : 2 5 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 1 0 0 7 1 5 7 - 0 7 RUN TIME: 0 8 / 0 8 / 1 0 1 3 : 4 2 : 2 8 COMMENT: SDG:MY71S3 CLIENTID:MY71T5 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.155730 .364001 233.7377
AL3082 UG/LITER 23478.55 277.63 1.182071
BA4934 UG/LITER 39.72989 .47201 1.188036
BE3130 UG/LITER 1.341311 .012207 .9097385
CA3179 UG/LITER 114895.6 947.4 .8245907
CD2265 UG/LITER 1.382617 .058348 4.220138
C02286 UG/LITER 117.3449 1.0972 .9349930
#1 #2 ft3
.0471078 -.575958 .0616592
23158.14 23643.94 23633.56
39.18771 40.04916 39.96279
1.330267 1.354588 1.340579
113807.2 115343.9 115535.6
1.355688 1.342684 1.449579
116.0784 117.9519 118.0044
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 13.10378 .42941 3.276964
CU3247 UG/LITER 20.05177 .27138 1.353412
FE2714 UG/LITER 42899.54 481.82 1.123125
MG2790 K_7664 UG/LITER UG/LITER 10876.97 H304860.3 91.88 3860.6 .8446770 1.266337
MN2676 UG/LITER 2366.670 29.149 1.231632
NA3302 UG/LITER 120722.0 1309.5 1.084724
#1 ft2 #3
12.77807 12.94287 13.59040
19.91324 19.87762 20.36446
42344.72 43212.70 43141.19
10771.41 H300403.0 10938.95 H307030.1 10920.54 H307147.8
2333.015 2383.839 2383.167
119220.0 121321.5 121624.4
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC HIGH 300000.0 -1000.00
LC PASS 40000.00 -16.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 339.2985 4.7669 1.404919
TL1908 UG/LITER .8379331 1.028733 122.7703
V_2924 UG/LITER 2.302107 .321060 13.94636
ZN2138 UG/LITER 1141.973 15.441 1.352146
PB2203 UG/LITER 4.338736 .322028 7.422171
SE1960 UG/LITER 2.757508 .625198 22.67259
SB2068 UG/LITER 2.357642 .372806 15.81268
#1 #2 #3
333.9883 340.6988 343.2084
.9785902 1.789100 -.253891
2.649482 2.240566 2.016271
1124.204 1149.589 1152.127
4.043584 4.290438 4.682186
3.478669 2.368330 2.425624
2.771859 2.049029 2.252039
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -6.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .2960270 .4943034 166.9792
22031 UG/LITER 3.723731 1.696203 45.55117
22032 UG/LITER 4.634091 1.033331 22.29846
20681 UG/LITER 2.680936 1.499848 58.11255
20682 UG/LITER 2.236561 1.231137 55.04597
19601 UG/LITER -2.74484 2.49497 90.89674
19602 UG/LITER 5.494948 .720792 13.11736
ftl #2 #3
.4649226 .6837459 -.260688
6.117251 1.835048 4.218893
3.492792 6.506153 4.903328
.9997025 2.759736 3.983368
3.647094 1.684570 1.378018
-.465846 -5.41060 -2.35806
5.438449 6.242328 4.804069
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 4.187913 3.700190 88.35403
BI2230 UG/LITER 2.674195 .787694 29.45536
MO2020 UG/LITER .8655949 .4436766 51.25684
TI3349 UG/LITER 4.622616 4.763057 103.0381
B_2496 UG/LITER 3499.030 37.160 1.062010
Y_3710 PPM 1274.600 9.927 .7788016
ftl ft2 ft3
7.238128 .0717537 6.263859
1.777905 3.256354 2.988327
.3815534 .9622662 1-262966
-.743576 6-261826 8.349598
3456.236 3523.144 3517.711
1286.000 1269.933 1267.867
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
145
148 ANALYSIS REPORT
QC STANDARD
08/08/10 01:56:25 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CRI RUN TIME: 08/08/10 13:49:28 COMMENT: CRI MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 8.495004 .180678 2.126871
AL3082 UG/LITER -28.6516 2.0967 7.317933
BA4934 UG/LITER -.393567 .019441 4.939601
BE3130 UG/LITER 4.870145 .024101 .4948624
CA3179 UG/LITER -634.197 .392 .0618091
CD2265 UG/LITER 5.338255 .125554 2.351976
C02286 UG/LITER 51.33035 .10120 .1971543
ftl ft2 ft3
8.618772 8.287670 8.578569
-26.3195 -29.2546 -30.3808
-.378393 -.415481 -.386828
4.897973 4.856200 4.856260
-634.569 -634.235 -633.787
5.368890 5.200218 5.445656
51.44437 51.26121 51.29545
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS .OOOOOOO 400.0000
QC PASS .OOOOOOO 400.0000
QC PASS 5.000000 1.600000
QC PASS .OOOOOOO 2000.000
QC PASS 5.000000 1.500000
QC PASS 50.00000 15.00000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 9.610616 .199329 2.074070
CU3247 UG/LITER 26.92560 .17864 .6890482
FE2714 UG/LITER -1.21664 2.39916 197.1962
K_7664 UG/LITER 1.061999 2.461330 231.7639
MG2790 UG/LITER 8.318285 1.729887 20.79620
MN2576 UG/LITER 14.54498 .10993 .7557944
NA3302 UG/LITER -8.96266 67.90632 757.6577
ftl ft2 ft3
9.425125 9.821342 9.585083
25.75541 25.90977 26.11163
-.535660 -3.88268 .7684240
3.747887 -1.08571 .5238186
10.26803 6.967392 7.719437
14.67145 14.47238 14.49110
50.23502 -83.0923 5.969321
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS 25.00000 7.500000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 2000.000
QC PASS .OOOOOOO 2000.000
QC PASS 15.00000 4.500000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 38.07646 .59410 1.560274
TL1908 UG/LITER 24.91290 1.96432 7.884740
V_2924 UG/LITER 50.71853 .03739 .0737178
ZN2138 UG/LITER 54.17009 .19289 .3560853
PB2203 UG/LITER 9.737345 .198371 2.037221
SE1960 UG/LITER 35.08679 .93224 2.656968
SB2068 UG/LITER 62.91098 1.48642 2.362737
ftl ft2 ft3
38.27559 37.40838 38.54541
23.34334 27.11574 24.27961
50.67942 50.72226 50.75391
54.14360 54.37486 53.99182
9.960462 9.670680 9.580894
34.43485 36.15459 34.67093
64.18819 61.27940 63.26536
ERRORS VALUE RANGE
QC PASS 40.00000 12.00000
QC PASS 25.00000 12.50000
QC PASS 50.00000 15.00000
QC PASS 60.00000 18.00000
QC PASS 10.00000 5.000000
QC PASS 35.00000 10.60000
QC PASS 60.00000 30.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 9.055884 1.199115 13.24128
22031 UG/LITER 11.27883 1.49391 13.24522
22032 UG/LITER 8.952834 .541073 6.043597
20681 UG/LITER 61.95419 1.53051 2.470386
20682 UG/LITER 63.37871 1.53155 2.416503
19601 UG/LITER 34.72493 1.17630 3.387468
19602 UG/LITER 35.25750 1.73648 4.925145
#1 ft2 ft3
7.683483 9.901030 9.583139
12.37428 11.88513 9.577094
8.740417 8.550202 9.567884
62.79183 60.18769 62.88303
64.87535 61.81449 63.44629
36.05651 34.29118 33.82711
33.61527 37.07495 35.08227
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
10.00000 3.000000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 52.02977 1.17445 2.257268
BI2230 UG/LITER 50.53694 1.27752 2.527895
MO2020 UG/LITER 51.15724 -41038 .8022029
TI3349 UG/LITER 52.72544 2.51954 4.778609
B_2496 UG/LITER 56.14376 .98186 1.748833
Y_3710 PPM 1228.667 1.714 .1394982
#1 ft2 #3
53.19656 52.04498 50.84779
51.64036 49.13734 50.83311
50.72681 51.20080 51.54411
54.35471 49.82341 53.99820
57.26030 55.75593 55.41506
1226.733 1229.267 1230.000
ERRORS VALUE RANGE
NOCHECK
QC PASS 50.00000 15.00000
NOCHECK
NOCHECK
QC PASS 50.00000 15.00000
NOCHECK
146
149 ANALYSIS REPORT
QC STANDARD
08/08/10 02:03:25 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSA RUN TIME: 08/08/10 13:56:28 COMMENT: ICSA MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0324389 .1641488 506.0246
AL3082 UG/LITER 255151.8 1050.8 .4118438
BA4934 UG/LITER 2.601125 .026397 1.014830
BE3130 UG/LITER .7981265 .0070270 .8804382
CA3179 UG/LITER 253800.0 913.2 .3598050
CD2265 UG/LITER 1.755873 .169087 9.629773
C02286 UG/LITER 5.385567 .282011 5.236417
#1 #2 ft3
-.045926 .2210839 -.077841
255721.2 263939.1 255795.0
2.631507 2.583812 2.588056
.7904577 .7996650 -8042567
254087.6 252777.6 254534.7
1.898966 1.569289 1.799364
5.073380 5.621876 5.461444
ERRORS VALUE RANGE
QC PASS .OOOOOOO 20.00000
QC PASS 243900.0 49997.06
QC PASS 2.000000 400.0000
QC PASS .OOOOOOO 10.00000
QC PASS 234100.0 47990.00
QC PASS .OOOOOOO 10.00000
QC PASS 3.000000 100.0000
ELEM UNITS AVGE SDEV %RSD
.CR2677 UG/LITER 46.29227 .51009 1.101887
CU3247 UG/LITER 24.39382 .11286 .4626516
FE2714 UG/LITER 101147-8 374.9 .3706116
K_7664 UG/LITER 2.178739 2.324091 106.6713
MG2790 UG/LITER 264967.7 970.8 .3663826
MN2676 UG/LITER 18.08131 .08886 .4914451
NA3302 UG/LITER 984.9497 71.8450 7.294277
ftl ft2 #3
46.86385 45.88332 46.12966
24.28299 24.38986 24.60860
101126.6 100783.9 101532.7
4.436622 -.206336 2.305933
266289.2 263864.6 265719.3
18.09398 17.98679 18.16315
1038.877 903.3914 1012.680
ERRORS VALUE RANGE
QC PASS 36.00000 20.00000
QC PASS 15.00000 50.00000
QC PASS 94900.00 19454.00
QC PASS .OOOOOOO 2000.000
QC PASS 248800.0 51003.00
QC PASS 19.00000 30.00000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 20.10426 .66011 3.283441
TL1908 UG/LITER -1.36378 3.22363 236.3738
V_2924 UG/LITER 1.111894 .094091 8.462211
ZN2138 UG/LITER 28.53914 .02372 .0831269
PB2203 UG/LITER 12.57465 1.11564 8.872101
SE1960 UG/LITER -4.53916 1.96427 43.27388
SB2068 UG/LITER 4.029755 2.112441 52.42107
ftl ft2 ft3
19.36394 20.36320 20.59565
2.260387 -3.91127 -2.44047
1.003426 1.171519 1.160737
28.56217 28.54046 28.51478
12.16206 11.73205 13.83985
-2.27111 -5.65543 -5.69093
4.328672 1.783778 6.976816
ERRORS VALUE RANGE
QC PASS 10.00000 80.00000
QC PASS .OOOOOOO 50.00000
QC PASS 1.000000 100.0000
QC PASS 39.00000 120.0000
QC PASS 5.000000 20.00000
QC PASS .OOOOOOO 70.00000
QC PASS .OOOOOOO 120.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .1678847 1.802864 1073.870
22031 UG/LITER -3.11786 1.12164 36.97149
22032 UG/LITER 20.39396 1.11763 5.480217
20681 UG/LITER 5.564492 2.229716 40.07043
20682 UG/LITER 3.253192 2.982257 91.67172
19601 UG/LITER -10.6539 5.1396 48.24160
19602 UG/LITER -1.49674 1.26670 84.63081
ftl tf2 »3
-1.66294 1.941420 .2261764
-3.42095 -4.06671 -1.87592
19.91252 19.59773 21.67163
3.264921 5.711475 7.717080
4.849359 -.187437 5.097663
-5.31610 -11.0763 -16.5692
-.761290 -2.95939 -.769533
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 20.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -4.71341 3.24049 68.75031
BI2230 UG/LITER 5.354517 2.055669 38.38943
MO2020 UG/LITER .9642445 .6454307 66.93642
TI3349 UG/LITER 4.443346 3.460224 77.87429
B_2496 UG/LITER -1.16560 .18305 15.70548
Y_3710 PPM 1186.178 4.623 .3897223
#1 ft2 »3
-1.85349 -4.05379 -8.23297
3.664289 4.914949 7.594313
1-664966 .8337121 .3940667
.4857254 5-946674 6.897636
--954159 -1.27397 -1.26837
1181.067 1190.067 1187.400
ERRORS VALUE RANGE
NOCHECK
NOCHECK
NOCHECK
NOCHECK
QC PASS .OOOOOOO 200.0000
NOCHECK
147
150 ANALYSIS REPORT
QC STANDARD
08/08/10 02:10:25 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSAB RUN TIME: 08/08/10 14:03:29 COMMENT: ICSAB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 206.6857 1.1966 .5789652
AL3082 UG/LITER 255070.0 1731.0 .6786326
BA4934 UG/LITER 522.5136 3.4621 .6625919
BE3130 UG/LITER 502.9909 3.6069 .7170820
CA3179 UG/LITER 254753.8 1541.9 .6052340
CD2265 UG/LITER 1008.491 5.634 .5686293
C02286 UG/LITER 513.1155 3.3457 .6520412
#1 ft2 ft3
205.3053 207.3223 207.4295
253423.6 254911.8 266874.7
519.2686 522.1140 626.1681
499.5668 502.6496 506.7563
253094.6 255024.1 256142.5
1002.981 1008.262 1014.241
510.1663 512.4290 516.7512
ERRORS VALUE RANGE
QC PASS 210.0000 43.00000
QC PASS 248400.0 50922.00
QC PASS 476.0000 400.0000
QC PASS 482.0000 98.00001
QC PASS 234300.0 48031.00
QC PASS 916.0000 187.0000
QC PASS 455.0000 100.0000
ELEM UNITS AVGE SDEV %RSD
CR2 677 UG/LITER 649.8411 3.3263 .6049520
CU3247 UG/LITER 541.5087 2.0443 .3775264
FE2714 UG/LITER 101206.5 626.6 .6191028
K_7664 UG/LITER 3.186428 2.233343 70.10491
MG2790 UG/LITER 265449.0 1817.8 .6848104
MN2576 UG/LITER 526.5900 3.2748 .6230659
NA3302 UG/LITER 998.9289 76.9761 7.705759
#1 #2 #3
546.6281 549.6262 553.2701
539.1892 642.2884 643.0484
100613.3 101144.5 101861.8
5.661378 2.576533 1.320875
263733.8 265258.8 267364.5
622.5322 525.1924 529.0454
926.5148 1079.771 990.6007
ERRORS VALUE RANGE
QC PASS 506.0000 103.0000
QC PASS 537.0000 110.0000
QC PASS 95100.00 19495.00
QC PASS .OOOOOOO 2000.000
QC PASS 254100.0 52090.00
QC PASS 483.0000 99.00000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1049.410 7.012 .6681457
TL1908 UG/LITER 98.32082 .86468 .8793412
V_2924 UG/LITER 517.1361 3.1523 .6095740
ZN2138 UG/LITER 1045.431 7.133 .6823258
PB2203 UG/LITER 63.79988 1.06428 1.652481
SE1960 UG/LITER 49.48990 2.37941 4.807863
SB2068 UG/LITER 627.7229 5.8188 .9269727
ftl #2 #3
1043.579 1047.461 1057.190
99.24043 97.52451 98.19752
514.3487 516.5024 520.6671
1038.584 1044.889 1052.819
63.00189 64.99506 63.40268
46.83712 51.43568 60.19691
623.1357 625.7647 634.2682
ERRORS VALUE RANGE
QC PASS 930.0000 190.0000
QC PASS 96.00000 60.00000
QC PASS 481.0000 99.99999
QC PASS 975.0000 199.0000
QC PASS 61.00000 20.00000
QC PASS 51.00000 70.00000
QC PASS 685.0000 120.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 101.4791 1.7478 1.722277
22031 UG/LITER 47.69554 2.94184 6.167961
22032 UG/LITER 71.82738 .79510 1.106960
20681 UG/LITER 627.7644 6.6082 1.052649
20682 UG/LITER 627.6959 5.4389 .8664894
19601 UG/LITER 42.88360 4.37496 10.20195
19602 UG/LITER 52.77766 3.09138 5.857357
ftl ft2 #3
103.2500 101.4317 99.75548
44.48466 50.26126 48.34070
72.23060 72.34008 70.91145
622.1614 626.0801 635.0517
623-6159 625-6010 633.8707
39.26687 41.63751 47.74643
60.60617 56.31699 51.40982
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
97.00000 20.00000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER 1012.336 6.825 .6741472
BI2230 UG/LITER 1033.304 7.681 .7433418
MO2020 UG/LITER 1005.448 7.031 .6992741
TI3349 UG/LITER 1018.751 6.433 .6314637
B_24 96 UG/LITER 1021.926 6.275 .6139969
Y_3710 PPM 1177.533 5.195 .4411999
#1 ft2 #3
1012.741 1005.318 1018.949
1027.307 1030.643 1041.961
999.3849 1003.804 1013.155
1012.895 1017.722 1025.637
1015.993 1021.291 1028.494
1181.267 1179.733 1171.600
ERRORS VALUE RANGE
QC PASS 1000.000 205.0000
QC PASS 1000.000 205.0000
QC PASS 1000.000 205.0000
QC PASS 1000.000 205.0000
QC PASS 1000.000 200.0000
NOCHECK
148
151 ANALYSIS REPORT
QC STANDARD
08/08/10 02:17:27 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCV RUNTIME: 08/08/10 14:10:30 COMMENT: CCV CVSl MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 102.5570 .4145 .4041556
AL3082 UG/LITER 50834.94 23.70 .0466252
BA4934 UG/LITER 1019.177 1.043 .1023110
BE3130 UG/LITER 1023.796 .983 .0960141
CA3179 UG/LITER 50042.84 172.37 .3444388
CD2266 UG/LITER 1007.210 .739 .0734170
C02286 UG/LITER 1007.468 .979 .0971260
ftl #2 ft3
102.9842 102.5304 102.1565
50859.87 50812.69 50832.26
1020.368 1018.731 1018.430
1024.535 1024.174 1022.681
60152.29 50132.08 49844.15
1008.048 1006.648 1006.934
1008.596 1006.965 1006.843
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1015.403 .854 .0840586
CU3247 UG/LITER 1020.210 1.293 .1266945
FE2714 UG/LITER 25310.34 15.78 .0623558
K_7664 UG/LITER 48792.02 73.50 .1506466
MG2790 UG/LITER 50923.36 22.79 .0447597
MN2576 UG/LITER 1002.374 .589 .0587487
NA3302 UG/LITER 51497.68 47.62 .0924663
ftl ft2 ft3
1016.388 1014.910 1014.910
1021.192 1020.693 1018.746
25326.61 25294.97 25309.55
48874.27 48769.07 48732.74
50949.38 60913.75 60906.94
1002.832 1002.580 1001.710
51457.66 51650.34 51485.03
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1013.340 .761 .0751210
TL1908 UG/LITER 1015.992 3.696 .3638009
V_2924 UG/LITER 1026.212 .739 .0720412
ZN2138 UG/LITER 1094.102 .650 .0594276
PB2203 UG/LITER 1006.570 1.026 .1019057
SE1960 UG/LITER 1015.345 3.291 .3241554
SB2068 UG/LITER 1035.030 -509 .0492192
#1 ft2 #3
1014.143 1013.249 1012.629
1014.993 1020.085 1012.898
1026.880 1026.338 1025.418
1093.477 1094.774 1094.054
1005.954 1006.002 1007.754
1013.975 1019.101 1012.961
1034.461 1035.407 1035.233
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
ASI890 UG/LITER 1022.731 .401 .0392171
22031 UG/LITER 1006.724 2.497 .2483134
22032 UG/LITER 1006.977 1.102 .1094167
20681 UG/LITER 1035.501 .763 .0736403
20682 UG/LITER 1034.792 .390 .0377093
19601 UG/LITER 1006.792 4.560 .4529226
19602 UG/LITER 1019.606 2.775 .2721848
#1 ft2 ft3
1022.799 1022.300 1023.093
1006.412 1002.966 1007.805
1005.711 1007.608 1007.714
1034.662 1036.152 1035.688
1034.342 1035.032 1035.003
1006.109 1011.655 1002.612
1017.892 1022.808 1018.117
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
SNI 899 UG/LITER 1017.417 1.025 .1007177
BI2230 UG/LITER 1015.114 2.611 .2572328
MO2020 UG/LITER 1030.777 .628 .0609539
TI3349 UG/LITER 1027.144 1.425 .1387693
B_2496 UG/LITER 1025.891 1.667 .1625296
Y_3710 PPM 1210.733 .400 .0330399
ftl »2 #3
1018.021 1017.997 1016.234
1016.033 1017.141 1012.167
1030.940 1031.308 1030.083
1028.457 1027.346 1025.628
1027.797 1024.701 1025.174
1210.733 1211.133 1210.333
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
149
152 ANALYSIS REPORT
QC STANDARD
08/08/10 02:24:29 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCB RUN TIME: 08/08/10 14:17:31 COMMENT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0814532 .1611146 197.8001
AL3082 UG/LITER 2.688588 2.173564 80.84405
BA4934 UG/LITER -.306220 .028446 9.289318
BE3130 UG/LITER .1253025 .0399326 31.86894
CA3179 UG/LITER -317.658 557.556 175.5209
CD2265 UG/LITER .3514129 .1271690 36.18791
C02286 UG/LITER .4219994 .2755316 65.29192
#1 #2 #3
.0087383 -.030487 .2661088
5.024078 2.316768 .7249193
-.332035 -.310900 -.275724
.1660879 .1235382 .0862813
-639.257 -639.869 326.1622
.4382006 .4106002 .2054380
.3501312 .7263435 .1895237
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 6.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .0622102 .3166236 508.9578
CU3247 UG/LITER .3760203 .0247185 6.573713
FE2714 UG/LITER 10.62173 3.73625 35.17550
K_7664 UG/LITER 5.024908 2.737589 64.48038
MG2790 UG/LITER 24.94363 1.67640 6.319867
MN2576 UG/LITER -.186070 .033222 17.86482
NA3302 UG/LITER -45.6349 104.8720 229.8064
ftl #2 #3
-.120458 -.120727 .4278156
.3681042 .3562295 .4037271
6.617945 11.23192 14.01532
7.360200 5.702310 2.012214
24.78466 26.59349 23.45273
-.205644 -.204855 -.147711
-99.7233 -112.420 75.23872
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 6000.000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -1.74971 .30123 17.21572
TL1908 UG/LITER -.836573 3.388996 405.1043
V_2924 UG/LITER .2644512 .4638676 171.6263
ZN2138 UG/LITER -.075328 .064049 86.02718
PB2203 UG/LITER .5789543 .4914724 84.88967
SE1960 UG/LITER -.648163 2.713457 418.6443
SB2068 UG/LITER 1.194766 .832701 69.69576
#1 ft2 #3
-1.47852 -1.69668 -2.07393
2.908738 -1.72700 -3.69146
.2604829 .7202898 -.187419
-.132808 -.006285 -.086392
.7762966 .0194826 .9410838
2.389402 -1.50151 -2.83236
1.919998 1.378887 .2854139
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
ASI890 UG/LITER .3213136 .3992475 124.2548
22031 UG/LITER -1.36260 .94628 69.44699
22032 UG/LITER 1.638425 .397585 25.84361
20681 UG/LITER 2..872486 1.533574 53.38840
20682 UG/LITER .3473131 .9853392 283.7034
19601 UG/LITER -2.35237 7.39028 314.1635
19602 UG/LITER .1928244 .6972802 361.6140
#1 #2 #3
.7392812 -.056122 .2807811
-.531729 -2.39260 -1.16347
1.419502 1.213873 1.981900
2.775031 4.452463 1.389963
1.483296 -.165442 -.275914
6.610726 -3.41250 -9.15532
.8212532 -.557289 .3145087
EMtORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1.139110 2.190201 192.2729
BI2230 UG/LITER .6837156 2.870414 419.8257
MO2020 UG/LITER 2.650677 1.456347 54.94245
TI3349 UG/LITER 4.355495 .694978 15.95635
B_2496 UG/LITER 2.302539 .903758 39.25049
Y_3710 PPM 1240.378 3.441 .2774260
#1 #2 #3
-1.23134 1.560989 3.087683
-2.38379 3.304712 1.130220
4.285620 1.492372 2.174038
4.552848 3.683184 4.930453
3.222845 2.268480 1.416292
1243.333 1241.200 1236.600
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
150
153 ANALYSIS REPORT
08/08/10 02:31:29 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 0072821-DUPl RUN TIME: 08/08/10 14:24:32 COMMENT: SDG:MY71S3 CLIENTID:MY71T5D 1:1 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.060669 .390339 643.3947
AL3082 UG/LITER 24227.57 167.90 .6930011
BA4934 UG/LITER 40.99372 .23250 .5671628
BE3130 UG/LITER 1.305125 .020941 1.604517
CA3179 UG/LITER 119065.3 356.3 .2992870
CD2265 UG/LITER 1.673800 .143156 8.552748
C02286 UG/LITER 121.4724 .6001 .4939826
ftl ft2 ft3
-.510769 .1849187 .1438443
24418.77 24104.16 24159.79
41.25871 40.82389 40.89858
1.327233 1.285589 1.302552
119462.9 118958.7 118774.5
1.761291 1.608696 1.751516
122.1558 121.2298 121.0316
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 13.93926 .13468 .9662116
CU3247 UG/LITER 23.06202 1.01345 4.396371
FE2714 UG/LITER 44469.74 268.33 .6034025
K_7664 MG2790 UG/LITER UG/LITER 11193.95 H317531.1 97.97 2117.4 .8752358 .6668458
MN2576 UG/LITER 2448.270 16.175 .6198241
NA3302 UG/LITER 124999.5 603.5 .4828081
ftl ft2 »3
13.87431 13.84936 14.09411
24.18799 22.72745 22.24061
44773.48 44264.89 44370.84
11306.95 H319938.0 11142.19 H315955.2 11132.71 H316700.2
2465.573 2437.223 2442.014
125695.1 124616.0 124687.3
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC HIGH 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 352.2913 2.6214 .7440956
TL1908 UG/LITER -3.58269 3.49251 97.48303
V_2924 UG/LITER 2.623682 .193824 7.387751
ZN2138 UG/LITER 1182.971 6.972 .5893405
PB2203 UG/LITER 3.086566 .288422 9.347469
SE1960 UG/LITER 3.391263 1.141269 33.65322
SB2068 UG/LITER 2.849146 1.697079 59.56448
#1 ft2 ft3
355.1224 349.9483 351.8031
-.514299 -7.38324 -2.85052
2.462644 2.838742 2.569358
1190.943 1178.013 1179.958
3.296294 3.203546 2.756867
4.034879 2.073556 4.066363
1.451247 2.358773 4.737417
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -6.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.516935 1.117659 216.2088
22031 UG/LITER 2.270201 1.569569 69.13786
22032 UG/LITER 3.480964 .566057 15.97424
20681 UG/LITER 4.659781 1.504381 32.28438
20682 UG/LITER 1.935475 1.911838 98.77874
19601 UG/LITER 2.076443 .776075 37.37519
19602 UG/LITER 4.037970 1.372050 33.97871
#1 ft2 ft3
-.254550 -1.74244 .4461880
4.067621 1.672755 1.170228
2.898569 4.006280 3.538044
4.129719 3.492177 6.357445
.1043228 1.783210 3.918893
2.809451 1.263490 2.156390
4.636971 2.468265 5.008673
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 6.158400 2.014958 39.06168
BI2230 UG/LITER .5603284 1.634274 273.8170
MO2020 UG/LITER 1.121088 .856905 76.43514
TI3349 UG/LITER 9.538545 1.671001 17.51841
B_2496 UG/LITER 3599.215 22.210 .6170894
Y_3710 PPM 1260.778 1.734 .1375154
ftl #2 ft3
6.939664 2.971474 5.564064
-1.03510 2.025095 .6909881
1.333220 1.852003 .1780415
11.45649 8.396919 8.762226
3624.337 3582.188 3691.119
1262.533 1260.733 1259.066
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
151
154 08/08/10 02:38:29 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0072821-MSl RUN TIME: 08/08/10 14:31:32 COMMENT: SDG:MY71S3 CLIENTID:MY71T5S MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR; 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 50.89898 .23653 .4646969
AL3082 UG/LITER 26061.31 32.77 .1267252
BA4934 UG/LITER 1968.823 3.434 .1744370
BE3130 UG/LITER 47.69728 .01750 .0366974
CA3179 UG/LITER 118644.4 355.4 .2995430
CD2265 UG/LITER 47.95016 .12724 .2653502
C02286 UG/LITER 591.7415 .4817 .0813991
ftl #2 #3
50.64780 51.11745 50.93167
26090.97 26066.81 26026.14
1972.320 1968.695 1965.455
47.71281 47.67831 47.70071
119000.1 118643.9 118289.3
47.80732 47.99182 48.06134
591.2636 592.2268 591.7340
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200-000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 201.8150 .6820 .3379512
CU3247 UG/LITER 273.5646 .1219 .0445495
FE2714 UG/LITER 46071.70 46.91 .1040873
MG2790 K_7664 UG/LITER UG/LITER 11178.87 H315839.4 175.2 8.66 .0775012 .0554790
MN2576 UG/LITER 2896.494 1.176 .0406202
NA3302 UG/LITER 124186.4 612.4 .4931392
#1 ft2 ft3
201.0813 202.4298 201.9340
273.6675 273.4300 273.5963
45018.22 45105.91 45090.96
11182.25 H315918.0 11185.34 H315961-6 11169.03 H315638.6
2895.881 2896.427 2894.173
124750.9 124273.1 123535.3
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC HIGH 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 816.6664 1.1688 .1431232
TL1908 UG/LITER 45.32532 2.33008 5.140793
V_2924 UG/LITER 480.2351 .2557 .0532543
ZN2138 UG/LITER 1655.094 2.584 .1560945
PB2203 UG/LITER 21.60291 .65525 2.570235
SE1960 UG/LITER 50.85887 .82512 1.622374
SB2068 UG/LITER 100.0577 .6885 .6880808
#1 ft2 #3
815.9407 816.0437 818.0147
45.95911 42.74392 47.27294
479.9398 480.3804 480.3850
1656.362 1666.290 1662.129
21.29682 21.26808 22.24384
51.29152 51.37768 49.90740
99.89706 99.46380 100.8123
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 39.06238 .35852 .9178101
22031 UG/LITER 21.25034 1.86106 8.757793
22032 UG/LITER 21.76603 .96468 4.432057
20681 UG/LITER 102.4055 3.3217 3.243683
20682 UG/LITER 98.87592 1.51445 1.531671
19601 UG/LITER 46.16902 .69224 1.532884
19602 UG/LITER 63.69464 1.02327 1.905729
#1 ft2 ft3
38.80994 38.90446 39.47275
22.56384 19.12064 22.06654
20.65213 22.32809 22.31788
98.69611 103.4153 106.1052
100.4869 97.48132 98.65949
44.90960 45.94139 44.62605
54.46779 54.08187 52.53426
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 4.237112 1.385181 32.69164
BI2230 UG/LITER .5226236 2.060859 394.3294
MO2020 UG/LITER 1.039207 .385456 37.09139
TI3349 UG/LITER 7.361204 2.013123 27.34774
B_2496 UG/LITER 3589.635 3-196 .0890477
Y_3710 PPM 1264.378 3.633 .2873628
#1 #2 ft3
2.643861 5-155768 4.911706
1.040161 2.275393 -1.74767
.7555823 1.478079 .8839598
5.036926 8.492268 8.554417
3585.950 3591.666 3591.287
1260.733 1264.400 1268.000
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
152
155 ANALYSIS REPORT
08/08/10 02:45:29 PM
METHOD: ALT-P3Q3 SAMPLE NAME: SDI1007157-07 RUN TIME: 08/08/10 14:38:32 COMMENT: SDG:MY71S3 CLIENTID:MY71T6L 1:5 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .1688744 .2949052 174.6299
AL3082 UG/LITER 4857.690 26.049 .5362460
BA4934 UG/LITER 7.994608 .016273 .2035499
BE3130 UG/LITER .1688793 .0261372 15.47683
CA3179 UG/LITER 24366.63 372.75 1.529773
CD2265 UG/LITER .5283195 .0376385 7.124184
C02286 UG/LITER 25.60230 .34139 1.333436
ftl
«2 ft3
.4542466 -.134719 .1870954
4869.419 4876.814 4827.839
8.012890 7.989226 7.981707
.1970348 .1642147 .1453886
24037.42 24771.31 24290.85
.4852966 .5445070 .5561561
26.94938 25.69060 25.26690
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 2.580454 .086296 3.344222
CU3247 UG/LITER 4.571614 .136941 2.995467
FE2714 UG/LITER 9206.721 56.177 .6101713
K_7664 UG/LITER 1842.380 10.531 .5715961
MG2790 UG/LITER 63302.57 257.30 .4064603
MN2576 UG/LITER 506.1620 2.2314 .4417175
NA3302 UG/LITER 26338.02 103.49 .4084276
#1 ft2 ft3
2.535171 2.679967 2.526226
4.619111 4.417248 4.678483
9214.348 9258.694 9147.120
1853.094 1842.004 1832.042
63369.99 63519.45 63018.27
505.9458 606.8958 602.6446
25220.59 25415.88 25377.60
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 70.94582 .51862 .7310066
TL1908 UG/LITER -.542041 2.021352 372.9146
V_2924 UG/LITER .7585550 .2607876 34.37962
ZN2138 UG/LITER 231.3694 1.1315 .4890641
PB2203 UG/LITER .2284240 .4831426 211.5113
SE1960 UG/LITER 3.280363 1.769293 63.93690
SB2068 UG/LITER .6461762 .6615462 102.3786
70.54977 71.53286 . 70.75486
-1.51018 -1.89723 1.781292
.7343854 1.030586 .6106936
231.5578 232.3949 230.1555
.4996566 .5150061 -.329391
1.247686 4.474373 4.119029
1.026625 1.029613 -.117710
ttl tt2 ft3
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -6.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.006870 1.281033 18647.27
22031 UG/LITER -.206226 1.822681 883.8279
22032 UG/LITER .4355526 .8056568 184.9505
20681 UG/LITER 2.378350 1.937848 81.46153
20682 UG/LITER -.228733 .800305 349.8867
19601 UG/LITER 1.930329 .984987 51.02691
19602 UG/LITER 3.944497 2.164313 54.86917
ftl
#2 #3
.6412308 .8206087 -1.48245
1.895191 -1.15592 -1.35795
-.206938 1.339315 .1742805
1.675266 4.570202 .8910325
.6929184 -.747930 -.631186
.8173990 2.689870 2.283719
1.462633 6.355386 5.025473
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER .7512976 1.285889 171.1558
BI2230 UG/LITER 1.226524 1.488962 121.3969
MO2020 UG/LITER .2330613 .4334533 185.9826
TI3349 UG/LITER 2.928842 .796421 27.19234
B_2496 UG/LITER 737.7173 3.5481 .4809518
Y_3710 PPM 1238.867 4.044 .3263986
ftl ft2 «3
.9178840 -.609766 1.945775
2.803491 1.031245 -.155163
.5865912 -.250533 .3631256
2.494328 3.848013 2.444183
739.6550 739.8746 733.6223
1238.633 1235.000 1243.066
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10-0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
153
156 08/08/10 02:52:29 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0072821-PSl RUN TIME: 08/08/10 14:45:32 COMMENT: SEX3:MY71S3 CLIENTID :MY71T5A MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.110928 .047092 42.45298
AL3082 UG/LITER -28.9433 3.4704 11.99044
BA4934 UG/LITER -.492360 .068932 14.00025
BE3130 UG/LITER -.149413 .037445 25.06134
CA3179 UG/LITER 119.8385 180.7498 150.8278
CD2265 UG/LITER .0780270 .2067186 264.9322
C02286 UG/LITER -.044935 .276797 615.9963
#1 ft2 ft3
-.066554 -.138603 -.137629
-32.0479 -29.5852 -25.1967
-.460342 -.571478 -.445260
-.174616 -.167236 -.106386
16.68878 328.5458 14.28096
-.039683 -.042954 .3167175
-.129310 -.269726 .2642309
ERRORS HIGH
LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.324159 .507569 156.6801
CU3247 UG/LITER 1.733651 .083120 4.794620
FE2714 UG/LITER -1.69484 6.28280 393.9463
K_7664 UG/LITER -1.25194 4.55830 364.0980
MG2790 UG/LITER 6.702821 1.505365 22.45867
MN2576 UG/LITER -.349302 .042484 12.16247
NA3302 UG/LITER 33.00618 32.19198 97.53320
#1 #2 ft3
-.356494 -.814788 .1988041
1.638656 1.769274 1.793023
-1.77103 -7.78768 4.774204
3.795111 -5.06913 -2.48181
7.767075 4.980465 7.360923
-.338684 -.396088 -.313134
2.953664 66.97864 29.08623
ERRORS HIGH
LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
Rf.F.M UNITS AVGE SDEV %RSD
NI2316 UG/LITER -2.26868 .70472 31.06309
TL1908 UG/LITER 1.394126 1.928670 138.3425
V_2924 UG/LITER -.208219 .259998 124.8678
ZN2133 UG/LITER -.209496 .039385 18.79980
PB2203 UG/LITER .1753375 .7056361 402.4444
SE1960 UG/LITER .8444404 1.182152 139.9924
SB2068 UG/LITER -.360419 -112881 31.31949
ftl #2 ft3
-1.74674 -3.07032 -1.98900
-.828924 2.390314 2.620990
-.006913 -.501474 -.117269
-.209584 -.248837 -.170068
.4683616 -.629599 .6872601
-.276719 2.079360 .7306805
-.477085 -.251747 -.352426
ERRORS HIGH
LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10-0000
LC PASS 50000.00 -60.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.966403 .709651 73.43214
22031 UG/LITER 1.361777 1.076048 79.52853
22032 UG/LITER -.421939 1.641094 366.2411
20681 UG/LITER .6121535 1.128135 184.2895
20682 UG/LITER -.855916 .563689 64.67793
19601 UG/LITER .7778143 2.597412 333.9373
19602 UG/LITER .8677648 2.423134 279.2385
ftl ft2 ft3
-.738629 -1.76197 -.398606
1.577571 2.295994 .1817650
-.096407 -2.10013 .9297218
-.197052 .1326875 1.900826
-.626874 -.463605 -1.48727
3.005543 1.403050 -2.07515
-1.92537 2.407079 2.121585
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.189182 3.105048 1641.300
BI2230 UG/LITER 1.648147 1.902865 115.4648
MO2020 UG/LITER -.325229 .442439 136.0391
TI3349 UG/LITER .2268350 3.018628 1330.769
B_2496 UG/LITER 3.244755 .899466 27.72061
Y_3710 PPM 1229.733 4.521 .3676427
ftl ft2 ft3
2.986990 -3.21900 -.334537
3.135403 -.496177 2.305215
-.576617 .1856330 --584804
.5148466 -2.92548 3.091135
4.278912 2.644439 2.810913
1224-733 1230.933 1233.533
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30-0000
LC PASS 40000.00 -50.0000
NOCHECK
154
157 08/08/10 02:59:29 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-01 RUN TIME: 08/08/10 14:52:32 COMMENT: SDG:MY71S3 CLIENTID:MY71S3 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.067330 .142149 211.1246
AL3082 UG/LITER -9.10466 6.09399 55.94991
BA4934 UG/LITER 30.82127 .06759 .2192994
BE3130 UG/LITER -.050641 .039144 77.29635
CA3179 UG/LITER 1318.246 328.005 24.88192
CD2265 UG/LITER -.007142 .193747 2712.813
C02286 UG/LITER .2344988 .1815575 77.42364
ftl ft2 ft3
-.225956 -.024550 .0485171
-4.12840 -8.87656 -14.3087
30.86087 30.74322 30.85971
-.006706 -.068880 -.077337
1312.764 1648.957 993.0158
-.069349 -.162145 .2100686
.0701360 .2039780 .4293823
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 26.71762 .07261 .2714091
CU3247 UG/LITER 2.921083 .226548 7.755601
FE2714 UG/LITER 35.39916 3.26864 9.233676
K_7664 UG/LITER 207.2453 5.2828 2.549049
MG2790 UG/LITER 162346.2 494.2 .3244236
MN2576 UG/LITER -2.98432 .07274 2.437336
NA3302 UG/LITER 3312.225 50.889 1.536391
ftl ft2 ft3
26.77037 26.63485 26.74734
2.707346 2.897335 3.158570
32.19545 35.27293 38.72908
212.5295 207.2424 201.9639
152826.4 151838.8 152370.2
-3.03010 -2.90045 -3.02241
3282.374 3283.317 3370.983
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -16.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 11.75377 .32753 2.786631
TLI908 UG/LITER -2.41398 1.54886 64.16212
V_2924 UG/LITER -.003947 .110677 2803.901
ZN2138 UG/LITER .4920021 .0721466 14.66388
PB2203 UG/LITER .2585861 .3294264 127.3962
SE1960 UG/LITER -.839957 2.657654 316.4037
SB2068 UG/LITER -.169681 .953514 561.9453
ftl ft2 #3
11.61058 11.52221 12.12851
-1.08098 -4.11311 -2.04786
.0936216 -.124213 .0187499
.4530618 .5762521 .4476923
.0750427 .6388983 .0618174
1.933179 -1.08836 -3.36469
.5671616 .1704077 -1.24661
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1.42246 .61673 43.35643
22031 UG/LITER 1.048488 1.464082 138.6838
22032 UG/LITER -.145742 1.191376 817.4629
20681 UG/LITER 1.032377 2.321372 214.4699
20682 UG/LITER -.804741 1.802870 224.0310
19601 UG/LITER -6.43191 2.18727 34.00659
19602 UG/LITER 1.941867 3.154108 162.4274
ftl ft2 ff3
-1.30466 -2.08959 -.873128
2.409168 -.483773 1.220068
-1.10027 1.189447 -.626409
-.833848 3.663706 .4172733
1.256621 -1.58367 -2.08728
-3.94265 -8.04646 -7.30662
4.856691 2.375627 -1.40665
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1.470717 2.348626 159.6926
BI2230 UG/LITER .3294322 1.819806 552.4070
MO2020 UG/LITER .4653171 .4555235 97.89527
TI3349 UG/LITER .4188671 .7752571 185.0843
B_2496 UG/LITER 40.89025 .70808 1.731667
Y_3710 PPM 1226.689 3.067 .2502178
ttl «2 tt3
2.376164 -1.19586 3.231852
.9118673 -1.71029 1.786720
.1378914 .9866351 .2725249
1.216667 .3716202 -.331686
41.54903 40.14147 40.98026
1222.600 1228.733 1225.733
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00
NOCHECK
155
158 08/08/10 03:06:29 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-02 RUN TIME: 08/08/10 14:59:33 COMMENT: SDG:MY71S3 CLIENTID:MY71S5 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.021729 .132658 610.5170
AL3082 UG/LITER -21.2065 .7947 3.747302
BA4934 UG/LITER 44.37318 .06423 .1447590
BE3130 UG/LITER -.126909 .021651 17.06042
CA3179 UG/LITER 1671.112 4.279 .2660841
CD2265 UG/LITER .0985724 .0521155 52.87027
C02286 UG/LITER .3506507 .2565439 73.16223
ftl *2 #3
.1122494 -.153026 -.024410
-21.2461 -21.9807 -20.3928
44.39042 44.42704 44.30209
-.103115 -.145450 -.132163
1676.032 1668.254 1669.049
.1092845 .0419332 .1444996
.0610310 .5493594 .4415617
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 11.36325 .35283 3.105044
CU3247 UG/LITER 5.295948 .196196 3.704642
FE2714 UG/LITER -33.3372 7.1780 21.53164
K_7664 UG/LITER 457.7273 8.9230 1.949418
MG2790 UG/LITER 170306.2 80.8 .0474693
MN2576 UG/LITER 10.46815 .02982 .2848687
NA3302 UG/LITER 4651.151 140.852 3.028333
ftl «2 #3
10.95583 11.66541 11.56850
5.105958 5.497811 5.284073
-38.8154 -35.9847 -25.2114
463.4439 447.4453 462.2927
170396-5 170240-7 170281.4
10.46810 10.43835 10.49799
4748.969 4489.711 4714.772
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 8.617510 .214058 2.483986
TL1908 UG/LITER -.340231 1.430424 420.4271
V_2924 UG/LITER -.073524 .253174 351.1438
ZN2138 UG/LITER 1.186461 .063823 5.379255
PB2203 UG/LITER .5937588 .6443861 108.5266
SE1960 UG/LITER .6672572 .9837892 147.4378
SB2068 UG/LITER .8645973 1.333843 156.0786
ftl #2 #3
8.391962 8.817844 8.642722
.9772700 -1.86168 -.136280
-.333972 .1823160 -.068915
1.133533 1.168515 1.257336
.6137102 1.227937 -.060371
.4178383 -.167817 1.751750
-.517392 .9344794 2.146704
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1B90 UG/LITER -.939474 .113897 12.12353
22031 UG/LITER 2.004436 1.334227 66.56374
22032 UG/LITER -.120997 .996037 823.1892
20681 UG/LITER 1.366372 .839120 44.95996
20682 UG/LITER .3398317 2.411416 709.5912
19601 UG/LITER -2.19471 3.94823 179.8978
19602 UG/LITER 2.086039 1.218355 58.40520
#1 #2 #3
-.867418 -1.07078 -.880219
.5468156 3.165299 2.301192
.6357666 .2606680 -1.24943
2.301406 1.618871 1.178840
-2.18438 .5840111 2.619868
-6.72631 -2.92578 2.067966
3.475224 1.199058 1.583836
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER 1.309877 1.291203 98.57436
BI2230 UG/LITER -.832757 1.738102 208.7165
MO2020 UG/LITER .3201122 .2722447 85.04666
TI3349 UG/LITER .8666992 3.123109 360.3452
B_2496 UG/LITER 200.6379 .5050 .2516948
Y_3710 PPM 1215.533 2.609 .2146023
ftl #2 ft3
2.261634 -.159895 1.827893
.9041670 -2.67203 -.830405
.1112827 .6280211 .2210327
-2.18396 .7265205 4.067537
201.2077 200.2457 200.4605
1212.533 1217.267 1216.800
ERRORS HIGH LOW
IC PAS.'; 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
156
159 08/08/10 03:13:29 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-03 RUN TIME: 08/08/10 15:06:32 COMMENT: SDG:MY71S3 CLIENTID:MY71S7 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0053176 .1047284 1969.455
AL3082 UG/LITER 11.84955 5.49822 46.40025
BA4934 UG/LITER 64.90073 .22445 .3458404
BE3130 UG/LITER .0014671 .0433448 2954.380
CA3179 UG/LITER 12377.35 475.93 3.845148
CD2265 UG/LITER .0855193 .0754612 88.23878
C02286 UG/LITER .0247467 .1086810 439.1734
ttl #2 #3
-.101803 .0102796 -1074768
16.60738 13.11107 5.830205
64.95290 65.09451 64.65479
.0513816 -.020299 -.026681
12324.96 11929.80 12877.31
-.001482 .1248355 .1332040
-.096934 .1121744 .0589998
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 15.09539 .23561 1-660810
CU3247 UG/LITER 18.00939 .07726 .4290027
FE2714 UG/LITER -32.0950 10.3028 32.10084
K_7 664 UG/LITER 920.0459 4.8951 .5320531
MG2790 UG/LITER 175156.2 482.7 .2755545
MN2576 UG/LITER -3.02612 .03934 1.300099
NA3302 UG/LITER 13506.25 63.30 .4686561
ftl tt2 ft3
16.35849 15.02382 14.90386
17.93023 18.01335 18.08460
-43.2261 -22.8933 -30.1656
925.6990 917.1705 917.2711
175205.8 175612.1 174650.7
-3.06444 -3.02811 -2.98583
13520.53 13437.03 13661.19
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1.775112 .221625 12.48511
TLI 908 UG/LITER -3.00411 1.69450 56.40620
V_2924 UG/LITER 1.035529 .207716 20.05891
ZN2138 UG/LITER .7819176 .0752732 9.626738
PB2203 UG/LITER .6409730 .8339596 130.1084
SE1960 UG/LITER 1.632030 .354703 21.73383
SB2068 UG/LITER 1.229903 .566392 46.05174
ttl ft2 ft3
1.995741 1.777090 1.552505
-3.32420 -4.51573 -1.17239
1.268099 .8684570 .9700318
.7443718 .8685785 .7328026
.5264975 1.526257 -.129835
1.222519 1.843079 1.830491
1.704754 .6030072 1.381948
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
ASI890 UG/LITER -.395440 .612636 154.9254
22031 UG/LITER 2.127683 .251724 11.83088
22032 UG/LITER -.111665 1.334818 1195.377
20681 UG/LITER 1.374895 1.747S93 127.1147
20682 UG/LITER 1.147534 .879677 76.65809
19601 UG/LITER -1.95806 1.05889 54.07864
19602 UG/LITER 3.414400 1.023745 29.98314
ftl tt2 «3
.1106827 -.220478 -1.07652
2.369289 1.866935 2.146823
-.403540 1.344939 -1.27639
.8566366 -.055054 3.323103
2.118154 .9215585 .4028886
-.891086 -1.97441 -3.00868
2.267714 3.738976 4.236512
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM LINITS AVGE SDEV %RSD
SN1899 UG/LITER 2.375642 2.711442 114.1399
BI2230 UG/LITER .9476132 1.743637 184.0030
MO2020 UG/LITER 1.217902 .714169 68.63926
TI3349 UG/LITER 1.929922 1.897829 98.33709
B_2496 UG/LITER 405.7402 1.1587 .2855731
Y_3710 PPM 1224.822 5.284 .4313813
ftl ft2 ft3
4.733923 -.587029 2.979731
-.948310 2.482410 1.308740
.3968427 1.561850 1.695013
1.132259 .5611114 4.096394
405.8388 406.8464 404.5353
1219.800 1224.333 1230.333
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
157
160 ANALYSIS REPORT
08/08/10 03:20:29 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-04 RUN TIME: 08/08/10 15:13:32 COMMENT: SDG:MY71S3 CLIENTID:MY71S9 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .2496824 .0648299 25.96497
AL3082 UG/LITER 134843.2 58.9 .0436457
BA4934 UG/LITER 13.64865 .06509 .4768979
BE3130 UG/LITER 6.571985 .014955 .2275639
CA3179 UG/LITER 230863.5 731.0 .3166467
CD2265 UG/LITER 11.44814 .12341 1.077966
C02286 UG/LITER 599.6192 .1048 .0174699
#1 *2 ft3
.1943906 .3210322 .2336245
134888.2 134864.8 134776.6
13.71294 13.58279 13.65023
6.588628 6.567667 6.559672
231420.1 231134.7 230035.6
11.41473 11.58481 11.34487
599.7009 599.6555 699.5011
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 75.14617 .38715 .5161928
CU3247 UG/LITER 5.921329 .098873 1.669784
FE2714 UG/LITER 501659.2 363.3 .0724129
K_7 664 UG/LITER 45962.87 56.82 .1236200
MG2790 UG/LITER 272287.5 55.4 .0203521
MN2676 UG/LITER 7787.054 1.013 .0130087
NA3302 UG/LITER 299386.8 28.1 .0093813
ftl ft2 ft3
74-98717 74.86384 75.58750
5.889665 5.842167 6.032156
601283.3 501685.8 502008.4
46025.33 45949.04 45914.24
272292.9 272340.0 272229.6
7788.220 7786.395 7786.545
299356.4 299392.4 299411.8
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
TL1908 NI2316 UG/LITER UG/LITER 1390.044 L-11.3342 3.3446 1.863 .1333181 29.50802
V_2924 UG/LITER 375.7377 .5161 .1373659
ZN2138 UG/LITER 2235.690 .945 .0422871
PB2203 SE1960 UG/LITER UG/LITER 33.31294 L-18.4514 1.1200 .75716 2.272857 6.070050
SB2068 UG/LITER 13.03851 .68753 5.273067
ftl ft2 ft3
1391.908 L-12.5744 1388.202 L-13.8816 1390.023 -7.54676
376.2333 375.2032 375.7767
2236.794 2236.580 2234.698
33.73516 L-19.0279 32.43882 L-19.1657 33.76485 L-17.1606
12.41366 12.92683 13.77506
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC LOW 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC LOW 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 46.06665 1.17627 2.553455
22031 UG/LITER 34.53688 1.47758 4.278260
22032 UG/LITER 32.68647 .40436 1.237072
20681 UG/LITER 22.42814 1.41851 6.324687
20682 UG/LITER 8.342981 .645970 6.544057
19601 UG/LITER -27.7320 1.1908 4.293992
19602 UG/LITER -13.8257 1.0863 7.857099
ftl #2 ft3
44.71952 46.89536 46.58210
35.47919 32.83395 35.29750
32.84903 32.22613 32.98425
21.81365 21.42057 24.06031
7.712999 8.678575 8.637371
-28.2706 -28.5586 -26.3671
-14.4213 -14.4840 -12.5719
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI 899 UG/LITER 1.909451 2-394747 125.4155
BI2230 UG/LITER 15-78153 1.47839 9.367876
MO2020 UG/LITER -2.78869 1.02001 36.57670
TI3349 UG/LITER 8.936405 1.965278 21.99182
B_2496 UG/LITER 9992.580 2.741 .0274314
Y_3710 PPM 1677.422 1.534 .0972351
ftl ft2 ft3
2.394148 -.690569 4.024774
14.10334 16.34964 16.89159
-1.95797 -3.92713 -2.48096
6.667146 10.05830 10.08377
9993-587 9994.675 9989.478
1575.867 1577.467 1578.933
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
158
161 08/08/10
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1 0 0 7 1 5 7 - 0 5 RUN TIME: 0 8 / 0 8 / 1 0 1 5 : 2 0 : 3 2 COMMENT: SDG:MY71S3 CLIENTID:MY7ITl MODE: CONC CORR. FACTOR: 1
0 3 : 2 7 : 2 9 PM
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.225249 .190159 84.42170
AL3082 UG/LITER 127994.9 178.4 .1394092
BA4934 UG/LITER 12.10782 .03669 .3030660
BE3130 UG/LITER 6.795706 .017058 .2510184
CA3179 UG/LITER 258730.9 346.6 .1339587
CD2265 UG/LITER 6.753583 .018009 .2666513
C02286 UG/LITER 600.9819 .3261 .0642587
#1 #2 #3
-.233352 -.411228 -.031168
128200.9 127895.6 127888.2
12.14945 12.09383 12.08018
6.815206 6.784058 5.787774
259094.2 258694.8 258403.8
6.772261 6.752159 6.736328
600.8994 600.7051 601.3414
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 36.31940 .33731 .9287423
CU3247 UG/LITER 6.807945 .100990 1.483411
FE2714 UG/LITER 324849.2 197.8 .0608887
K_7664 UG/LITER 46190.71 74.68 .1616693
MG2790 UG/LITER 295045.7 338.1 .1145939
MN2576 UG/LITER 8219.326 6.269 .0762771
NA3302 UG/LITER 321685.0 972.5 .3023225
#1 ft2 ft3
36.43353 36.58484 35.93982
6.922730 6.732741 6.768364
324655.2 324841.6 325050.6
46276.92 46149.43 46145.80
295430.7 294909.4 294797.1
8226-196 8213.914 8217.869
322798-5 321254.2 321002.3
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM LTNITS AVGE SDEV %RSD
NI2316 UG/LITER 1414.797 .905 .0639641
TL1908 UG/LITER -5.50511 2.70161 49.07453
V_2924 UG/LITER 16.30568 .07525 .4614996
ZN2138 UG/LITER 2226.958 4.206 .1889634
PB2203 SE1960 UG/LITER UG/LITER 20.97082 L-12.0109 .98940 .2600 4.718000 2.165092
SB2068 UG/LITER 9.792727 1.050602 10.72840
ftl ft2 ft3
1414.690 1414.014 1416.788
-8.56420 -3.44623 -4.50491
16.29629 16.23556 16.38518
2230.800 2223.206 2223.863
19.86189 L-11.7841 21.28736 L-11.9539 21.76322 L-12.2947
9.072844 9.307036 10.99830
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC LOW 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 3.024721 .813708 26.90192
22031 UG/LITER 17.59361 .76169 4.329372
22032 UG/LITER 22.64406 1.31306 5.798675
20681 UG/LITER 17.66952 2.27441 12.87192
20682 UG/LITER 5.852575 .468998 8.013525
19601 UG/LITER -22.7966 .7767 3.406975
19602 UG/LITER -6.63379 .41697 6.285479
ftl ft2 ft3
3.290391 2.111383 3.672390
16.94872 18.43400 17.39811
21.30437 22.69908 23.92875
16.38032 16.33261 20.29564
5.416889 5.791863 6.348971
-23.0407 -21.9272 -23.4219
-6.17189 -6.98241 -6.74709
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER 4.822724 1.515282 31.41963
BI2230 UG/LITER 10.61336 2.36651 22.29748
MO2020 UG/LITER -2.94248 .75978 25.32119
TI3349 UG/LITER 10.01764 2.39931 23.95081
B_2496 UG/LITER 11083.30 5.10 .0460369
Y_3710 PPM 1596.844 6.981 .4371546
ftl ft2 ft3
3.362565 6.387687 4.717920
13.34605 9.308815 9.186200
-3.50154 -3.24850 -2.07741
7.699383 9.863026 12.49052
11087.63 11084.58 11077.67
1589.333 1598.066 1603.133
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.OOOO
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
159
162 08/08/10 03:34:29 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-06 RUN TIME: 08/08/10 15:27:33 COMMENT: SDG:MY71S3 CLIENTID:MY71T3 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM imiTS AVGE SDEV %RSD
AG3280 UG/LITER .0934822 .0999153 106.8816
AL3082 UG/LITER 20747.62 35.58 .1714858
BA4934 UG/LITER 43.67685 .05180 .1186009
BE3130 UG/LITER 1.155647 .032943 2.850634
CA3179 UG/LITER 106107.9 566.1 .5335164
CD2265 UG/LITER .9779299 .1645729 16.82871
C02286 UG/LITER 116.0901 .4834 .4163982
ttl ft2 ft3
.1772277 .1203341 -.017115
20710.83 20750.16 20781.85
43.62041 43.72222 43.68793
1.192547 1.145201 1.129193
105454.3 106443.4 106425.9
1.033472 1.107546 .7927723
116.6321 115.7034 115.9350
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS lOOOO.OO -6.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 14.03839 .20655 1.471345
CU3247 UG/LITER 3.217941 .116949 3.634273
FE2714 UG/LITER 53161.82 45.29 .0852118
K_7664 UG/LITER 10308.60 8.01 .0777119
MG2790 UG/LITER 209644.7 278.3 .1327690
MN2676 UG/LITER 2532.907 2.205 .0870356
NA3302 UG/LITER 109883.9 206.0 .1874697
ftl #2 #3
14.22028 13.81383 14.08104
3.182318 3.348559 3.122947
53121.55 63130.02 53203.89
10299.35 10312.91 10313.53
209373.1 209631.6 209929.3
2531.240 2532.075 2536.407
109672.3 109895.6 110083.8
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 290.6255 .4356 .1498907
TL1908 UG/LITER -4.72268 2.09249 44.30818
V_2924 UG/LITER 2.885148 .095011 3.293095
ZN2138 UG/LITER 371.0147 .3818 .1029137
PB2203 UG/LITER 3.980978 .445727 11.19642
SE1960 UG/LITER -1.55776 2.58119 166.6983
SB2068 UG/LITER 3.105504 .202326 6.615070
ftl #2 ft3
290.7240 291.0034 290.1490
-2.47959 -6.62205 -5.06609
2.991512 2.855246 2.808686
370.7332 370.8056 371.4554
3.503194 4.054147 4.385594
-2.33683 -3.65968 1.323220
3.312294 2.907959 3.096261
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -6.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .9404730 .7481260 79.54773
22031 UG/LITER 4.634747 .140012 3.020912
22032 UG/LITER 3.639400 .733139 20.14450
20681 UG/LITER 5.353631 1.388207 25-93020
20682 UG/LITER 1.973432 .897497 45.47902
19601 UG/LITER -8.46959 1.52087 17.96689
19602 UG/LITER 1.883271 3.768392 199.5672
ftl #2 ft3
.2246998 1.717218 .8795012
4.796385 4.651076 4.556780
2.842351 3.790887 4.284962
5.187566 6.817400 4.055925
2.366345 .9464834 2.607465
-6.93666 -9.97812 -8.49399
-.050081 -.514889 6.214783
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI 89 9 UG/LITER 2.25243 8 .268132 11.90409
BI2230 UG/LITER 2.256152 .976301 43.22852
MO2020 UG/LITER .6490664 .7146039 110.0818
TI3349 UG/LITER 3.788222 1.665530 41.32623
B_2496 UG/LITER 3680.685 1.141 .0309934
Y_3710 PPM 1262.489 2.505 .1984456
ttl ft2 ft3
2.271019 2.510795 1.975498
3.371177 1.835579 1.561701
1.445414 .4376794 .0641062
5.437527 2.322689 3.604450
3681.981 3680.243 3679.832
1259.600 1263.800 1264.066
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -60.0000
NOCHECK
160
163 ANALYSIS REPORT
QC STANDARD
08/08/10 03:41:31 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCV RUN TIME: 08/08/10 15:34:34 COMMENT: CCV CVSl MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 101.8309 .1669 .1638578
AL3082 UG/LITER 50659.14 134.47 .2654467
BA4934 UG/LITER 1015.630 2.198 .2163841
BE3130 UG/LITER 1011.978 1.748 .1726947
CA3179 UG/LITER 49672.52 115.25 .2320154
CD2265 UG/LITER 998.7067 .5297 .0530356
C02286 UG/LITER 998.4706 .5543 .0555194
ttl tt2 tt3
101 .6706 102,.0037 101..8183
50794 .93 50666 .47 50526..02
1017..687 1015..887 1013..314
1013..920 1011..481 1010..533
49794 .31 49658 .07 49565 .18
999.2512 998.1932 998.5758
999.0802 997.9968 998.3347
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1006.851 1.431 .1421317
CU3247 UG/LITER 1015.199 1.443 .1421639
FE2714 UG/LITER 25361.64 28.64 .1129410
K_7664 UG/LITER 48741.27 146.42 .3004040
MG2790 UG/LITER 51008.63 71.90 .1409532
MN2676 UG/LITER 994.3066 1.4842 .1492665
NA3302 UG/LITER 50963.10 327.75 .6431158
ttl ft2 ft3
1008.451 1005.694 1006.407
1016.739 1014.981 1013.877
25388.28 25331.34 25365.29
48883.43 48749.43 48590.93
51088.97 50986.69 50950.34
996.0115 993.6058 993.3027
51285.68 50973.21 50630.41
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1007.088 1.416 .1406185
TL1908 UG/LITER 1005.812 6.136 .6100652
V_2924 UG/LITER 1017.013 1.379 .1356035
ZN2138 UG/LITER 1084.851 2.157 .1988599
PB2203 UG/LITER 1000.040 1.450 .1450225
SE1960 UG/LITER 1007.468 .925 .0918187
SB2068 UG/LITER 1029.432 .853 .0828598
ftl ft2 ft3
1008-398 1005.586 1007.279
1005.189 1000.011 1012.236
1018.602 1016.125 1016.313
1086.722 1085.341 1082.492
999.5043 998.9343 1001.682
1008.472 1007.281 1006.651
1028.465 1029.758 1030.076
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1018.219 1.832 .1799204
22031 UG/LITER 997.6836 1-9370 .1941626
22032 UG/LITER 1001.202 2.838 .2834542
20681 UG/LITER 1023.566 2.200 .2149736
20682 UG/LITER 1032.358 1.984 .1921949
19601 UG/LITER 1007.056 1.970 .1955789
19602 UG/LITER 1007.664 .418 .0414835
ttl ft2
#3
1020.282 1016.783 1017-591
999.8339 997.1418 996.0752
999.3246 999.8141 1004.466
1024.103 1025.447 1021.146
1030.638 1031.906 1034.529
1009.257 1006.450 1005.460
1008.071 1007.685 1007.235
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1009.092 5.392 .5343903
BI2230 UG/LITER 1016.644 4.756 .4678332
MO2020 UG/LITER 1019.936 2.188 .2145426
TI3349 UG/LITER 1019.175 1.102 .1081314
B_2496 UG/LITER 1036.848 2.166 .2088567
Y_3710 PPM 1214.089 2.775 .2285458
ftl ft2 #3
1015.067 1007.620 1004.588
1021.808 1015.681 1012.443
1019.765 1017.838 1022.205
1019.910 1019.707 1017.908
1039.309 1035.999 1035.236
1211.200 1214.333 1216.733
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104-0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
161
164 ANALYSIS REPORT
QC STANDARD
08/08/10 03:48:32 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCB RUN TIME: 08/08/10 15:41:35 COMMENT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0487949 .1010961 207.1859
AL3082 UG/LITER 35.59266 4.24243 11.91940
BA4934 UG/LITER -.173358 .021854 12.60655
BE3130 UG/LITER .3064856 .0337789 11.02136
CA3179 UG/LITER -755.211 197.347 26.13142
CD2265 UG/LITER .5921664 .1301269 21.97473
C02286 UG/LITER .2291379 .2088379 91.14070
#1 ft2 ft3
.1297632 -.064518 -0811493
40.25803 34.56379 31.96615
-.158776 -.162812 -.198485
.3427244 .3008590 .2758733
-983.088 -641.423 -641.122
.7152900 .6051931 .4560160
.2395695 .4325645 .0162797
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 6.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .2448547 .1654015 67.56090
CU3247 UG/LITER .6095485 .1431600 23.48459
FE2714 UG/LITER 20.86629 4.49393 21.53679
K_7664 UG/LITER 6.428318 1.968294 30.46355
MG2790 UG/LITER 66.70337 1.47274 2.643898
MN2576 UG/LITER -.018605 .032064 172.3374
NA3302 UG/LITER -84.8886 4.0481 4.768721
ftl #2 ft3
.1073077 .4283813 .1988750
.4749728 .7599565 .5937162
25.92614 17.33946 19.33327
8.430530 6.337308 4.517115
56.03731 66.98047 54.09234
-.037522 -.036710 .0184159
-89.5007 -81.9239 -83.2413
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 6000.000
QC PASS .OOOOOOO 6000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -1.79211 .25196 14.05898
TL1908 UG/LITER 2.364260 1.600404 67.69154
V_2924 UG/LITER .1283284 .0785216 61.18807
ZN2138 UG/LITER .1278815 .0934082 73.04279
PB2203 UG/LITER .3891923 1.072739 275.6320
SE1960 UG/LITER .4675823 3.527715 754.4685
SB2068 UG/LITER .8504458 1.232291 144.8994
ttl tt2 ft3
-1.97295 -1.89905 -1.50432
3.638635 .5680773 2.886068
.1974701 .0429617 .1445532
.0734544 .0744516 .2357385
-.569856 .1897921 1.547641
1.459129 -3.44980 3.393417
-.494536 1.925191 1.120683
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .ooooooo 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .5144679 2.093994 407.0213
22031 UG/LITER 1.072766 1.347022 126.6653
22032 UG/LITER .0380326 2.035295 5351.443
20681 UG/LITER 1.793920 1.488475 82.97332
20682 UG/LITER .3695299 1.188219 321.5489
19601 UG/LITER -3.23080 6.23711 193.0516
19602 UG/LITER 2.304112 2.188897 94.99959
ftl ft2 #3
2.234475 -1.81727 1.126196
2.533786 -.119841 .8043534
-2.12923 .3344842 1.908844
.0768291 2.687219 2.717711
-.789674 1.684781 .3134821
-1.90382 -10.0246 2.236037
3.128198 -.177214 3.961352
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10-00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER .4232608 3-844990 908.4211
BI2230 UG/LITER 1.513248 1.427210 94.31432
MO2020 UG/LITER 2.214707 1.275066 57.57265
TI3349 UG/LITER 2.358435 1.659550 70.36659
B_2496 UG/LITER 8.088562 1.635480 20.21966
Y_3710 PPM 1236.244 .823 .0666671
ftl #2 #3
1.377921 -3.80912 3.700983
2-107916 -.115140 2.546969
3.627855 1.865978 1.150289
1.017397 4.214416 1.843492
9-772739 7.986378 6.506570
1236.933 1235.333 1236.467
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
162
165 08/08/10 03:55:32 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-08 RUN TIME: 08/08/10 15:48:36 COMMENT:- SDG:MY71S3 CLIENTID:MY71T7 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0969461 .2335374 240.8941
AI,3082 UG/LITER 23802.77 19.50 .0819072
BA4934 UG/LITER 43.46572 .04884 .1123667
BE3130 UG/LITER 1.263856 .024191 1.914083
CA3179 UG/LITER 116587.3 605.8 .5195817
CD2265 UG/LITER 1.562285 .006841 .4378840
C02286 UG/LITER 113.3247 .1326 .1168940
ftl #2 #3
-.045647 -.029975 .3664600
23817.15 23810.67 23780.68
43.52108 43.42873 43.44735
1.287993 1.239611 1.263965
116211.3 117286.1 116264.4
1.567380 1.554510 1.564966
113.1991 113.3118 113.4631
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 16.17577 .11745 .7739636
CU3247 UG/LITER 14.34418 .22655 1.579368
FE2714 UG/LITER 52263.32 68.44 .1309492
K_7664 UG/LITER 10595.68 16.69 .1575056
MG2790 UG/LITER 293472.0 123.6 .0421157
MN2576 UG/LITER 2252.494 1.413 .0627331
NA3302 UG/LITER 124578.2 88.1 .0707390
ftl ft2 ft3
15.06400 15.29819 15.16613
14.08295 14.46293 14.48667
52328.71 52269-06 52192.19
10613.58 10692.92 10580.56
293528.7 293557.1 293330.2
2253.916 2252.475 2251.091
124496.5 124566.5 124671.6
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM NI2316 UNITS • UG/LITER 310.3394 AVGE SDEV .5810 %RSD .1872251
TL1908 UG/LITER -4.08543 3.38286 82.80309
V_2924 UG/LITER 4.251568 .125198 2.944760
ZN2138 UG/LITER 973.4944 .8085 .0830510
PB2203 UG/LITER 4.524938 .878545 19-41561
SE1960 UG/LITER 1.125460 1.888140 167.7660
SB2068 UG/LITER 3.021180 .364093 12.05136
#1 #2 #3
311.0104 310.0048 310.0031
-7.96066 -1.72273 -2.57290
4.300252 4.109341 4.345112
974.0687 973.8446 972.5698
5.539355 4.025449 4.010010
.0925548 -.020886 3.304712
3.343003 3.094548 2.626990
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -60.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1.873566 .922208 49.22211
22031 UG/LITER 1.930523 1.430479 74.09800
22032 UG/LITER 5.805025 .604094 10.40640
20681 UG/LITER 6.830623 2.121198 31.05423
20682 UG/LITER 1.109620 1.186396 106.9190
19601 UG/LITER -3.29531 3.03389 92.06699
19602 UG/LITER 3.322833 1.730051 52.06554
ftl ft2 #3
1.168098 1.535499 2.917100
3.580493 1.172387 1.038689
6.502119 5.434678 5.478279
5.273962 9.246660 5.971246
2.369261 .0134172 .9461825
-3.10063 -6.42184 -.363442
1.677046 3.165108 5.126347
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1.792019 2.523941 140.8434
BI2230 UG/LITER 2.674887 .881743 32.96374
MO2020 UG/LITER 1.826349 .486193 26.56628
TI3349 UG/LITER 6.401548 1.102481 20.41046
B_2496 UG/LITER 3646.082 3.486 .0982992
Y_3710 PPM 1262.800 1.675 .1326160
ttl #2 «3
-1.06219 3.729409 2.708840
2.650271 1.862082 3.612309
2.381494 1.483407 1.614147
5.495834 4.254951 6.453857
3549.603 3546.011 3542.632
1260.867 1263.800 1263.733
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
163
166 08/08/10
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1 0 0 7 1 5 7 - 0 9 RUN TIME: 0 8 / 0 8 / 1 0 1 5 : 5 5 : 3 6 COMMENT: SDG:MY71S3 CLIENTID:MY71T9 MODE: CONC CORR. FACTOR: 1
0 4 : 0 2 : 3 3 PM
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.436795 .182596 41.80368
AL3082 UG/LITER 1164.263 1.583 .1371272
BA4934 UG/LITER 15.32105 .03570 .2330314
BE3130 UG/LITER .0473095 .0302090 63.85394
CA3179 UG/LITER 1142.384 185.343 16.22419
CD2265 UG/LITER .2747507 .0701052 25.51591
C02286 UG/LITER 47.24845 .11424 .2417952
ftl
#2 ft3
-.416714 -.628602 -.265069
1154.658 1155.610 1152.520
15.34108 15.27983 15.34224
.0638770 .0656100 .0124415
1356-399 1035.186 1035.567
.3146387 .3158103 .1938031
47.24997 47.13345 47.36192
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000-00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 230.9598 .4114 .1781051
CU3247 UG/LITER 4.892221 .151601 3.098823
FE2714 UG/LITER 12491.03 5.52 .0442097
K_7664 UG/LITER 225.7789 4.9686 2.200648
MG2790 UG/LITER 147625.9 58.8 .0398365
MN2576 UG/LITER 398.7501 .2250 .0564307
NA3302 UG/LITER 1927.816 31.039 1.610068
#1 #2 ft3
230.6475 230.8069 231.4259
4.927844 4.725980 5.022839
12489.25 12497.23 12486.62
229.3724 220.1089 227.8564
147558.8 147650.2 147668.6
398.7475 398.5264 398.9764
1955.168 1894.082 1934.199
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 959.7942 2.4315 .2533350
TL1908 UG/LITER -3.15626 2.66639 84.47935
V_2924 UG/LITER 4.025599 .420812 10.45340
ZN2138 UG/LITER 7.302986 .092406 1.265322
PB2203 UG/LITER .9666792 1.028775 106.5448
SE1960 UG/LITER .1332374 .8827882 662.5681
SB2068 UG/LITER .8042644 .8436792 104.9007
#1
ft2 ft3
957.5309 959.4871 962.3647
-5.80805 -3.18525 -.475500
4.511506 3.780905 3.784386
7.276506 7.226708 7.405740
1.449117 1.663503 -.215882
1.111293 -.107054 -.604527
1.731324 .0814757 .5999937
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.692643 1.315288 189.8941
22031 UG/LITER 2.139981 2.168351 101.3267
22032 20681 UG/LITER •UG/LITER .3679112 .9014664 .5918938 2.483881 160.8795 275.5381
20682 UG/LITER .7457413 2.066886 275.8177
19601 UG/LITER -.818909 2.219225 270.9977
19602 UG/LITER .5986013 1.745395 291.5788
ttl #2 #3
-1.42283 .8257518 -1.48085
3.769595 2.971385 -.321039
.2791940 .9991558 -.174616
.7765759 3.445435 -1.51761
2.197965 -1.60797 1.647224
-1.59709 1.684604 -2.64424
2.453438 -1.01152 .3538899
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 5.621979 1.524399 27.11500
BI2230 UG/LITER .5302955 2.088467 393.8309
MO2020 UG/LITER .8105324 .2989951 36.88874
TI3349 UG/LITER 10.65518 .71690 6.728159
B_2496 UG/LITER 63.94158 1.75261 2.740954
Y_3710 PPM 1222.467 2.254 .1843730
#1 #2 tt3
3.924066 6.068926 6.872945
1.803867 -1.87996 1.666983
.5807123 .7023166 1.148568
10.43403 11.45660 10.07492
65.74098 63.84390 62.23985
1219.867 1223.867 1223.667
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
164
167 08/08/10 04:09:34 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1007167-10 RUN TIME: 08/08/10 16:02:36 COMMENT: SDG:MY71S3 CLIENTID:MY71W1 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0195060 .3196809 1638.887
AL3082 UG/LITER 4970.765 10.820 .2176731
BA4934 UG/LITER 27.45853 .06072 .2211247
BE3130 UG/LITER .2569615 .0221224 8.609217
CA3179 UG/LITER 180522.0 256.3 .1419609
CD2265 UG/LITER .5766856 .2282951 39.58746
C02286 UG/LITER 28.02352 .26448 .9437684
ftl ft2 ft3
.0443074 -.311853 .3260637
4983.251 4964.119 4964.926
27.52702 27.43729 27.41129
.2809297 .2526287 .2373261
180796.1 180288.4 180481.6
.8191983 .3659343 .5449241
28.31220 27.96545 27.79290
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 4.151839 .292615 7.047847
CU3247 UG/LITER 4.650776 .080826 1.737912
FE2714 UG/LITER 11337.24 33.37 .2943590
MG2790 K_7664 UG/LITER UG/LITER 12299.03 H377668.4 865.8 28.05 .2280295 .2292369
MN2676 UG/LITER 786.3547 2.2013 .2799418
NA3302 UG/LITER 212712.5 284.7 .1338324
ftl ft2 ft3
4.484899 3.936045 4.034573
4.678483 4.559741 4.714106
11375.44 11313.72 11322.56
12331.38 H378647.9 12284.19 H377005.0 12281.52 H377351.4
788.8791 784.8343 785.3508
212835.9 212387.0 212914.7
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC HIGH 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 78.99439 .55352 .7007054
TLI908 UG/LITER -3.59283 2.05943 57.32041
V_2924 UG/LITER 1.321338 .200681 15-18774
ZN2138 UG/LITER 169.9584 .5264 .3097246
PB2203 UG/LITER 1.063062 .342819 32.24828
SE1960 UG/LITER 4.096977 .710201 17.53002
SB2068 UG/LITER .0967030 .4722748 488.3768
ftl ft2 ft3
79.60210 78.51908 78-86199
-4.04292 -1.34558 -5.38999
1.544810 1.262688 1.156516
170.6514 169.5464 169.7774
1.458579 .8511680 .0794393
3 .508845 3.884695 4.897391
.1854252 -.413641 .5183244
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.461333 1.262007 273.5564
22031 UG/LITER .5806980 .8189027 141.0204
22032 UG/LITER 1.292387 .193778 14.99378
20681 UG/LITER .6373185 .5500705 86.31014
20682 UG/LITER -.183417 .626906 341.7926
19601 UG/LITER 2.535726 2.328316 91.82050
19602 UG/LITER 4.866212 1.512036 31.07214
#1 #2 #3
.9403903 -.817173 -1.50722
1.479516 .3856432 -.123065
1.436585 1.072116 1.368461
1.238477 .1591618 .5143165
-.350570 -.709804 .5101234
4.252579 -.114450 3.469049
3.127277 5.871071 5.600290
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1.753279 .196664 11.21691
BI2230 UG/LITER -.312703 .393649 125.8858
MO2020 UG/LITER 1.915145 .637991 33.31292
TI3349 UG/LITER 9.126558 1.911144 20.94024
B_2496 UG/LITER 5510.752 9.348 .1696327
y_3710 PPM 1199.844 4.176 .3480680
ftl #2 #3
1.926216 1.539350 1.794270
-.531463 .1417382 -.548384
2.325450 2.239869 1.180115
10.07851 6.926506 10.37495
6621.421 5506.841 5503.996
1195.067 1202.800 1201.667
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
165
168 08/08/10 04:16:34 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-11 RUN TIME: 08/08/10 16:09:37 COMMENT: SDG:MY71S3 CLIENTID:MY71W5 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.115747 .205835 177.8322
AL3082 UG/LITER 62.32196 7.62428 12.23370
BA4934 UG/LITER 16.49086 .17102 1.037089
BE3130 UG/LITER .1160677 .0482566 41.57624
CA3179 UG/LITER 115636.0 1574.6 1.361665
CD2265 UG/LITER .0150784 .0706724 468.6988
C02286 UG/LITER .4174613 .1296635 31.06001
ttl ft2 ft3
-.013472 .0189198 -.352688
70.36878 61.39146 55.20564
16.68833 16.39435 16.38991
.1253032 .1690392 .0638608
117339.3 115335.1 114233.6
-.023425 -.027981 .0966414
.4747553 .5086086 .2690200
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 20.62194 .52966 2.567956
CU3247 UG/LITER 8.272445 .047989 .5801067
FE2714 UG/LITER 87.60001 .54086 .6174175
K_7664 UG/LITER 3397.609 35.897 1.056548
MG2790 UG/LITER 215356.3 1977.5 .9182436
MN2576 UG/LITER 4.037542 .071046 1.759643
NA3302 UG/LITER 542869.2 3799.8 .5999518
ftl #2 «3
20.53358 21.19012 20.14211
8.228906 8.264528 8.323899
88.22407 87.26707 87.30890
3438.837 3373.273 3380.718
217637.1 214122.2 214309.5
4.104965 3.963356 4.044306
547190.8 540051.6 541365.1
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.OO
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 14.89275 .41691 2.799439
TL1908 UG/LITER -.948375 .413961 43.64955
V_2924 UG/LITER 4.265718 .017389 .4076342
ZN2138 UG/LITER 1.399619 .090834 6.489890
PB2203 UG/LITER .0483298 .5691486 1177.636
SE1960 UG/LITER 126.6284 2.6260 2.073798
SB2068 UG/LITER .3574310 .7031572 196.7253
ftl #2 #3
15.37119 14.69975 14.60730
-.746960 -1.42450 -.673658
4.245600 4-276852 4.274621
1.391471 1.494252 1.313134
.5877756 .1036895 -.546476
127.7601 128.4988 123.6263
-.368842 .4062015 1.034933
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10-0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1.414311 .669225 47.31810
22031 UG/LITER -.458762 1.871669 407.9828
22032 UG/LITER .2907513 .8066503 277.4366
20681 UG/LITER 2.332853 1.405743 60.25854
20682 UG/LITER -.639116 .890359 139.3110
19601 UG/LITER 126.4764 3.2734 2.588122
19602 UG/LITER 126.6939 2.8560 2.254221
ttl #2 ft3
2.114160 1.348146 .7806256
-.390855 1.378030 -2.36346
1.065924 -.544066 .3503963
2.143629 1.031306 3.823625
-1.63363 .0838592 -.367580
125.3720 130.1591 123.8980
128.9419 127.6595 123.4804
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -1,0.0000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER 5.483386 4.130547 75.32840
BI2230 UG/LITER 1.763569 1.812904 102.7975
MO2020 UG/LITER 25.44263 .51425 2.021208
TI3349 UG/LITER 19.61403 .53012 2.702775
8_2496 UG/LITER 6576.831 57.962 .8813078
Y_3710 PPM 1187.800 11.374 .9575536
#1 ft2 #3
7-801091 7.934602 .7144640
3.794318 .3081174 1.188272
25.68760 25.78859 24.85170
19.66948 19.06264 20.11996
6643.757 6543.831 6542.904
1174.667 1194.333 1194.400
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
166
169 08/08/10 04:23:34 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-12 RUN TIME: 08/08/10 16:16:37 COMMENT: SDG:MY71S3 CLIENT1D:MY71W9 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .1005276 .1563181 155.4978
AL3082 UG/LITER 37.25534 3.52874 9.471782
BA4934 UG/LITER 23.60573 .02432 .1030423
BE3130 UG/LITER .0346551 .0167483 48.32867
CA3179 irc/LITER 192798.0 306.5 .1589642
CD2265 UG/LITER .1560285 .0899632 57.65815
C02286 UG/LITER 1.063261 .252433 23.74143
ftl #2 *3
-.069669 .2376861 -1335652
41.18694 36.21630 34.36276
23.57778 23-62214 23.61726
.0539710 .0258205 .0241737
193144.4 192687.5 192562.1
.2503263 .1466198 .0711395
1.257219 -7778469 1.154719
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 6.725662 -091320 1.357786
CU3247 UG/LITER 3.372308 .082268 2.439511
FE2714 UG/LITER 582.5796 6.9263 1.188909
MG2790 K_7664 UG/LITER UG/LITER 6795.706 H305919.6 444.6 12.933 .1903115 .1453455
MN2576 UG/LITER 578.6425 .8677 .1499482
NA33 02 UG/LITER 593456.8 928.4 .1564372
#1 #2 tt3
6.760819 6.794179 6.621989
3.277313 3.419805 3.419805
578.8445 578.3225 590.5718
6810.342 H305758.7 6785.817 H305577.8 6790.959 H306422.3
578.5361 577.8329 579.5584
592788.0 593065.6 594516.8
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC HIGH 'LC PASS 300000.0 40000.00 -1000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 15.29113 .55406 3.623344
TL1908 UG/LITER .9042064 2.711165 299.8392
V_2924 UG/LITER 1.415427 .258556 18.26699
PB2203 ZN2138 UG/LITER UG/LITER 1.949207 .0140340 .1254 64 .8243732 6.436647 5874.118
SE1960 UG/LITER 81.18209 .33065 .4072919
SB2068 UG/LITER .3517448 .6320509 179.6902
ftl tt2 tt3
14.94192 15.92997 15.00150
2.147806 -2.20567 2.770481
1.197734 1.347331 1.701216
1.859174 1.895930 2.092518
.2582758 -.904862 .6886883
80.81035 81.29256 81.44336
.1744710 -.172741 1.063504
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 2.276899 .966637 42.45409
22031 UG/LITER -.594818 .826407 130.9346
22032 UG/LITER .3067469 1.624864 529.7083
20681 UG/LITER 1.178764 3.206543 272.0259
20682 UG/LITER -.071536 1.079351 1508.826
19601 UG/LITER 78.68635 2.37261 3.015279
19602 UG/LITER 82.41769 .74658 .9058538
#1 ft2 *3
1.512686 1.954469 3.363541
-1.17652 .3511412 -.959076
.9629018 -1.54359 1.500930
-1.84999 .8487213 4.537564
1.174790 -.693078 -.696319
76.43779 78.45517 81.16609
82.98296 82.69875 81.57137
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER 4.661983 1.725985 37.02256
BI2230 UG/LITER 1.872009 .965289 51.56433
MO2020 UG/LITER 20.82024 .71794 3.448270
TI3349 UG/LITER 18.70429 2.02818 10.84342
B_24 96 UG/LITER 7071.005 7.517 .1063067
Y_3710 PPM 1180.533 1.842 .1559894
ftl ft2 ft3
2.780080 6.171139 5.034730
2.984436 1.376315 1.255276
21.61560 20.62499 20.22012
17.08836 18.04424 20.98029
7070.090 7063.987 7078.938
1179.933 1182.600 1179.067
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
167
170 08/08/10
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1 0 0 7 1 5 7 - 1 3 RUN TIME: 0 8 / 0 8 / 1 0 1 6 : 2 3 : 3 8 COMMENT: SDG:MY71S3 CLIENTID:MY71X1 MODE: CONC CORR. FACTOR: 1
04:30:34
PM
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.068725 .116511 169.5316
AL3082 UG/LITER 24905.66 540.68 2.170923
BA4934 UG/LITER 42.04481 .89729 2.134138
BE3130 UG/LITER 1.522173 .094911 6.235199
CA3179 UG/LITER 122170.1 2498.3 2.044912
CD2265 UG/LITER 1.610228 .143615 8.918911
C02286 UG/LITER 124.3830 2.4202 1.945740
ftl tt2 #3
.0637740 -.155167 -.114782
25529.95 24599.51 24587.52
43.08069 41.54562 41.50812
1.631731 1.469793 1.464996
125004.4 121218.0 120287.8
1.772846 1.567065 1.500782
127.1771 123.0278 122.9440
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 13.95440 .66230 4.746141
CU3247 UG/LITER 21.51627 .14000 .6506478
FE2714 UG/LITER 46084.08 974.59 2.114804
K_7664 MG2790 UG/LITER UG/LITER 11589.29 H329329.5 231.77 6937.0 1.999890 2.106390
MN2576 UG/LITER 2511.282 53.136 2.116894
NA3302 UG/LITER 127061.4 2194.2 1.726854
ftl ft2 #3
14.67213 13.36688 13.82419
21.48065 21.39753 21.67064
47209.43 45525.07 45517.73
11856.73 H337339.6 11464.09 H325312.5 11447.04 H325336.3
2672.638 2480.465 2480.743
129591.7 125684.7 125907.6
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC HIGH 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 357.2266 8.2933 2.321594
TL1908 UG/LITER -3.16614 1.17613 37.14703
V_2924 UG/LITER 2.632268 .188991 7.179773
ZN2138 UG/LITER 1209.340 27.474 2.271346
PB2203 UG/LITER 3.015918 .542172 17.97703
SE1960 UG/LITER 2.868005 .955131 33.30296
SB2068 UG/LITER 2.864373 .794262 27.72901
ttl #2 #3
366.8029 352.4506 352.4263
-3.08829 -4.37926 -2.03088
2.850490 2.524483 2.521830
1241.045 1192.524 1194.450
2.618726 3.633596 2.796432
3.729984 3.032860 1.841181
2.497474 3.775759 2.319886
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .8205174 1.845063 224.8657
22031 UG/LITER 1.963969 2.322636 118.2623
22032 UG/LITER 3.528576 .469003 13.29157
20681 UG/LITER 4.066018 1.601060 39.47369
20682 UG/LITER 2.259705 .492466 21.79338
19601 UG/LITER -4.64332 3.85804 83.08797
19602 UG/LITER 6.608296 1.526730 23.10323
ttl #2 ft3
2.566711 1.004473 -1.10963
1.017923 4.610327 .2636666
3.405469 3.133404 4.046854
3.863400 5.744673 2.559981
1.805569 2.783157 2.190390
-4.66575 -.779079 -8.49513
7.906600 4.926329 6.991960
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.166865 1.696005 73.60888
BI2230 UG/LITER 2.685576 .821490 30-58896
M02020 UG/LITER 1.516064 .902196 59.50912
TI3349 UG/LITER 6.814365 2.536972 37.22976
B_2496 UG/LITER 3734.119 75.391 2.018988
Y_3710 PPM 1257.400 24.668 1.961028
ftl ft2 ft3
3.217657 2.951399 .3315384
3.632093 2.168231 2.266404
1.429800 2.458294 .6600984
9.717575 6.024002 5.701519
3821.107 3693.568 3687.681
1228.933 1272.133 1271.133
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
168
171 08/08/10 04:37:35 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-14 RUN Tllffi: 08/08/10 16:30:38 COMMENT: SDG:MY71S3 CLIENTID:MY71X3 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.117910 .115057 97.58065
AL3082 UG/LITER 126933.1 320.8 .2527484
BA4934 UG/LITER 11.96769 .04122 .3444111
BE3130 UG/LITER 6.713660 .049828 .7421879
CA3179 UG/LITER 258560.9 928.2 .3589895
CD2265 UG/LITER 6.903809 .223156 3.232363
C02286 UG/LITER 596.6943 1.8169 .3044929
ftl ft2 ft3
-.217063 .0082482 -.144916
127302.6 126725.1 126771.7
11.99279 11.99016 11.92012
6.769495 6.673713 6.697773
259506.5 257651.1 258525.0
6.646305 7.040752 7.024370
598.4951 694.8617 596.7263
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 36.24380 .39422 1.087691
CU3247 UG/LITER 8.114121 .112858 1.390889
FE2714 UG/LITER 322027.2 746.3 .2317493
K_7664 UG/LITER 45680.20 166.24 .3639267
MG2790 UG/LITER 293928.8 706.2 .2399381
MN2576 UG/LITER 8157.691 19.825 .2430275
NA3302 UG/LITER 319373.3 448.5 .1404282
ftl ft2 ft3
36.25892 35.84223 36.63024
8.110163 8.228906 8.003293
322857.2 321411.5 321812.8
45867.61 45622.60 45550.50
294722.3 293373.5 293690.7
8180.157 8142.648 8150.268
319889.8 319082.9 319147.1
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1404.043 2.589 .1843742
TLI908 UG/LITER -8.22646 1.36527 16.59607
V_2924 UG/LITER 16.15915 .17600 1.089184
ZN2138 UG/LITER 2211.154 5.351 .2420159
SE1960 PB2203 UG/LITER UG/LITER 21.04314 L-12.1718 2.5200 .59990 2.850824 20.70389
SB2068 UG/LITER 7.968142 .340425 4.272322
#1 ft2 #3
1406.466 1401.316 1404.346
-6.76965 -9.47663 -8.43312
16.34852 16-00059 16.12833
2217.330 2207.901 2208.231
20.81835 L-14.5451 20.58810 L-9.52700 21.72298 L-12.4433
7.791653 7.752204 8.360571
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC LOW 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1.792400 1.471111 82.07495
22031 UG/LITER 17.09874 .82060 4.798579
22032 UG/LITER 22.99850 1.13604 5.157016
20681 UG/LITER 16.12592 1.25865 7.805163
20682 UG/LITER 3.887607 .356784 9.177470
19601 UG/LITER -22.7321 6.5556 28.83851
19602 UG/LITER -6.90733 1.06538 15.42392
ftl ft2 ft3
.2045641 2.063683 3.109053
16.55035 18.04201 16.70387
22.93522 21.84537 24.21491
16.32587 14.77926 17.27263
3.523152 4.236190 3.903479
-29.8442 -16.9312 -21.4209
-6.91480 -5.83823 -7.96895
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 3.977034 3.943555 99.15819
BI2230 UG/LITER 10.63485 .51912 4.881335
MO2020 UG/LITER -3.04491 .49006 16.09441
TI3349 UG/LITER 9.711594 1.759651 18.11908
B_2496 UG/LITER 10946.81 24.82 .2267513
Y_3710 PPM 1575.800 4.688 .2974746
ftl #2 #3
2.473507 8.451187 1.006409
10.31942 11.23401 10.35114
-3.60592 -2.70028 -2.82853
9.669804 7.973209 11.49177
10975.31 10929.90 10935.23
1570.467 1677.667 1579.267
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
169
172 ANALYSIS REPORT
QC STANDARD
08/08/10 04:44:35 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CRI RUN TIME: 08/08/10 16:37:38 COMMENT: CRI MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 8.074947 .170878 2.116150
AL3082 UG/LITER -3.31162 1.70441 51.46755
BA4934 UG/LITER -.447265 .033181 7.418645
BE3130 UG/LITER 5.054570 .010005 .1979350
CA3179 UG/LITER -100.861 511.067 506.7047
CD2265 UG/LITER 5.288914 .069594 1.315848
C02286 UG/LITER 50.99752 .15840 .3105996
ttl #2 #3
7.931795 8.028923 8.264124
-4.32371 -1.34380 -4.26733
-.424731 -.485368 -.431696
5.066116 5.048457 5.049138
337.3068 22.39440 -662.284
5.250373 5.369253 5.247117
51.15268 50.83607 51.00382
ERRORS VALUE RANGE
QC PASS 10.OOOOO 3.000000
QC PASS .OOOOOOO 400.0000
QC PASS .OOOOOOO 400.0000
QC PASS 5.000000 1.600000
QC PASS .OOOOOOO 2000.000
QC PASS 5.000000 1.500000
QC PASS 50.00000 15.00000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 9.671768 .133519 1.380504
CU3247 UG/LITER 25.59312 .06540 .2555315
FE2714 UG/LITER 7.367452 6.391800 86.75727
K_7664 UG/LITER .9524710 3.026881 317.7924
MG2790 UG/LITER 11.45735 1.77903 15.52742
MN2576 UG/LITER 14.54467 .05349 .3677933
NA3302 UG/LITER -77.3263 93.1069 120.4078
#1 #2 #3
9.798414 9.532301 9.684589
25.52980 25.66041 25.58917
4.743628 2.705105 14.65362
4.444765 -.915815 -.671537
13.33356 11.24369 9.794791
14.54792 14.48962 14.59646
20.73087 -88.1778 -164.532
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS 25.00000 7.500000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 2000.000
QC PASS .OOOOOOO 2000.000
QC PASS 15.00000 4.500000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 38.57240 .33767 .8764257
TL1908 UG/LITER 25.18840 1.78646 7.092385
V_2924 UG/LITER 50.72487 .23641 .4660578
ZN2138 UG/LITER 54.21568 .24236 .4470261
PB2203 UG/LITER 10.42328 .75755 7.267842
SE1960 UG/LITER 36.40238 2.19824 6.038717
SB2068 UG/LITER 61.67022 .75710 1.227655
ftl ft2 ft3
38.83436 38.69152 38.19131
25.11079 23.44201 27.01240
50.55300 50.62714 50.99448
54.08684 54.06476 54.49514
10.86670 9.548572 10.85458
36.96620 33.97715 38.26379
60.83251 61.87257 62.30558
ERRORS VALUE RANGE
QC PASS 40.00000 12.00000
OC PASS 25.00000 12.50000
QC PASS 50.00000 15.00000
QC PASS 60.00000 18.00000
QC PASS 10.00000 5.000000
QC PASS 35.00000 10.50000
QC PASS 60.00000 30.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 9.551048 .767001 8.030543
22031 UG/LITER 10.08943 1.11026 10.19578
22032 UG/LITER 10.17571 .75783 7.447398
20681 UG/LITER 62.19289 2.47071 3.972657
20682 UG/LITER 61.39938 .10079 .1641626
19601 UG/LITER 37.16043 .82660 2.224399
19602 UG/LITER 36.01402 3.33069 9.248306
#1 ft2 ft3
8.690324 10.16212 9.800703
12-06179 9.053959 10.75255
10.25618 9.381284 10.89067
59.44453 62.90430 64.22986
61.51554 61.34760 61.33499
38.08602 36.89943 36.49584
36.39721 32.50031 39.13654
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
10.00000 3.000000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 52.30815 .44068 .8424596
BI2230 UG/LITER 51.68834 .33748 .6529144
MO2020 UG/LITER 51-75361 -38914 .7519086
B_2496 TI3349 UG/LITER UG/LITER 50.81409 Q74.60327 5.55616 2.37739 4.678612 7.447616
Y_3710 PPM 1234.467 2.384 .1931393
ttl
62.78143 51.90964 52.23339
52.07367 51.54597 51.44537
51.54433 51.51389 52.20261
48.48874 Q80.31189 50.71320 Q74-28465 53.24032 Q69.21327
1231.933 1236.667 1234.800
NOCHECK
QC PASS 50.00000 15.00000
NOCHECK
NOCHECK
NOCHECK
#2 #3 ERRORS VALUE RANGE
QC FAIL 50.00000 15.00000
170
173 ANALYSIS REPORT
QC STANDARD
08/08/10 04:51:36 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSA RUN TIME: 08/08/10 16:44:38 COMMENT: ICSA MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0566259 .2746580 485.0393
AL3082 UG/LITER 256595.6 160.2 .0624410
BA4934 UG/LITER 2.681454 .058096 2.166590
BE3130 UG/LITER .7695137 .0354450 4.606148
CA3179 UG/LITER 255100.4 1434.1 .5621887
CD2265 UG/LITER 2.074006 .151714 7.315020
C02286 UG/LITER 5.198046 .036903 .7099385
ftl ft2 #3
-.255629 .1646961 .2608110
256478.9 256529.5 256778.2
2.670726 2.629469 2.744166
.8089263 .7593643 .7402507
253446.6 256002.2 265852.3
1.990081 2.249140 1.982798
5.232905 5.159392 5.201841
ERRORS VALUE RANGE
QC PASS .OOOOOOO 20.00000
QC PASS 243900.0 49997.06
QC PASS 2.000000 400.0000
QC PASS .OOOOOOO 10.00000
QC PASS 234100.0 47990.00
QC PASS .OOOOOOO 10.00000
QC PASS 3.000000 100.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 45.89943 .61830 1.347070
CU3247 UG/LITER 24.42548 .09274 .3796933
FE2714 UG/LITER 102461.9 37.8 .0368691
K_7664 UG/LITER 3.817680 2.626125 68.78851
MG2790 UG/LITER 270044.5 277.8 .1028677
MN2576 UG/LITER 18.00564 .03665 .2035576
NA3302 UG/LITER 931.6721 43.2148 4.638413
ttl tt2 #3
45.31662 45.83369 46.54797
24.31861 24.47298 24.48485
102420.8 102495.1 102469.6
5.771708 4.848865 .8324669
269723.8 270207.4 270202.4
17.98405 18.04796 17.98491
904.4224 909.0946 981.4993
ERRORS VALUE RANGE
QC PASS 36.00000 20.00000
QC PASS 15.00000 50.00000
QC PASS 94900.00 19454.00
QC PASS .OOOOOOO 2000.000
QC PASS 248800.0 61003.00
QC PASS 19.00000 30.00000
QC PASS -OOOOOOO 2000-000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 20.32217 .31216 1.536035
TL1908 UG/LITER -4.40632 1.14226 25.92317
V_2924 UG/LITER 1.093026 .166648 15.24644
ZN2138 UG/LITER 28.83589 .17530 .6079154
PB2203 UG/LITER 12.99601 .94066 7.238045
SE1960 UG/LITER -2.07394 1.69321 81.64227
SB2068 UG/LITER 1.382342 .235988 17.07169
ftl ft2 #3
20.27862 20.65382 20.03408
-3.09395 -5.17661 -4.94841
1.134832 1.234790 .9094554
28.64656 28.86857 28.99256
13.63323 13.43916 11.91562
-3.46772 -.189616 -2.66448
1.654578 1.236920 1.256528
ERRORS VALUE RANGE
QC PASS 10.00000 80.00000
QC PASS .OOOOOOO 50.00000
QC PASS 1.000000 100.0000
QC PASS 39.00000 120.0000
QC PASS 5.000000 20.00000
QC PASS .OOOOOOO 70.00000
QC PASS .OOOOOOO 120.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .0005675 1.203353 215847.2
22031 UG/LITER -4.17696 .86557 20.72236
22032 UG/LITER 21.55515 1.27870 6.932218
20681 UG/LITER 3.856322 2.238730 58.05350
20682 UG/LITER .1367580 1.210165 884.8876
19601 UG/LITER -8.23707 1.63872 19.89443
19602 UG/LITER .9925512 1.920770 193.5184
ttl #2 #3
.4477516 -1.36237 .9162893
-4.64239 -3.17826 -4.71024
22.74287 21.72093 20.20164
3.674444 6.180443 1.714079
.6357026 -1.24310 1.017669
-10.1002 -7.01939 -7.59159
-.166899 3.209686 -.065134
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 20.00000
ELEM UNITS AVGE SDEV %RSD
SNI 8 99 UG/LITER .2887637 .6850920 237.2501
BI2230 UG/LITER 5.767748 .637996 11.06144
MO2020 UG/LITER .6968307 .3766015 54.04490
TI3349 UG/LITER 3.465966 1.858693 63.62698
B_2496 UG/LITER 7.412233 1.624121 21.91135
Y_3710
ftl #2 #3
-.255697 .0639796 1.058008
6.467717 5.616690 5.218837
.9789320 .2691744 .8423857
1.491566 6.181896 3.724438
9.018538 7.447298 5.770865
1173.600 1172.733 1176.800
ERRORS VALUE RANGE
NOCHECK
NOCHECK
NOCHECK
NOCHECK
QC PASS .OOOOOOO 200.0000
NOCHECK
PPM 1174.378 2.142 .1823929
171
174 ANALYSIS REPORT
QC STANDARD
0 8 / 0 8 / 1 0 0 4 : 6 8 : 3 6 PM
METHOD: ALT-P3Q3 SAMPLE NAME: ICSAB RUN TIME: 0 8 / 0 8 / 1 0 1 6 : 5 1 : 3 8 COMMEIC": ICSAB MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 206.2797 .4189 .2040388
AL3082 UG/LITER 257402.2 2311.3 .8979158
BA4934 UG/LITER 528.2891 4.8736 .9225199
BE3130 UG/LITER 504.9087 4.3254 .8566708
CA3179 UG/LITER 255218.9 2301.1 .9016084
CD2265 UG/LITER 1015.258 8.962 .8827195
C02286 UG/LITER 515.3943 4.9826 .9667506
ftl ft2 ft3
205.3078 204.8475 205.6838
256157.1 255980.5 260069.1
525.7624 525.1977 533.9072
502.1687 502.6624 509.8951
253108.7 254875.6 267672.3
1009.333 1010.873 1025.568
511.8134 513.2849 521.0846
EFIRORS VALUE RANGE
QC PASS 210.0000 43.00000
QC PASS 248400.0 50922.00
QC PASS 475.0000 400.0000
QC PASS 482.0000 98.00001
QC PASS 234300.0 48031.00
QC PASS 916.0000 187.0000
QC PASS 455.0000 100.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 565.0072 5.0256 .9055107
CU3247 UG/LITER 541.6552 2.4525 .4527856
FE2714 UG/LITER 103056.0 1022.4 .9920594
K_7664 UG/LITER 1.764892 3.326763 188.4966
MG2790 UG/LITER 270897.1 2361.6 .8717590
MN2576 UG/LITER 528.1309 4.4623 .8449159
NA3302 UG/LITER 974.1480 202.0825 20.74454
#1 ft2 ftl
551.7744 562.4499 560.7972
.540.3292 540.1511 544.4852
102344.7 102595.7 104227.6
2.316334 4.781478 -1.80314
269443.8 269626.6 273622.0
525.3546 525.7600 533.2781
1159.520 1004.202 758.7216
ERRORS VALUE RANGE
QC PASS 506.0000 103.0000
QC PASS 537.0000 110.0000
QC PASS 95100.00 19495.00
QC PASS .OOOOOOO 2000.000
QC PASS 254100.0 52090.00
QC PASS 483.0000 99.00000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1060.492 10.94 6 1.032207
TL1908 UG/LITER 103.5234 .2776 .2681788
V_2924 UG/LITER 521.2390 4.6666 .8950943
ZN2138 UG/LITER 1052.031 9.009 .8563363
PB2203 UG/LITER 64.01533 2.09178 3.267620
SE1960 UG/LITER 50.23179 4.29401 8.548395
SB2068 UG/LITER 632.3443 6.5531 1.036313
ffl #2 #3
1052.969 1055.458 1073-050
.103.8353 103.3031 103.4320
518.5030 518.6879 526.6262
1046.681 1046.980 1062.432
61.60557 65.07770 65.36272
45.76145 50.60939 54.32453
627.2233 630.0804 639.7291
ERRORS VALUE RANGE
QC PASS 930-0000 190.0000
QC PASS 96.00000 60.00000
QC PASS 481.0000 99.99999
QC PASS 976.0000 199.0000
QC PASS 51.00000 20.00000
QC PASS 51.00000 70.00000
QC PASS 585.0000 120.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 103.4175 .8038 .7772588
22031 UG/LITER 46.62443 2.43494 5.222464
22032 UG/LITER 72.68507 2.47842 3.409803
20681 UG/LITER 631.6774 7.3712 1.166923
20682 UG/LITER 632.6710 6.1452 .9713072
19601 UG/LITER 43.35642 2.86096 6.698688
19602 UG/LITER 53.65382 6.24679 9.778976
ttl #2 ft3
104.1340 103.5702 102.5483
44-57687 49.31691 45.97951
70.09099 72.93539 75.02882
626.8326 629.2413 639.9583
627.9113 630-4930 639.6085
41.48279 41.93692 46.64954
47.88708 54.92866 58.14572
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
97.00000 20.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1009.230 9.747 .9657682
BI2230 UG/LITER 1048.081 7.388 .7049516
MO2020 UG/LITER 1014.317 9.060 .8931714
TI3349 UG/LITER 1029.265 10.100 .9812664
B_2496 UG/LITER 1042.205 9.585 .9196637
Y_3710 PPM 1169.844 4.227 .3613336
ftl ft2 tt3
1000.507 1007.433 1019.750
1044.989 1042.741 1056.513
1008.893 1009.281 1024.775
1022.793 1024.100 1040.903
1036.151 1037.208 1053.255
1170.867 1173.467 1165.200
ERRORS VALUE RANGE
QC PASS 1000.000 205.0000
QC PASS 1000.000 205.0000
QC PASS 1000.000 205.0000
QC PASS 1000-000 206.0000
QC PASS 1000.000 200.0000
NOCHECK
172
175 ANALYSIS REPORT
QC STANDARD
08/08/10 05:05:37 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCV RUN TIME: 08/08/10 16:58:40 COMMENT: CCV CVSl MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 101.9266 .1019 .0999347
AL3082 UG/LITER 50606.64 61.96 .1224370
BA4934 UG/LITER 1015.825 1.460 .1436924
BE3130 UG/LITER 1017.217 .393 .0386320
CA3179 UG/LITER 49690.04 121.29 .2441025
CD2265 UG/LITER 1005.095 2.128 .2117231
C02286 UG/LITER 1002.604 1.661 .1556643
ttl tt2 ft3
102.0435 101.8569 101.8793
50663.79 50540.79 50616.36
1017.474 1014.701 1015.299
1017.665 1016.932 1017.054
49622.96 49830.06 49617.11
1007.491 1004.368 1003.426
1004.066 1002.786 1000.960
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1013.185 .575 .0567454
CU3247 UG/LITER 1016.240 .031 .0030895
FE2714 UG/LITER 26486.95 33.46 .1312878
K_7664 UG/LITER 48679.68 114.30 .2347970
MG2790 UG/LITER 51315.88 41.93 .0817075
MN2576 UG/LITER 997.2059 .7980 .0000251
NA3302 UG/LITER 50788.75 155.95 .3070475
#1 ft2 #3
1013.845 1012.913 1012.796
1016.216 1016.228 1016.276
25524.23 25459.53 25477.09
48802.86 48577.06 48659.11
51357.63 61273.77 51316.25
998.1230 996.8250 996.6697
50787.43 50633.47 50945.35
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
N12316 UG/LITER 1012.154 1.169 .1154690
TL1908 UG/LITER 1015.399 6.573 .6473060
V_2924 UG/LITER 1021.827 .523 .0512252
ZN2138 UG/LITER 1087.743 1.072 .0985549
PB2203 UG/LITER 1003.438 1.316 .1311561
SE1960 UG/LITER 1010.995 2.011 .1988844
S32068 UG/LITER 1028.965 1.154 .1121765
#1 tt2 ft3
1013.041 1012.591 1010.830
1022.925 1012.482 1010.789
1022.268 1021.964 1021.248
1088.939 1086.868 1087.424
1002.870 1002.501 1004.943
1013.143 1009.158 1010.684
1029.272 1027.689 1029.935
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1020.418 4.793 .4696970
22031 UG/LITER 997.8353 2.1690 .2173748
22032 UG/LITER 1006.221 1 -374 .1365103
20681 UG/LITER 1028.063 3.764 .3661441
20682 UG/LITER 1029.412 .177 .0171632
19601 UG/LITER 998.9957 2.5468 .2649423
19602 UG/LITER 1016.976 2.459 .2418279
ftl #2 ft3
1025.682 1016-306 1019-265
998.6888 995.3693 999.4476
1004.943 1006.047 1007.674
1029.284 1023.840 1031.065
1029.262 1029.607 1029.368
999.7674 996.0489 1001.171
1019.811 1015.693 1015.423
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
.NOCHECK
VALUE RANGE
1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1012.327 2-717 .2684101
BI2230 UG/LITER 1012.951 2.180 .2151793
MO2020 UG/LITER 1024.859 1.595 .1556420
TI3349 UG/LITER 1020.942 .520 .0509647
B_2496 UG/LITER 1027.978 1.696 .1650273
Y_3710 PPM 1216.444 1.580 .1298458
#1 #2 #3
1012.180 1009.685 1015.114
1013.100 1010.701 1015.053
1024.647 1023.380 1026.549
1021.526 1020.527 1020.775
1029.927 1026.828 1027.181
1215.467 1218.267 1215.600
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
173
176 ANALYSIS REPORT
QC STANDARD
08/08/10 05:12:39 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCB RUN TIME: 08/08/10 17:05:41 COMMENT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .1111694 .2736290 246.1369
AL3082 UG/LITER 34.50612 7.10738 20.59745
BA4934 UG/LITER -.094519 .039061 41.32571
BE3130 UG/LITER .3116136 .0464638 14.91070
CA3179 UG/LITER -319.201 327.615 102.6360
CD2265 UG/LITER .6674305 .2461054 36.87356
C02286 UG/LITER .4431471 .1098020 24.77778
ftl #2 #3
-.136966 .0658434 .4046313
29 .76232 31 .07827 42 .67778
-.136709 -.087235 -.059613
.2738706 .2974626 .3635075
13.01277 -642.016 -328.601
.5679355 .9477066 .4866495
.3896483 .3703479 .5694449
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .4762799 .4089661 86.04532
CU3247 UG/LITER .7599668 .2792357 36.74363
FE2714 UG/LITER 23.57289 7.42362 31.49220
K_7664 UG/LITER 6.247626 2.577179 41.25053
MG2790 UG/LITER 60.55855 1.95665 3.231007
MN2576 UG/LITER -.035907 .029768 82.90249
NA3302 UG/LITER -24.6637 63.0261 215.9695
#1 »2 #3
.1530638 .9353489 .3374269
.7480825 1.044940 .4868476
20.58858 32.02426 18.10584
7.176905 3.334685 8.231287
58.30613 61.54367 61.82685
-.065881 -.035491 -.006349
19.00462 -9.06657 -83.5991
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -1.59990 .25102 15.68977
TL1908 UG/LITER 1.955275 .816793 41.77383
V_2924 UG/LITER .3022136 .1689582 55.90688
ZN2138 UG/LITER .1966410 .0844353 42.93379
PB22 03 UG/LITER -6579194 .2974173 45.20574
SE1950 UG/LITER .7411225 .8943349 120.6730
SB2068 UG/LITER 2.400949 .229205 9.546454
#1 ft2 ft3
-1.35153 -1.59469 -1.85349
1.562522 2.894254 1.409047
.1439741 .4801619 .2825050
.1928021 .1141906 .2829302
.9492075 .6698203 .3547302
-.220159 .8949780 1.548548
2.582621 2.476790 2.143435
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS -OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .6038812 1.416066 234.4941
22031 UG/LITER .2690658 1.076232 399.9884
22032 UG/LITER .8421484 .5500113 77.18488
20681 UG/LITER 3.468605 1.475496 42.53862
20682 UG/LITER 1.858014 .758817 40.84023
19601 UG/LITER -1.24627 2.60959 209.3918
19602 UG/LITER 1.723423 .788274 45.73883
ftl #2 tt3
2.232981 -.332187 -.089151
1.064307 -.955579 .6984691
.8818734 1.471386 .1731857
2.443467 5.159594 2.802653
2.642223 1.127434 1.804387
-2.92734 -2.57149 1.760012
1.121630 2.615698 1.433042
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER .7948918 1.716314 215.9180
BI2230 UG/LITER -1.56302 .90623 57.97949
MO2020 UG/LITER 2.366067 .890204 37.62378
TI3349 UG/LITER 2.535318 2.298664 90.66570
B_2496 UG/LITER 4.125532 .463493 11.23475
Y_3710 PPM 1233.622 3.930 .3185379
#1 ft2 ft3
1.322948 -1.12340 2.185131
-.592225 -2.38668 -1.71016
2.603890 3.113207 1.381106
-.070730 4.274507 3.402177
4.329841 4.461768 3.594986
1238.000 1232.467 1230.400
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
174
177 ANALYSIS REPORT
0 8 / 0 8 / 1 0 0 5 : 1 9 : 3 9 PM
METHOD: A L T - P 3 Q 3 SAMPLE NAME: 1 0 0 7 1 5 7 - 1 5 RUN T I M E : 0 8 / 0 8 / 1 0 1 7 : 1 2 : 4 2 COMMENT: SDG:MY71S3 CLIENTID: MY71X6 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.159237 .102322 64.25785
AL3082 UG/LITER -2.34560 8.58524 366.0140
BA4934 UG/LITER 268.7781 .3528 .1312541
BE3130 UG/LITER .0082581 .0356678 431.9105
CA3179 UG/LITER 5.284643 328.4332 6214.860
CD2265 UG/LITER .1318508 .0756213 57.35366
C02286 UG/LITER .2003538 .1856345 92.65337
ttl tt2 ft3
-.177528 -.251179 -.049002
-4.22820 -9.83331 7.024702
269.1835 268.6095 268.5412
.0493971 -.010615 -.014008
15.65163 -328.209 328.4116
.0453352 .1648681 .1853491
-0403560 .4038869 .1568184
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.092623 .132854 143.4347
CU3247 UG/LITER 4.152055 .080826 1.946660
FE2714 UG/LITER 9.226061 1.373630 14.88858
K_7664 UG/LITER 10.62903 4.46252 41.98432
MG2790 UG/LITER 22.10763 11.06394 50.04579
MN2576 UG/LITER -.164470 .041965 25.51562
NA3302 UG/LITER 44.94536 55.59959 123.7048
ttl tt2 tt3
-.169589 -.169063 .0607828
4.061019 4.215384 4.179761
8.152382 8.751828 10.77397
15.73394 8.683991 7.469139
14.63006 16.87562 34.81722
-.200832 -.174027 -.118550
108.6672 19.86354 6.305303
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 3.938145 .298102 7.569613
TL1908 UG/LITER -.703609 1.956770 278.1045
V_2924 UG/LITER -.143196 .195313 136.3961
ZN2138 UG/LITER 47.45864 .03850 .0811186
PB2203 UG/LITER -.264100 .530355 200.8158
SE1960 UG/LITER .9801980 .9701145 98.97128
SB2068 UG/LITER 2.496008 1.408616 55.43478
ttl tt2 ft3
4.046982 4.166535 3.600917
-.541834 1.167250 -2.73624
.0767499 -.296357 -.209980
47.44006 47.43297 47.50291
-.779373 -.293078 .2801494
2.029704 .7945975 .1162923
2.648610 1.017304 3.822110
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.720159 .630874 87.60206
22031 UG/LITER -.008038 1.278792 15909.36
22032 UG/LITER -.405988 .214177 52.75448
20681 UG/LITER 4.568257 1.718521 37.61874
20682 UG/LITER 1.451520 2.078465 143.1923
19601 UG/LITER -1.76684 3-42283 193.7265
19602 UG/LITER 2.341739 3.144044 134.2611
ftl #2 #3
-.014198 -.917521 -1.22876
-1.38549 .2199409 1.141432
-.491664 -.564064 -.162236
6.530287 3.330059 3.844426
.7007527 -.147249 3.801057
-5.68283 -.272003 .6543228
5.070260 1.317190 -.162232
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI 899 UG/LITER -.267624 2.815277 1051.953
BI2230 UG/LITER .6455722 2.686667 416.1683
MO2020 UG/LITER 1.269958 .547662 43.12439
TI3349 UG/LITER 1.245251 .609578 48.95227
B_2496 UG/LITER 2.248765 .102425 4.554714
y_3710 PPM 1232.289 1.300 .1055067
#1 #2 #3
2.607961 -.392389 -3.01844
2.544586 -2.42843 1.820563
1.689849 .6504980 1.469528
.6783503 1.890023 1.167378
2.134366 2.331955 2.279974
1230.800 1233.200 1232.867
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10-0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00
NOCHECK
175
178 08/08/10 05:26:39 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-16 RUN TIME: 08/08/10 17:19:42 COMMENT: SDG:MY71S3 CLIENTID:MY71X6 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0268882 .1775364 660.2770
AL3082 UG/LITER -1.69482 .94938 56.01664
BA4934 UG/LITER 14.30405 .09371 .6551079
BE3130 UG/LITER -.003348 .035252 1052.863
CA3179 UG/LITER 1105.213 188.472 17.05301
CD2265 UG/LITER .1570388 .0344852 21.95966
C02286 UG/LITER .3279568 .2903884 88.54469
ttl ft2 ft3
-.178113 .1297254 .1290519
-2.16557 -2.31684 -.602054
14.34939 14.36647 14.19630
-.036783 -.006737 .0334756
1322.657 1004.262 988.7200
.1730259 .1806290 .1174614
.0510394 .3026690 .6301621
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 18.24286 .16881 .9253562
CU3247 UG/LITER 1.971138 .264454 13.41629
FE2714 UG/LITER -28-4188 5.8134 20.45601
K_7664 UG/LITER 228.2260 3.8113 1.669954
MG2790 UG/LITER 133673.1 673.0 .5034769
MN2576 UG/LITER -2,58387 .01473 .5700356
NA3302 UG/LITER 3044.942 64.174 2.107568
ttl #2 #3
18.07114 18.24885 18.40860
2.018635 2.208624 1.686154
-34.3138 -28.2620 -22.6907
227.3768 232.3902 224.9109
134058.4 134064.9 132896.0
-2.56838 -2.59770 -2.58552
3034.630 3113.648 2986.549
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -16.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 4.310318 .273451 6.344106
TL1908 UG/LITER -.134301 3.535862 2632.795
V_2924 UG/LITER -.015496 .178865 1154.269
ZN2138 UG/LITER .4564466 .0687824 15.06909
PB2203 UG/LITER 1.113124 .432758 38.87782
SE1960 UG/LITER 1.054505 1.395107 132.2997
SB2068 UG/LITER .7166895 .6668896 93.05140
ftl #2 ft3
4.100919 4.619687 4.210348
2.611383 1.109771 -4.12406
-.153810 .1864937 -.079172
.5337248 .4019306 .4336845
1.469043 .6314032 1.238924
.7743606 2.668427 -.179272
1.161562 1.038595 -.050089
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -60.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000,00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1.88488 1.15270 61.15503
22031 UG/LITER 1.935877 1.607830 83.05435
22032 UG/LITER .6923476 1.040352 150.2643
20681 UG/LITER 2.476939 .986006 39.80742
20682 UG/LITER -.172132 .523999 304.4167
19601 UG/LITER -.746923 6.315934 845.5941
19602 UG/LITER 1.943852 1.249144 64,26125
ftl #2 #3
-1.56035 -3.16605 -.929229
.6111667 1.471745 3.724721
1.887280 .2018090 -.012046
2.961267 3.136139 1.343412
.2579921 -.018657 -.755732
-3.79919 6.515392 -4.95697
3.047650 .5878493 2.196058
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.490532 1.277538 260.4393
BI2230 UG/LITER 1.171248 2.437900 208.1455
MO2020 UG/LITER 1.038708 .213552 20.65939
TI3349 UG/LITER 5.295503 3.616868 68.29927
B_2496 UG/LITER 70.70730 .26006 .3677912
Y_3710 PPM 1220.000 8.205 .6725509
#1 #2 ft3
-1.96192 .3365749 .1537539
.4750163 -.842797 3.881525
1.273297 .9872185 .8556081
1.350006 8.464092 6.082712
70.88530 70.82774 70.40886
1214.933 1215.600 1229.467
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000,00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
176
179 ANALYSIS REPORT
08/08/10 05:33:39 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-17 RUN TIME: 08/08/10 17:26:42 COMMENT: SDG:MY71S3 CLIENTID:MY71X8 NODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.180284 .251475 139.4882
AL3082 UG/LITER 30.02819 4.43768 14.77839
BA4934 UG/LITER 30.05829 .08953 .2978557
BE3130 UG/LITER .0241470 .0470270 194.7532
CA3179 UG/LITER 1648.544 582.947 35.36135
CD2265 UG/LITER .1789545 .0525766 29.37986
C02286 UG/LITER .3050591 .0786194 25.77186
ftl tt2 ft3
.0812710 -.420292 -.201831
35..03608 28 .46889 26 .58062
30..02503 30..15969 29..99014
,0652965 .0342575 -.027113
1313 .316 2321 .671 1310 .645
.1512432 .2395900 .1460303
.3712366 .3257886 .2181620
ERRORS HIGH LOW
LC PASS 1000.000 -10.OOOO
LC PASS 400000.0 -200.000
LC PASS 60000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000,00 -5.00000
LC PASS 60000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 16.42666 .29173 1.776054
CU3247 UG/LITER 3.700831 .244026 6,593829
FE2714 UG/LITER -35.0763 13.2639 36.76613
K_7 664 UG/LITER 327.3015 7.2133 2.203879
MG2790 UG/LITER 156487,2 146,4 ,0935737
MN2576 UG/LITER -2.89426 .05945 2.053941
NA33 02 UG/LITER 4320.993 48.620 1.125211
ttl tt2 ft3
16.76059 16.28940 16.22699
3.954150 3,467302 3,681040
-21.6176 -47.6806 -38.9308
335.5585 322.2250 324.1210
156331.8 156622.7 156507.1
-2.87021 -2.86060 -2.96196
4276.088 4314.264 4372.627
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 4.500998 .209613 4,657040
TL1908 UG/LITER -1,16294 3,99261 343.3201
V_2924 UG/LITER .0520649 .1395740 268.0768
ZN2138 UG/LITER .6531147 .0765097 11.71459
PB2203 UG/LITER .3664901 .7607510 207.5775
SE1960 UG/LITER -.337528 2.327355 689.5323
SB2068 UG/LITER -.073926 1.607566 2174.553
ftl #2 tt3
4,515886 4.284338 4.702770
,7628742 1,501738 -5,75344
.1925622 -.086567 .0501997
.6094593 .7414585 .6084263
.3318642 -.376357 1.143963
-2.30182 2.232948 -.943709
.0978880 -1.76050 1.440830
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000,00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -,433667 1.268084 292,4095
22031 UG/LITER 1.299618 1.179679 90,77121
22032 UG/LITER -.109367 .554048 606.5933
20681 UG/LITER -.812257 ,626600 77,14311
20682 UG/LITER .2846921 2.356450 827.7186
19601 UG/LITER -2.33849 2.67597 114.4312
19602 UG/LITER .5514604 2.266150 347.8569
ftl #2 ft3
-.076111 ,6172511 -1.84214
1.332257 .1039586 2.462640
-.177582 -.626149 .4756289
-.096226 -1,26029 -1.08026
.1847992 -2.02022 2.689500
-6.15661 .1680386 -2.02691
-.886567 3.253866 -.412908
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10,0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2,126637 1.518184 71.38899
BI2230 UG/LITER .2575152 1.423235 552,5801
MO2020 UG/LITER .6007505 .0680684 11.33056
TI3349 UG/LITER 1,590719 1.701897 106,9892
B_2496 UG/LITER 205.9061 .8099 .3933237
Y_3710 PPM 1222.889 .888 .0725942
ttl ft2 #3
3,857015 1.504816 1.018080
1,104947 1,053223 -1.38562
.6980629 .5340666 .5701228
2,986557 2,090790 -,305191
206.6475 206.0291 205.0418
1222.133 1222.667 1223.867
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
177
180 08/08/10 05:40:39 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-18 RUN TIME: 08/08/10 17:33:42 COMMENT: SIX3:MY71S3 CLIENTID:MY7lY0 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM imiTS AVGE SDEV %RSD
AG3280 UG/LITER -,040132 .322977 804.7776
AL3082 UG/LITER 64.21941 2.06987 3.223125
BA4934 UG/LITER 30.82272 .09671 .3137512
BE3130 UG/LITER -.007686 .036479 474.5876
CA3179 UG/LITER 1551.751 201.243 12.96879
CD2265 UG/LITER .0929195 .0312538 33.63540
C02286 UG/LITER .1643303 .0953384 58.01631
ftl S2 #3
.0410840 .2344843 -.395966
65.79829 61.87603 64.98391
30.92211 30,81710 30.72894
-.030100 -.027365 .0344059
1673.296 1319.459 1662.497
.1178640 .0578612 .1030333
.2317647 .2059713 .0552549
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 60000,00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 16.78060 .39322 2.343296
CU3247 UG/LITER 1.452625 .239948 16.51822
K_7664 FE2714 UG/LITER UG/LITER -17.1651 338.9068 4.4229 5,0940 29.67642 1.305062
MG2790 UG/LITER 153737.4 172.8 .1124032
I4N2676 UG/LITER -1.53972 .06131 3.981811
NA3302 UG/LITER 4313.447 110,466 2,560936
#1 ft2 #3
16.73388 17.19509 16.41283
1.591160 1.591160 1.175558
-20,1436 -20.0684 -11,2832
343.9696 335.7986 336.9492
153910.5 153736.7 163564.9
-1.51634 -1.49353 -1.60927
4321.547 4419.639 4199.166
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15,0000
LC PASS 700000,0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 6.426601 ,509479 7,927667
TL1908 UG/LITER -1.72140 1,34864 78,34589
V_2924 UG/LITER .1022870 .1626906 159.0531
ZN2138 UG/LITER .6625932 .0773161 11.84751
PB2203 UG/LITER .1441077 .3426932 237.8035
SE1960 UG/LITER ,3055542 ,7936826 259.7518
SB2068 UG/LITER ,7573150 1,227768 162.1212
ttl #2 ft3
6.857910 5,864466 6.557425
-1.36411 -3.21271 -.587372
.2732276 .0842905 -.050657
.7418112 .6107933 .6051751
-.247512 .2907868 .3890488
1.156057 .1759646 -.415359
.6930753 2.015942 -.437072
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1.05741 1.32280 125.0983
22031 UG/LITER 1.451410 .939843 64.75376
22032 UG/LITER -.518503 .966470 186.1676
20681 UG/LITER 1.044271 .496822 47.57594
20682 UG/LITER .6040127 1.694837 264.0403
19601 UG/LITER -3.31686 .46511 14.02678
19602 UG/LITER 2.103507 .972973 46.25480
ftl ft2 #3
,3023185 -2.33989 -1.13466
2.506802 .7048162 1.142613
-1.63267 .0740467 .0028175
.9483257 1.582067 .6024192
.5556737 2.222517 -.966053
-2.90854 -3.21638 -3.82266
3.175242 1.859556 1.275724
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000,00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER .2949856 1.663343 563.8729
BI2230 UG/LITER ,9767065 .6736125 68.78944
MO2020 UG/LITER .7646748 .4955789 64.80911
TI3349 UG/LITER 1.331320 1.871577 140,5805
B_2496 UG/LITER 214.0014 .2935 .1371650
Y_3710 PPM 1217.378 3,243 .2663927
ftl tt2 ft3
-1.21790 2,076169 .0266861
1.624104 .7686262 .5343894
.8800311 .2215915 1.192402
1.334713 3.201199 -.541950
214,3141 213.9584 213.7318
1214.000 1217.667 1220.467
ERRORS HIGH LOW
LC PASS 40000.00 -20,0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
178
181 ANALYSIS REPORT
08/08/10 05:47:39 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 0080607-BLKl RUN TIME: 08/08/10 17:40:42 COMMENT: SDG:MY71S4 CLIENTID:PBW 1:1 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.099667 .298540 299.5367
AL3082 UG/LITER 14.69122 5.49015 37.37028
BA4934 UG/LITER -.483897 .043233 8.934249
BE3130 UG/LITER .0056466 .0408921 724,1975
CA3179 UG/LITER 117.9294 182.4564 154.7167
CD2265 UG/LITER .1623484 .1052593 64.83546
C02286 UG/LITER .0189692 .1462471 770.9734
ftl #2 #3
.0732830 -.444390 .0721058
20.81008 13.06752 10.19605
-.441356 -.482547 -.527789
.0520570 -.010028 -.025090
328.6119 12.52328 12.65288
.2735972 .1491185 .0643294
.1448790 .0534732 -.141445
ERRORS HIGH LOW
LC PASS 5.000000 -5.00000
LC PASS 200.0000 -200.000
LC PASS 200.0000 -200.000
LC PASS 5.000000 -5.00000
LC PASS 5000.000 -5000.00
LC PASS 5.OOOOOO -5.00000
LC PASS 50.00000 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.106733 .173092 162.1732
CU3247 UG/LITER .2968580 .1399960 47.15925
FE2714 UG/LITER 1.885079 3.285588 174.2944
K_7664 UG/LITER 3.373670 3.764018 111.5704
MG2790 UG/LITER 10.65400 .66440 6.236137
MN2576 UG/LITER -.323363 .016655 5.150635
NA3302 UG/LITER 113.8962 113.3185 99.49281
ttl tt2 #3
-.031072 .0156478 -.304773
.4512240 .2612349 .1781151
3.470693 -1.89260 4.077145
7.447549 .0250547 2.648397
11.37014 10.05764 10.53422
-.312736 -.342558 -.314794
142.3614 -10.9411 210.2682
ERRORS HIGH LOW
LC PASS 10.00000 -10.0000
LC PASS 26.00000 -25.0000
LC PASS 100,0000 -100,000
LC PASS 5000.000 -5000.00
LC PASS 5000.000 -5000.00
LC PASS 15.00000 -15.0000
LC PASS 5000.000 -5000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -2.44475 .15628 6.392394
TL1908 UG/LITER -.168889 2.414819 1429.825
V_2924 UG/LITER -,013599 .232781 1711.780
ZN2138 UG/LITER 7.738563 .095738 1.237150
PB22Q3 UG/LITER .4121546 .3557229 86.30812
SE1960 UG/LITER -.750221 .593995 79.17598
SB2068 UG/LITER 2.354279 .853718 36.26239
ftl ft2 ft3
-2.36559 -2.62477 -2.34390
-2.14402 2.523226 -.886869
.2281858 -.032796 -.236186
7.834872 7.643407 7.737412
.8141761 .2841020 .1381869
-1.42998 -.489542 -.331139
3,187660 2.393592 1.481583
ERRORS HIGH LOW
LC PASS 40.00000 -40.0000
LC PASS 10.00000 -10.0000
LC PASS 50.00000 -50.0000
LC PASS 60.00000 -60.0000
LC PASS 10.00000 -10.0000
LC PASS 35.00000 -35.0000
LC PASS 60.00000 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1,77086 .46329 26.16212
22031 UG/LITER 1.433614 1,055133 73.59951
22032 UG/LITER -.108923 .148927 136.7265
20681 UG/LITER 2.843527 .944170 33.20420
20682 UG/LITER 2.100142 1.616224 76.95784
19601 UG/LITER -3.61745 1.27321 35.19624
19602 UG/LITER .6713635 .6927613 103.1872
ftl ft2 ft3
-1.62646 -1.39696 -2.28916
2.648546 .7470207 .9052760
-.112793 ,0419010 -.255878
1.813767 3.668493 3.048322
3.863657 1.747240 .6895279
-4.69218 -2.21131 -3,94886
.1887491 .3601938 1.465148
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
10.00000 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER .6458036 1.5156S4 250.1773
BI2230 UG/LITER .4394152 .2740176 62.35960
MO2020 UG/LITER ,9524572 .3047856 31.99993
T13349 UG/LITER 3.213699 2.463152 76.64538
B_2496 UG/LITER 1.746515 .486773 27.87109
Y_3710 PPM 1236.800 4.396 .3554291
#1 tt2 #3
-1.00100 2.228392 .7100197
.6839778 .1432733 .4909946
,8695726 1,290112 ,6976869
6.034508 1.488025 2.118564
2.030116 1.184446 2.024984
1231,733 1239,600 1239,066
ERRORS HIGH LOW
LC PASS 100.0000 -100.000
LC PASS 50.00000 -50.0000
LC PASS 10.OOOOO -10.0000
LC PASS 40.00000 -40,0000
LC PASS 10.00000 -10.0000
NOCHECK
179
182 ANALYSIS REPORT
0 8 / 0 8 / 1 0 0 5 : 5 4 : 3 9 PM
HETHOD: ALT-P3Q3 SAMPLE NAME: 0 0 8 0 6 0 7 - B S l RUN TIME: 0 8 / 0 8 / 1 0 1 7 : 4 7 : 4 3 COMMENT: SDG:MY71S4 CLIENTID:LCSW MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV *RSD
AG3280 UG/LITER 508.1322 1.2319 .2424428
AL3082 BA4934 UG/LITER UG/LITER 2582.402 •512.2814 .5788 2.822 .1092957 .1129853
BE3130 UG/LITER 495.6995 .8385 .1792512
CA3179 UG/LITER 9231.827 382.616 4.144528
CD2266 UG/LITER 502.1522 .3708 .0738465
C02286 UG/LITER 506.8540 .5900 .1163956
fl #2 »3
506.7641 508.5160 509,1266
2579.238 2583.306 2584.662
512.6431 512.5872 511.6138
496.3553 496.0561 494.6883
9046.435 9671.823 8977.224
602.5123 502.1728 501.7715
607.5220 506.6356 506.4044
ERRORS HIGH LOW
LC PASS 594,0000 396,0000
LC PASS 2978.000 1986.000
LC PASS 602.0000 402.0000
LC PASS 591.0000 396.0000
LC PASS 12216,00 8144,000
LC PASS 692.0000 395.0000
LC PASS 695.0000 397.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 501,8949 .4673 ,0931151
CU3247 UG/LITER 511.9931 1.5803 ,3086650
FE2714 UG/LITER 5115.819 1.411 .0275780
K_7664 UG/LITER 8937,215 11.713 .1310553
MG2790 UG/LITER 6080.676 5.364 .0882131
MN2676 UG/LITER 493.7292 .6263 .1266516
NA3302 UG/LITER 10210,96 140.35 1.374530
#1 #2 #3
502,4248 601,7185 601.6415
610.1684 612.8876 512.9233
5114.379 5117.199 5115.878
8939.161 8947.833 8924.651
6078.557 6086.775 6076.695
494.2719 493.8704 493.0454
10340.34 10230.81 10061,76
ERRORS HIGH LOW
LC PASS 688.0000 392.0000
LC PASS 688.0000 392.0000
LC PASS 6128.000 4086.000
LC PASS 12009.00 8007.000
LC PASS 7203.000 4803.000
LC PASS 594.0000 396.0000
LC PASS 12046.00 8031.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 506.0463 .6729 .1329811
TL1908 UG/LITER 1035.725 1.122 .1083603
V_2924 UG/LITER 507.2488 .6725 .1325810
ZN2138 UG/LITER 986.3402 1.8292 .1854511
PB2203 UG/LITER 1009.413 2.015 .1996427
SE1950 UG/LITER 992.7678 1.3894 .1399508
SB2068 UG/LITER 1004.867 3.411 .3394455
#1 #2 #3
505.7207 506.5961 506,8190
1035.041 1035.114 1037.021
507,4725 507.7811 506.4930
987.1381 987.5349 984.2476
1009.388 1011.440 1007.410
994.1012 992.8738 991.3285
1005.206 1008.096 1001.300
ERRORS HIGH LOW
LC PASS 590.0000 394,0000
LC PASS 1232.000 822.0000
LC PASS 601,0000 401.0000
LC PASS 1200.000 800.0000
LC PASS 1195.000 797.0000
LC PASS 1206.000 804.0000
LC PASS 1190.000 794.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1004,318 1.927 .1918716
22031 UG/LITER 1009.462 3.964 .3927290
22032 UG/LITER 1009.375 1.053 .1042901
20681 UG/LITER 998.7264 2.6442 .2647621
20682 UG/LITER 1007.930 4.349 .4315095
19601 UG/LITER 986.8165 2.5770 .2611460
19602 UG/LITER 995.4679 2.8659 .2879012
ttl #2 tt3
1006.522 1002.951 1003.481
1009.694 1013.304 1005.386
1009.223 1010.495 1008.406
996.6279 1001.696 997.8526
1009.485 1011.288 1003.017
984.2847 989.4364 986,7253
998.7203 994.3073 993.3461
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
1195.000 797,0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -,931171 .467143 50.16722
BI2230 UG/LITER .4233205 2.669279 630.5574
MO2020 UG/LITER .6344616 .6922377 109.1063
B_2496 TI3349 UG/LITER UG/LITER 2.727380 Ll.633064 .474653 2.462299 90.28074 29.06617
Y_3710 PPM 1227,511 4.471 .3642183
ftl #2 ft3
-,843776 -,513898 -1,43584
2.503123 -2.58657 1.363411
-.112345 1.254660 .7610799
2.186767 L2,179311 .5803083 Ll,321141 5.415065 Ll. 398739
1222,933 1227.733 1231.867
ERRORS HIGH LOW
NOCHECK
NOCHECK
NOCHECK
NOCHECK
LC LOW 1200.000 800.0000
NOCHECK
180
183 ANALYSIS REPORT
08/08/10 06:01:39 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 1007159-07 RUN TIME: 08/08/10 17:54:43 COMMENT: SDG:MY71S4 CLIENTID:MY71T6 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.232055 .080794 34.81659
AL3082 UG/LITER 575.9468 4.5655 .7927032
BA4934 UG/LITER 23.21483 .06709 .2889850
BE3130 UG/LITER .1291941 ,0564456 43.69056
CA3179 UG/LITER 121006.5 597.9 .4941030
CD2265 UG/LITER .3820997 .0942973 24.67871
C02286 UG/LITER 62.44237 ,15224 .2438121
ftl tt2 #3
-.315131 -.153756 -.227277
581.0083 572.1392 574.6930
23.24559 23.13788 23.26102
.1941666 ,1011844 .0922313
120810.4 120531.3 121677.8
.3816039 .2880513 .4766439
62.38950 62.32362 62.61401
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.OOOOO
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -6.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .2006433 .2498454 124.6221
CU3247 UG/LITER 3.289188 .094995 2.888085
FE2714 UG/LITER 456.4173 4.9858 1.092369
MG2790 K_7664 UG/LITER UG/LITER 11790.52 H333593.2 1014.9 35.23 .2987666 .3042474
MN2576 UG/LITER 2059.183 5.796 .2814548
NA33 02 UG/LITER 128278.2 463.3 .3611902
ttl #2 ft3
.2948910 -.082618 .3896567
3.194193 3.289188 3.384182
453.9833 453,1161 462.1526
11815.86 H333652.8 11750.29 H332599.1 11805.40 H334627.8
2059.168 2053.395 2064,986
128066.9 127958.2 128809.5
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC HIGH 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 191.4329 .8223 .4295619
TLI908 UG/LITER -3.09658 1.36519 44.08706
V_2924 UG/LITER -.187923 .211076 112.3206
ZN2138 UG/LITER 90.33864 .28910 .3200159
PB2203 UG/LITER .1807796 .7930344 438.6747
SE1960 UG/LITER 4.372543 .807570 18.46911
SB2068 UG/LITER 1.537432 .887672 57.73083
ftl ff2 ft3
191.7195 190.5056 192.0735
-1.76192 -4.49038 -3.03745
-.030335 -.106697 -.427738
90.35475 90.04182 90.61936
-.115280 -.421634 1.079253
5,302056 3.972389 3.843185
1.037583 2.562209 1.012603
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.855549 .658486 76.96649
22031 UG/LITER .8896174 1.497349 168.3138
22032 UG/LITER -.184571 .568362 307.9372
20681 UG/LITER 1.858906 2.156066 115.9858
20682 UG/LITER 1.367173 .828986 60.63600
19601 UG/LITER -1.09187 2.18275 199.9087
19602 UG/LITER 7.090462 1.664312 23.47255
ftl ft2 ft3
-.232705 -.789277 -1.54466
-.239221 .3198642 2.588209
-.064879 -.803246 .3144132
2.260652 3.785839 -.469777
.4167634 1.941161 1.743695
-1.00131 -3.31849 1.044183
8.438805 7.602213 5.230367
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.537939 .544593 21.45807
BI2230 UG/LITER .6279660 .8419606 134.0774
MO2020 UG/LITER 1.121703 ,340101 30.32006
TI3349 UG/LITER 7.402145 3.306639 44.67136
B_2496 UG/LITER 3721.212 10.979 .2950305
Y_3710 PPM 1202.178 3.830 .3186256
ftl ft2 ft3
3.126449 2.051789 2.435579
1.343567 -.299777 .8401074
.7387040 1.388386 1.238018
4.749466 6.350182 11.10679
3722.335 3709.716 3731.586
1200.667 1206.533 1199,333
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000,00 -10,0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
181
184 08/08/10 06:08:40 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0080607-DUPl RUN TIME: 08/08/10 18:01:43 COMMENT: SDG:MY71S4 CLIENTID:MY71T6D 1:1 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.194299 .125525 64.60426
AL3082 UG/LITER 560.2193 4.1929 .7484325
BA4934 UG/LITER 22.86946 .11759 .5141671
BE3130 UG/LITER .0862021 .0376858 43.60195
CA3179 UG/LITER 118228.0 230.2 .1947098
CD2265 UG/LITER .3124007 .1286226 41.17230
C02286 UG/LITER 61.23279 .10815 .1766179
ftl ft2 ft3
-.073072 -.323721 -.186104
562.6317 555.3778 562.6484
23.00036 22.77277 22,83526
.0857287 .0488552 .1240223
118470.2 118012.0 118201.7
.4567452 .2099424 ,2705144
61.30049 61.28982 61.10807
ERRORS HIGH LOW
LC PASS 1000.000 -10,0000
LC PASS 400000.0 -200.000
LC PASS 60000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.084168 .047513 56.45064
CU3247 UG/LITER 1.278469 .076341 5.971281
FE2714 UG/LITER 447.0627 8.8284 1.974749
K_7664 MG2790 UG/LITER UG/LITER 11580.54 H328013.3 37.41 535.9 .3230077 .1633863
MN2676 UG/LITER 2020.174 3.707 .1835058
NA3302 OG/LITER 126846.2 380.4 .2999190
ftl «2 tt3
-.084779 -.131372 -.036352
1.365547 1.246804 1.223055
453.8480 437.0815 450.2587
11622.35 H328631.5 11550.24 H327680.6 11569.03 H327727.7
2024.424 2018.494 2017.505
127098.8 127031.1 126408.6
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000,00 -25.0000
LC PASS 700000,0 -100.000
LC PASS 400000.0 -1000.00
LC HIGH 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 187.9277 1.0410 .5539142
TL1908 UG/LITER -3.44444 2.13647 62.02558
V_2924 UG/LITER -.165447 .059130 35.73964
ZN2138 UG/LITER 85.36433 .21555 .2525038
PB2203 UG/LITER -.041840 1.057841 2528.299
SE1960 SB2068 UG/LITER ' UG/LITER 4.991106 .9538787 2.125451 .5703871 42.58478 59.79660
ftl ft2 ft3
189.1248 187.4230 187.2352
-.986573 -4.48988 -4.85685
-.144724 -.232149 -.119467
85.58539 85,15595 85.35062
-1.03510 -.160917 1.070501
2.666342 6.834772 5.472204
1.612496 .6276164 .5215241
ERRORS HIGH LOW
LC PASS 60000.00 -40,0000
LC PASS 60000.00 -10,0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20,0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5,00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1,41465 1.46110 103,2834
22031 UG/LITER 2.531243 1.461591 57.74204
22032 UG/LITER -1.33796 .98979 73.97803
20681 UG/LITER 1.483704 .954801 64.35257
20682 UG/LITER .6791477 .5096787 75.04681
19601 UG/LITER -1.29367 3.15700 244.0341
19602 UG/LITER 8.118563 2.133014 25.27330
ftl ft2 ft3
-2.08707 -2.41778 .2616954
.8639277 3.138418 3.591382
-1.99472 -1.81959 -.199521
2.431608 .5221510 1.497352
1.193300 .6700629 .1740721
-4.76709 -.515180 1.401253
6.367239 10.49402 7.494426
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 3.090622 2.705170 87,52833
BI2230 UG/LITER ,1842537 1.902527 1032.559
MO2020 UG/LITER .7501572 .5028836 67.03709
TI3349 UG/LITER 7.628838 ,862677 11.30810
B_2496 UG/LITER 3656.072 4,087 ,1117735
Y_3710 PPM 1198.844 3,064 .2555813
ftl #2 #3
4.846595 4,449902 -.024631
2.086554 .1847080 -1.71850
.1973591 .8725998 1.180513
7,711685 6,727726 8,447102
3658,188 3551.362 3658.667
1195,400 1199,867 1201.267
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000,00 -50.0000
NOCHECK
182
185 08/08/10 06:15:40 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0080607-MSl RUN TIME: 08/08/10 18:08:43 COMMENT: SDG:MY71S4 CLIENTID:MY71T6S MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 50.66348 .35462 .6999507
AL3082 UG/LITER 2653.765 9.034 .3404408
BA4934 UG/LITER 2079.904 2.086 .1002644
BE3130 UG/LITER 49.47553 .07705 .1557369
CA3179 UG/LITER 120338.4 688.3 .5719516
CD2266 UG/LITER 49.77714 .14272 ,2867234
C02286 UG/LITER 564.3212 .3356 .0594761
ftl ft2 ft3
60.35952 50.57785 51.05307
2662.209 2654.847 2644.238
2081.377 2080.817 2077,618
49.56368 49.42102 49.44190
120791.1 120677.9 119646.4
49.93917 49.67003 49.72224
564.2950 564.6691 563.9994
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 200.9640 ,4183 .2081409
CU3247 UG/LITER 257.4709 .7547 .2931036
FE2714 UG/LITER 1480.582 1.874 .1265627
MG2790 K_7664 UG/LITER UG/LITER 11692.44 H331843.9 28.05 272.3 .2399119 .0820605
MN2576 UG/LITER 2642.024 1.837 .0722536
NA3302 UG/LITER 127569.3 100.9 .0790666
ftl ft2 ft3
201.4315 200.8352 200.6252
256.6041 257.9816 267.8272
1482.196 1481.026 1478.526
11717.42 H332157.8 11697.80 H331702.0 11662.09 H331671.8
2544,131 2540,764 2641.176
127477.3 127553.5 127677.2
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC HIGH 300000.0 -1000.00
LC PASS 40000.00 -16.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 693.7790 1.4311 .2062730
TL1908 UG/LITER 45.50809 3.28052 7.208650
V_2924 UG/LITER 509.4939 .2962 .0581418
ZN2138 UG/LITER 575.0592 .7888 .1371673
PB2203 UG/LITER 20.59594 1.57261 7.635520
SE1960 UG/LITER 56.77832 4.46267 7.859822
SB2068 UG/LITER 104.2433 .0491 .0471149
ftl ft2 tt3
695.1869 693.8242 692.3258
43,70052 43.52894 49.29481
509.6200 . 676.9059 509.7062 574.9264 509.1555 574.3452
22.04322 20.82211 18.92250
61.93102 54,25412 54.14982
104.2628 104.1875 104.2797
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000,00 -60,0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 39.63677 1.72856 4.372035
22031 UG/LITER 22.78517 1,51686 6,657244
22032 UG/LITER 19.48767 1.63524 8.391174
20681 UG/LITER 104.8714 .5234 .4991133
20682 UG/LITER 103.9196 .3021 .2907335
19601 UG/LITER 51.30554 5.68731 11.08518
19602 UG/LITER 59.50027 3.85303 6,475659
ftl ft2 ft3
40.34221 37.55248 40.71562
24,40077 22,56324 21,39149
20.85087 19.93758 17.67468
104.2716 105.2360 105.1065
104.2482 103.6538 103,8568
57.86780 48.24371 47.80511
63.94923 57.24449 57.30710
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10,0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.501668 .606645 23.27912
BI2230 UG/LITER ,3415361 1.090047 319.0657
MO2020 UG/LITER 1,490874 .692077 46.42091
TI3349 UG/LITER 4.341438 2.033438 46.83790
B_2496 UG/LITER 3695.168 4.419 .1195873
Y_3710 PPM 1201.022 2,795 .2327591
ftl ft2 tt3
3.300077 2,221244 2.283583
-.881362 1.210835 .6954353
1.416834 .8387930 2.216994
4.853622 2.100876 6.069817
3699.115 3695.996 3690.394
1197.800 1202.467 1202.800
ERRORS HIGH LOW
LC PASS 40000,00 -20.0000
LC PASS 40000,00 -10,0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
183
186 08/08/10 06:22:40 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: SDI1007159-07 RUN TIME: 08/08/10 18:15:44 COMMENT: SDG:MY71S4 CLIENTID:MY71T6L 1:5 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .1507863 .1583639 105.0254
AL3082 UG/LITER 100.0452 4.8745 4.872309
BA4934 UG/LITER 4.215260 .016740 .3971182
BE3130 UG/LITER .0055001 .0400260 727,7329
CA3179 UG/LITER 23908.54 445.14 1.861833
CD2265 UG/LITER .0601725 .0899901 149.5534
C02286 UG/LITER 12.71557 .21477 1.689023
#1 «2 ft3
.0889313 .0326850 .3307426
97.05576 97.40968 105.6701
4,227126 4.222541 4.196113
-.029758 -.002751 .0490085
23411.69 24042.98 24270.97
-.036138 .0746439 .1421121
12.69772 12.51029 12.93871
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000,00 -200.000
LC PASS 4000.000 -5.OOOOO
LC PASS 400000.0 -1000,00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.141404 .176201 124.6087
CU324 7 UG/LITER .4591405 .0675202 14.70579
FE2714 UG/LITER 52.16536 4.99394 9.573282
K_7664 UG/LITER 1861.564 1.974 .1060156
MG2790 UG/LITER 64313,44 41,75 ,0649210
MN267 6 UG/LITER 409.8985 .4359 .1063478
NA33 02 UG/LITER 25470.79 63.71 .2501171
ftl #2 ft3
-.265833 -.218599 ,0602202
.4393499 .4037271 .5343446
47.15274 57.14041 52.20294
1859.490 1863.419 1861.783
64355.47 64312.86 64271.97
410.3521 409.8608 409.4827
25542,59 25448,78 26421.01
ERRORS HIGH LOW
LC PASS 60000,00 -10.0000
LC PASS 60000.00 -25,0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000,00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 36.77508 .64461 1.752833
TL1908 UG/LITER -,603639 3,112034 515,6456
V_2924 UG/LITER -.003387 .167765 4953.328
ZN2138 UG/LITER 16.66943 .12629 .7576195
PB2203 UG/LITER -.175822 .499679 284.1958
SE1960 UG/LITER .3811042 1.224411 321.2798
SB2068 UG/LITER ,5409558 1.118476 206.7693
ftl ft2 ft3
36.24815 36.58327 37.49382
.5383501 1.776070 -4.12534
.0276620 .1466844 -.134507
16.80957 16.63428 16.56444
.1456407 .0783865 -.751493
-.997450 1.342178 .7985842
-.290426 .1007303 1.812563
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.658215 .334441 50.81035
22031 UG/LITER -.914861 ,738003 80.66827
22032 UG/LITER .1810626 .7500226 414.2339
20681 UG/LITER 2.573966 1.789837 69.53613
20682 UG/LITER -.484028 .783327 151.0350
19601 UG/LITER -1.73009 4.14869 239.7966
19602 UG/LITER 1.425114 2.198079 154.2388
ttl ft2 »3
-.363149 -.589986 -1.02151
-1.48452 -.081157 -1.17890
.9482214 ,1455268 -,550560
1.243278 1.869834 4.608787
-1.06615 -.792505 .4065746
-2.48031 2.742524 -5.45247
-.267157 .6330455 3.909466
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -1.14252 .67308 58.91225
BI2230 UG/LITER .5661414 1.852023 327.1308
MO202O UG/LITER .5693290 .4146863 72.83772
TI3349 UG/LITER 3.102652 3.279442 105.6980
B_2496 UG/LITER 738.3575 1.9983 .2706405
Y_3710 PPM 1222.622 3.311 .2707965
ftl ft2 ft3
-1.89125 -.587614 -.948694
-.428798 2.702989 -.575767
.2203363 1.027753 ,4598927
-.684115 5.001831 4.990241
740.3793 735.3836 738.3096
1219.800 1221.800 1226,267
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
184
187 ANALYSIS REPORT
QC STANDARD
08/08/10 06:29: 41 PM
PAGE :
OPERATOR:
SAMPLE NAME: CCVl METHOD: ALT-P3Q3 RUN TIME: 08/08/10 18:22:44 COMMENT: CCV CVSl MODE: CONC CORR:. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 101.7740 .4361 .4285188
AL3082 UG/LITER 50700.44 60.71 .1197504
BA4934 UG/LITER 1019.216 1.554 .1525035
BE3130 UG/LITER 1016.122 1.659 .1632904
CA3179 UG/LITER 49728.04 452,32 ,9095775
CD2265 UG/LITER 1008.386 1.393 .1381070
C02286 UG/LITER 1004.438 .649 .0645986
#1 #2
ft3
101.2996 102.1576 101.8647
50748.15 50632.10 50721.07
1020.807 1017.701 1019.141
1015.251 1015.080 1018.035
49335.29 50222.57 49626.25
1009.006 1006.791 1009.361
1004.519 1003.753 1005.043
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1014.895 1.197 .1179268
CU3247 UG/LITER 1022.126 .268 .0262449
FE2714 UG/LITER 25530.42 47.54 .1861910
K_7 664 UG/LITER 48882.56 104.10 .2129632
MG2790 UG/LITER 51342.24 45.47 .0885664
MN2576 UG/LITER 998.8680 1.0456 ,1046768
NA3302 UG/LITER 50420.66 166.95 .3112775
ftl ft2 ft3
1016.263 1014.042 1014.379
1022.379 1021.845 1022.154
25580.62 25486.09 25524.56
49001.55 48837.89 48808.26
51369.55 51289.75 51367.42
999,4376 997.6612 999,5051
50318,84 50341.72 50601.40
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1016.078 1.136 .1117794
TL1908 UG/LITER 1016.173 7.944 .7817641
V_2924 UG/LITER 1024.304 1.410 .1376374
ZN2138 UG/LITER 1088.580 1.339 .1229598
PB2203 UG/LITER 1007.344 1.631 .1618936
SE1960 UG/LITER 1012.825 1.523 .1504113
SB2068 UG/LITER 1034.184 1.745 .1687282
ftl ft2 ft3
1017.357 1015.689 1016.187
1011.187 1011.998 1025.334
1025.203 1022.680 1025.031
1088.287 1087.413 1090.041
1006.583 1006.232 1009.216
1013.238 1011.138 1014.100
1032,191 1035.436 1034.926
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104,0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1023.506 .791 .0772603
22031 UG/LITER 1001.555 1.860 .1857305
22032 UG/LITER 1010.219 2.493 .2468216
20681 UG/LITER 1026.493 2.040 .1987450
20682 UG/LITER 1038,021 1.622 .1562261
19601 UG/LITER 1006.957 3.342 .3318658
19502 UG/LITER 1015,745 3.445 .3391774
#1 ft2 #3
1024.103 1023.806 1022.609
1003.382 999.6635 1001.618
1008.167 1009.496 1012.994
1024.255 1028.248 1026.975
1036.149 1039.020 1038.892
1003.266 1009.777 1007,828
1018.206 1011.808 1017.221
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1017.642 ,563 .0553355
BI2230 UG/LITER 1018,486 3.910 .3838794
MO2020 UG/LITER 1025.760 1.734 ,1690508
TI3349 UG/LITER 1019.443 2.445 .2397911
B_2496 UG/LITER 1033.732 2.875 .2781686
Y_3710 PPM 1223.444 1.452 .1186743
ftl #2 tt3
1017.049 1017,708 1018.169
1020.262 1021.192 1014.003
1023.869 1026.138 1027.274
1018.794 1017.388 1022.146
1036.898 1031.283 1033.016
1222.267 1225.056 1223.000
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000-000 104.0000
QC PASS 1000-000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
185
188 ANALYSIS REPORT
QC STANDARD
08/08/10 06:36:42 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCBl RUN TIME: 08/08/10 18:29:46 COMMENT: CCB HODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV iRSD
AG3280 UG/LITER -.145882 .062722 42.99472
AL3082 UG/LITER -13.0070 4.1211 31.68400
BA4934 UG/LITER -.434847 .041034 9.436326
BE3130 UG/LITER ,0210189 .0255687 121.6463
CA3179 UG/LITER -101,397 197.140 194.4253
CD2266 UG/LITER .1963444 .0793776 40.42775
C02286 UG/LITER .0034147 .2316204 6782.996
Itl ff2 It3
-.073563 -.186428 -.178666
-8.95495 -12.8721 -17,1939
-.391564 -.473182 -,439795
.0603271 .0094511 .0032784
-329.033 13.09921 11.74460
.2319895 .1053927 .2516510
-.020752 .2461711 -.215175
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.061384 .141036 229.7603
CU3247 UG/LITER .3799785 .3267055 85.98000
FE2714 UG/LITER 1.651091 3.235372 194.7739
K_7664 UG/LITER -1.96672 1.55988 79.31406
MG2790 UG/LITER 7.288783 .551333 7.564127
MN2576 UG/LITER -.054685 .030049 54.94980
NA3302 UG/LITER -133.964 118.571 88,60974
lfl #2 #3
-.215473 .0613066 -.029984
.3918530 .7005848 .0474976
-.498543 5.380910 .1009045
-.338563 -2.11366 -3.44793
7.796884 7.366912 6.702653
-.089368 -.036462 -.038226
-91.2482 -42.6690 -267.974
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS ,0000000 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS ,0000000 6000.000
QC PASS ,0000000 10,00000
QC PASS ,0000000 6000,000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER ,2030200 .0898380 44.25081
TL1908 UG/LITER 2.082273 .485264 23.30455
V_2924 UG/LITER -.186386 .289324 155.2280
ZN2138 UG/LITER -.025020 .082133 315.6533
PB2203 UG/LITER .3674326 .6840635 186.1712
SE1960 UG/LITER .6227073 1.862726 299.1333
SB2068 UG/LITER 1.283394 .600485 46.78882
#1 #2 #3
.1207780 .2988966 .1893865
2.162081 2.522686 1.562052
-.338538 .1472661 -.367888
-.091260 -.053014 .0652129
-.421386 .7264307 .7972526
2.764871 -.615990 -.280759
1.566001 .5937454 1.690435
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1.34130 ,31573 23,53898
22031 UG/LITER 1,879448 1.092904 58.15024
22032 UG/LITER -.397320 .481167 121.1030
20681 UG/LITER 2.140207 2.345933 109.6124
20682 UG/LITER .8461641 1,003690 118.6164
19601 UG/LITER -1.65751 2,16963 130.8969
19602 UG/LITER 1.751227 2.666256 152,2507
#1 #2 ft3
-.986414 -1,58775 -1.45075
,6234186 2.401487 2.613438
-.962924 -.119714 -.119323
4.809134 .4044672 1.207020
-.063054 .6783705 1.923176
-.674558 -.153330 -4.14464
4.472087 -.856845 1.638440
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -2,02057 1.37372 67.98674
BI2230 UG/LITER -,270430 ,585179 216,3882
MO2020 UG/LITER 1.819791 .676798 37.19096
TI3349 UG/LITER -.704605 3.205760 454.9728
B_2496 UG/LITER 3.497534 .824368 23.56996
Y_3710 PPM 1236.955 4.748 .3838486
#1 #2 tf3
-2.96942 -2.64700 -.445296
-,868370 -.244015 .3010938
2.492061 1.828755 1.138555
-1.25548 2.740896 -3.59923
4.304002 3.532238 2.656353
1231.867 1237.733 1241.267
ERRORS VALUE RANGE
QC PASS ,0000000 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
186
189 ANALYSIS REPORT
08/08/10
METHOD: ALT-P3Q3 SAMPLE NAME: 0 0 8 0 6 0 7 - P S l RUN T I M E : 0 8 / 0 8 / 1 0 1 8 : 3 6 : 4 6 COMMENT: SDG:MY71S4 CLIENTID:MY71T6A MODE: CONC CORR. FACTOR: 1
0 6 : 4 3 : 4 3 PM
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %ESD
AG3280 UG/LITER -.097165 .116674 120.0779
AL3082 UG/LITER 1.730936 2.513135 145,1893
BA4934 UG/LITER -.483323 .032766 6,779389
BE3130 UG/LITER .1036035 .0453065 43,73065
CA3179 UG/LITER -216.777 399.191 184,1480
CD2265 UG/LITER .0785555 .1648276 209,8229
C02286 UG/LITER -,087819 .016470 18,75472
ftl *2 ft3
.0000827 -.065043 -.226535
2.615512 -1.08089 3.758189
-.452262 -.517563 -.480143
.0709318 .0845543 .1553243
-677.721 15.05689 12.33198
-.075524 .2523569 .0588333
-.104957 -.086392 -.072109
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000,00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.417086 .099301 23.80825
CU3247 UG/LITER .OOOOOOO .1439685 12E9
FE2714 UG/LITER .6520329 1.086472 166.6283
K_7664 UG/LITER -1.10618 .23692 21.41808
MG2790 UG/LITER 7.664128 1.383662 18.05374
MN2576 UG/LITER -.357924 .046139 12.89079
NA3302 UG/LITER -33.2828 64,1528 192.7508
Sl #2 #3
-.454576 -.492184 -.304498
.1306174 -.154366 ,0237488
1.680312 -.484523 .7603097
-1.06403 -1.36135 -.893166
6.204659 7.830848 8.956876
-.307515 -.368193 -.398063
37.64919 -50.2534 -87.2441
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -2.06842 .40966 19.80530
TLI908 UG/LITER 1.595713 3.066481 192.1700
V_2924 UG/LITER -.088886 .106256 119.5416
ZN2138 UG/LITER -.138286 .099584 72.01355
PB2203 UG/LITER -.236457 .737046 311.7033
SE1960 UG/LITER .4556674 2.964518 650.5881
SB2068 UG/LITER .5778319 .6945423 120.1980
ftl ft2 ff3
-2,22304 -1,60395 -2.37826
.8725842 -1,04468 4,959131
.0326552 -.164187 -.135127
-.075729 -.253123 -.086006
-.794349 .5990888 -.514112
1.000721 -2.74356 3.109837
-.146069 .6408436 1.238721
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000,00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000,00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
ASI390 UG/LITER .0243531 1.328635 5345.957
22031 UG/LITER 1.807334 1.798723 99.52353
22032 UG/LITER -1.26677 .54250 42.82549
20681 UG/LITER ,7273601 1.079236 148.3772
20682 UG/LITER .4932276 1.051348 215.1843
19601 UG/LITER 1,464872 4,120101 281,2602
19502 UG/LITER -.058307 2,389175 4097.605
ffl «2 ft3
.0155548 -1.29911 1,358113
-.145852 3.396627 2.172237
-1.12818 -.807015 -1.86513
1.001471 -.462500 1.643110
-.729050 1.181758 1.026974
2.359475 -3,02903 5.064173
.3122928 -2,61113 2,123913
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -1.25713 3.22466 256.5103
BI2230 UG/LITER 1.063158 1.590286 149.5813
MO2020 UG/LITER .6817020 .6918055 101.4821
TI3349 UG/LITER .8910910 1.050873 117.9310
B_24 96 UG/LITER 2,234404 ,664734 29,74996
Y_3710 PPM 1227,978 13,220 1.076558
ftl ft2 «3
-4.82774 1.442788 -.386436
.0698440 2.897352 .2222791
.1820320 .3917756 1.471298
1.144203 1.792292 -.263222
2.588353 2.647270 1.467589
1213.667 1230.533 1239,733
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
187
190 08/08/10 06:50:44 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1007159-01 RUN TIME: 08/08/10 18:43:47 COMMENT: SDG:MY71S4 CLIENTID:MY71S4 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.231857 .225767 97.37334
AL3082 UG/LITER -2.43496 3.03781 124.7581
BA4934 UG/LITER 27.30014 .03816 .1397764
BE3130 UG/LITER .0437105 .0199366 45.51042
CA3179 UG/LITER 1335.597 333.965 25.00488
CD2265 UG/LITER .0972216 .0528295 54.33924
C02286 UG/LITER .1192623 .0843893 70.75941
ttl ft2 tt3
-.315228 .0237389 -.404083
1.002418 -4.75914 -3.54816
27.27880 27.27743 27.34420
.0666068 .0301922 .0343326
1005.061 1672.888 1328.843
.1579844 .0715159 .0621645
.0275518 .1936383 .1366966
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 24.85840 .19947 .8024157
CU3247 UG/LITER 16.01846 .06611 .4127306
FE2714 UG/LITER -46.8264 4.1201 8.798614
K_7664 UG/LITER 229.7215 3.7114 1.615595
MG2790 UG/LITER 156264.3 386.8 .2475449
MN2576 UG/LITER -4.27073 ,03495 ,8183762
NA3302 UG/LITER 3568.607 157.544 4.414831
ttl tt2 #3
24.70684 25.08438 24.78396
15.94722 16.03033 16.07783
-42.0802 -49.4835 -48.9154
233.3542 225.9362 229.8741
155921.0 156188.5 156683.4
-4.26213 -4.24088 -4.30918
3485.235 3470.075 3760.212
ERRORS HIGH LOW
LC PASS 60000.00 -10,0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 3,941092 ,120829 3,065875
TL1908 UG/LITER -3.64607 2.25632 61.88370
V_2924 UG/LITER -.110136 .074034 67.22028
ZN2138 UG/LITER 2.395682 .085407 3.565044
PB2203 UG/LITER 1.676470 .197828 11.80024
SE1960 UG/LITER 1.664978 2.423499 146.5674
SB2068 UG/LITER 1.339678 .761694 56.11421
ttl #2 ft3
3,876360 4,080495 3.866420
-6.07418 -1.61397 -3.25005
-.068735 -.195608 -.066064
2.482623 2.392527 2.311896
1.802735 1.448479 1.778199
2.909683 3.213198 -1.12796
1.919692 .4903752 1.608666
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3,00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1.23841 1.13342 91.62208
22031 UG/LITER 1.889867 .988956 62.32940
22032 UG/LITER 1.569869 .717954 46.02689
20681 UG/LITER 3.059982 1.567365 54.48938
20682 UG/LITER ,4714320 ,6713737 142.4116
19601 UG/LITER -1.99328 4.81938 241.7816
19602 UG/LITER 3.481290 1.278442 36.72322
ttl ft2 ft3
-2.43063 -1.10985 -.174754
2.234965 2.660036 .7746016
1.576881 .8335446 2.269151
3.250320 1.305616 4.624011
1.246572 .0733020 ,0944222
-.138085 1.622815 -7.46456
4.421217 3.997133 2.025519
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER 1.063369 2.801455 263.4509
BI2230 UG/LITER 1.443361 2.261599 156.6897
MO2020 UG/LITER .9620405 .3768023 39.16699
TI3349 UG/LITER 1.010726 2.269397 224.5314
B_2496 UG/LITER 42.17834 .10647 .2524371
Y_3710 PPM 1213.200 2.023 .1667654
ftl ft2 ft3
-2.14783 3.007042 2.330896
3.745573 1.359819 -.775309
.8819236 1.372458 .6317397
-1.28823 3.249355 1.071056
42.19350 42.27642 42.06510
1214.467 1214.267 1210.867
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
188
191 08/08/10
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1 0 0 7 1 5 9 - 0 2 RUN TIME: 0 8 / 0 8 / 1 0 1 8 : 5 0 : 4 7 COMMENT: SDG:MY71S4 CLIENTID:MY71S6 MODE: CONC CORR. FACTOR: 1
0 6 : 5 7 : 4 4 PM
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.320487 .153645 47.94099
AL3082 UG/LITER -10.8324 3.1967 29,51056
BA4934 UG/LITER 44.57193 .05682 .1274823
BE3130 UG/LITER -.015501 .034058 219.7153
CA3179 UG/LITER 1665.300 666.259 40.00834
CD2265 UG/LITER .1581289 .0647385 40.94031
C02286 UG/LITER .0391553 .1768368 451.6293
ttl tt2 ft3
-.476945 -.169819 -.314698
-11.3749 -13.7232 -7.39921
44.61923 44.58766 44.50890
-.032123 -.038055 .0236761
1000.086 2332.598 1663.215
.1144697 .2325082 .1274088
-.164633 .1521903 .1299081
ERRORS HIGH LOW
LC PASS 1000.000 -10,0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000,00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 11.05297 .18623 1,675810
CU3247 UG/LITER .8114122 .1612173 19.86873
FE2714 UG/LITER -54.9602 6.0542 11.01556
K_7 664 UG/LITER 459.7317 3.1981 .6956410
MG2790 UG/LITER 171462.2 139.9 .0815929
MN2576 UG/LITER 3.272721 .029349 .8967807
NA3302 UG/LITER 4629.208 93.936 2.029198
ftl tt2 tt3
11.13011 11.18715 10.84163
.8312030 .9618204 .6412131
-52.4926 -50.5296 -61.8585
461.1108 462.0088 456.0754
171376.5 171623.6 171386.4
3.246599 3.304480 3.257085
4559.724 4736.082 4591.820
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -26.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 2.569820 .121155 4.714542
TL1908 UG/LITER -1.43911 3.19341 221.9010
V_2924 UG/LITER -.018730 .141069 753.1877
ZN2138 UG/LITER 2.471076 .054664 2.212160
PB2203 SE1960 UG/LITER UG/LITER -.567384 1.063515 .746794 .1.070463 131.6206 100.6533
SB2068 UG/LITER 1,093845 1,101763 100.7238
ftl ft2 ft3
2.679646 2.439858 2.589955
-3.57938 -2.96942 2.231462
-.127967 -.068757 .1405355
2.440356 2.534190 2.438684
-.970691 .2943522 -1.02681
1.092839 2.119013 -.021309
2.129094 1.216595 -.064152
ERRORS HIGH LOW
LC PASS 60000,00 -40,0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -,162804 1.496430 919.1615
22031 UG/LITER .8179203 .8885229 108.6320
22032 UG/LITER -1.26986 1.51884 119.6068
20681 UG/LITER 1.921748 1.246523 64.86403
20682 UG/LITER .6704884 2.010473 299.8521
19601 UG/LITER -2.03826 1.55574 76.32714
19602 UG/LITER 2.602049 1.199469 46.09709
ttl ft2 tt3
-1,32654 1,525224 -.687092
1.693246 -.083235 .8437509
-2.31194 .4728276 -1.97046
.6471943 3.138209 1.979840
2.858906 .2471922 -1.09463
-,722494 -1,63693 -3,75534
1.989119 3.984137 1.832892
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI 899 UG/LITER 2.029430 .536994 26.46034
BI2230 UG/LITER .8999588 1.325649 147.3011
MO2020 UG/LITER .1782233 .6048486 339.3769
TI3349 UG/LITER .5704854 2,935692 514.5780
B_2496 UG/LITER 200.9411 ,4901 .2439041
Y_3710 PPM 1218.778 1.167 .0957340
ttl tt2 tt3
2.506342 2.134163 1.447785
1.357319 1,936372 -.593814
-.507082 .6375340 .4042181
-2.52816 3.309971 .9296494
201.4686 200.8548 200,4998
1218.800 1217,600 1219.933
ERRORS HIGH LOW
LC PASS 40000,00 -20.0000
LC PASS 40000,00 -10.0000
LC PASS 40000,00 -10.0000
LC PASS 40000,00 -30.0000
LC PASS 40000.00 -60.0000
NOCHECK
189
192 ANALYSIS REPORT
08/08/10 07:04:44 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 1007159-03 RUN TIME: 08/08/10 18:57:47 COMMENT: SDG:MY71S4 CLIENTID:MY71S8 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.524820 .078850 15.02412
AL3082 UG/LITER 9.699290 9.806391 101.1042
BA4934 UG/LITER 63.31018 .48897 .7723352
BE3130 UG/LITER .1510764 .0699619 46.30893
CA3179 UG/LITER 11793.51 366.47 3.107385
CD2265 UG/LITER -.051323 .106775 208.0428
C02286 UG/LITER .0554963 .1697042 305.7939
ftl #2 #3
-.506399 -.611249 -.456811
21.02074 4.222440 3.854686
63.84298 62.88198 63.20557
.2277684 .1347171 .0907437
11665.43 11508.27 12206.83
.0604772 -.152238 -.062209
-.079455 .2460192 -.000075
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 14.71372 .08142 .5533593
CU3247 UG/LITER .5818417 .2827486 48.59546
FE2714 UG/LITER -53.7255 4.9606 9.233240
K_7664 UG/LITER 899.7787 9.8923 1.099417
MG2790 UG/LITER 172033.9 1061.5 .6170348
MN2576 UG/LITER -3.46142 .07686 2.220541
NA3302 UG/LITER 13039.27 63.39 .4861705
ftl #2 ft3
14.76447 14 .61980 14.75688
.6887108 .2612349 .7955794
-54.3019 -58.3728 -48.5019
911.2004 894.2012 893.9346
173188.4 171100.0 171813.3
-3.45981 -3.63908 -3.38638
13055.58 12969.32 13092.92
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25,0000
LC PASS 700000.0 -100,000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000,0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.447846 .483662 107.9973
TL1908 UG/LITER -3.40861 4.69896 134.9218
V_2924 UG/LITER 1.168836 .237761 20.34169
ZN2138 UG/LITER 1.628524 .044312 2.720985
PB2203 UG/LITER -.450597 ,778977 172.8767
SE1960 UG/LITER .8509899 .4306340 50.60389
SB2068 UG/LITER 1.219234 1.073807 88.07227
-.004582 -.963700 -.375257
-8.38625 .6826159 -2.62219
.9997896 1.066013 1,440702
1.644750 1.662435 1.578386
,3485089 -.492550 -1,20775
.8059145 1.302389 .4446666
.0751851 1.377223 2,205294
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000,00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000,00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.557835 1.109606 198,9131
22031 UG/LITER 2.293744 2,948499 128,5452
22032 UG/LITER -1.83108 ,94138 51,41139
20681 UG/LITER 1.616785 1.344015 88,60946
20682 UG/LITER 1.060728 1.035538 97.62517
19601 UG/LITER -3.39684 1,74488 51,36781
19602 UG/LITER 2.961767 .863126 29.14226
ftl #2 #3
-1.77916 .3832274 -.282567
5.619309 -.000787 1.262711
-2.29297 -.747962 -2.45230
-.034564 2,329395 2,255523
,1199466 ,8919511 2,170287
-5,32042 -1,91692 -2.95417
3.854469 2.899233 2.131609
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1,826302 2.594207 142.0469
BI2230 UG/LITER .2575681 1.701476 660.5922
MO2020 UG/LITER 1.278807 ,737007 57.63235
TI3349 UG/LITER -.768101 1.486508 193.5303
B_2496 UG/LITER 393.7684 3,2367 .8217292
Y_3710 PPM 1228.111 8.333 .6785342
#1 ft2 tt3
4.485166 -.698023 1.691774
.2222171 -1.42596 1.976443
1.905811 1.463631 .4669795
-.297470 -2.43296 .4261246
397.2528 390.8583 393.1940
1218.733 1234.667 1230.933
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
ftl «2 ft3
190
193 08/08/10
ANALYSIS REPORTMETHOD: ALT-P3Q3 SAMPLE NAME: 1 0 0 7 1 5 9 - 0 4 RUN TIME: 0 8 / 0 8 / 1 0 1 9 : 0 4 : 4 8 COMMENT: SDG:MY71S4 CLIENTID:MY71T0 MODE: CONC CORR. FACTOR: 1
0 7 : 1 1 : 4 5 PM
PAGE 1
OPERATOR: 1:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0257503 .1709267 663.7856
AL3082 UG/LITER 131678.2 115.8 .0879075
BA4934 UG/LITER 13.58242 .03241 .2386447
BE3130 UG/LITER 6.540165 .033092 .5059887
CA3179 UG/LITER 227743.6 725.8 .3187011
CD2265 UG/LITER 10.63276 .04906 .4614485
C02286 UG/LITER 588.4327 .5554 .0943903
#1 #2 #3
-.158890 .1784592 .0576820
131755.4 131734.2 131545.1
13.61801 13.57465 13.55460
6.577041 6.530402 6.513052
228436.0 227806.2 226988.4
10.58375 10.68188 10.63266
588.7712 588.7353 587.7917
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200,000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 73.21663 .16523 .2270335
CU3247 UG/LITER 4.662651 .273453 5.864752
FE2714 UG/LITER 496946.3 253.6 .0510267
K_7664 UG/LITER 46120.02 114.80 .2544416
MG2790 UG/LITER 269407.4 277.2 .1028832
MN2575 UG/LITER 7661.213 5.855 .0764190
NA3302 UG/LITER 293766.2 234.6 .0798681
#1 #2 #3
73.40156 73.07964 73.16869
4.381626 4.678483 4.927844
496826.2 497236.5 496773.2
45224.53 45138.38 44997.14
269436.9 269668.7 269116.7
7663.315 7665.727 7654.598
293594.4 294033.5 293670.6
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV *RSD
NI2316 TL1908 UG/LITER UG/LITER 1365.083 L-11.2153 1,063 1,1408 .0778564 10.17160
V_2924 UG/LITER 367,0693 ,4040 .1100712
ZN2138 UG/LITER 2194,252 2.131 .0971393
PB2203 SE1960 UG/LITER UG/LITER 34.13695 L-15.4693 .56215 3.4645 1.646741 22.39581
SB2068 UG/LITER 12.52292 1.27000 10.14141
#1 #2 ft3
1366.092 L-11.4900 1365.182 L-12.1936 1363.974 -9.96225
367.5270 366.7621 366.9189
2193.483 2196.561 2192.612
33.96685 L-11.5172 33.67950 L-16.9088 34,76460 L-17.9820
13.33346 13.17603 11.06927
ERRORS HIGH LOW
LC PASS 60000,00 -40.0000
LC LOW 60000,00 -10.0000
LC PASS 60000,00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3,00000
LC LOW 30000.00 -5.00000
LC PASS 40000,00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 46.11081 1,04288 2.261674
22031 UG/LITER 37,00520 1,45163 3.922781
22032 UG/LITER 32,68861 ,56613 1.731887
20681 UG/LITER 23.16717 1.27080 5.487736
20682 UG/LITER 7.205986 1.994020 27.67171
19601 UG/LITER -31.0667 3.5107 11.30049
19602 UG/LITER -7.69010 4.22128 54.89231
#1 #3
47.29985 45,68131 45.35127
37.74786 35.33250 37,93525
32.06281 32.83787 33.16516
21.95195 24.48471 23.03485
9.022892 7.522382 5.072684
-28.8413 -29.2450 -35.1138
-2.87584 -10.7578 -9.43670
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 3.186421 4.592390 144.1238
BI2230 UG/LITER 13.96481 1.62625 11.64538
MO2020 UG/LITER -2.22825 .54113 24.28500
TI3349 UG/LITER 8.737020 1.423036 16.28743
B_2496 UG/LITER 9825.930 8.856 .0901302
Y_3710 PPM 1572.400 1.737 .1104795
ttl #2 #3
5.366804 -2.09000 6.282456
15.72146 13.66122 12.51173
-2.01989 -2.84259 -1.82227
7.492237 8.430477 10.28834
9828.306 9833.355 9816.128
1572.267 1570.733 1574.200
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
tt2
191
194 08/08/10 07:18:45 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1007159-05 RUN TIME: 08/08/10 19:11:48 COMMENT: SDG:MY71S4 CL1ENTID:MY71T2 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.445617 .364481 81.79242
AL3 082 UG/LITER 124910.2 756.0 .6052640
BA4934 UG/LITER 11.83783 .06292 .5315264
BE3130 UG/LITER 6.686618 .042929 .6420166
CA3179 UG/LITER 262362.2 1736.7 .6881649
CD2265 UG/LITER 6.233411 .222768 3.673611
C02286 UG/LITER 584.1235 4.0659 .6943644
ttl ft3
-.866072 -.219281 -.251498
124544.2 124406.7 125779.6
11.83421 11.77680 11.90249
6.651240 6.674236 6.734377
261512.6 251213.9 254360.1
6.463432 6.018707 6.218094
582.2215 581.3680 588.7809
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -6.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 35.76666 .26901 .7521248
CU3247 UG/LITER 7,136468 ,139996 1.961699
FE2714 UG/LITER 317664.6 1960.6 .6174067
K_7664 UG/LITER 44976.82 218.56 .4859278
MG2790 UG/LITER 288542.1 1873.8 .6494046
MN2676 UG/LITER 8003.964 60.684 .6332380
NA3302 UG/LITER 312463.6 1455.9 .4659570
ftl #2 ft3
35.61846 35.60434 36.07718
7.017726 7.290834 7.100845
316352.7 316494.0 319817.0
44877.81 44825.30 46227.36
287333.4 287592.2 290700.6
7976.073 7974.332 8062.488
312071.0 311244.0 314075.4
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1379.263 6.955 .5042883
TL1908 UG/LITER -5.76182 1.90208 33.01173
V_2924 UG/LITER 15.41693 .13221 ,8575487
ZN2138 UG/LITER 2161.762 14.432 .6676034
SE1960 PB2203 UG/LITER UG/LITER 20.80981 L-12.1862 .73263 .7868 3.520613 5.466863
SB2068 UG/LITER 8.536283 .653614 7.656896
#1 tt2 ft3
1374.853 1375.654 1387.281
-7.78452 -4.00925 -5.49168
15.26586 15.47341 15.51152
2153.573 2153.170 2178.415
21.11086 L-12.2894 21.34396 L-12.9147 19.97461 L-11.3615
9.267276 8.333420 8.008155
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC LOW 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 2.434731 .148425 6.096158
22031 UG/LITER 16.95126 .79957 4.716885
22032 UG/LITER 22.72242 .70216 3.090152
20681 UG/LITER 15.17581 1.74342 11.48812
20682 UG/LITER 5.213788 1.192416 22.87046
19601 UG/LITER -20.4950 1.2515 6.106294
19602 UG/LITER -8.04424 1.74870 21.73847
ftl *3
2.482825 2.268222 2.553144
17.18578 17.60736 16,06066
23,05475 23.19672 21.91579
16.00750 13.17229 16.34764
5.894495 5.909935 3.836932
-21.0698 -19.0594 -21.3559
-7.91350 -9.85464 -6.36459
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 5.596412 1.618151 28.40649
BI2230 UG/LITER 9.278594 1.002322 10.80252
MO2020 UG/LITER -3.05563 ,74061 24.23750
TI3349 UG/LITER 8.791751 1,299983 14.78640
B_2496 UG/LITER 10806.14 68,70 .5432273
Y_3710 PPM 1585.800 5,893 .3715956
ftl tt2 ft3
4.193185 7.409089 5.486962
8.702220 10.43597 8.697590
-2.77096 -2.49959 -3.89633
7.928688 10,28691 8.159557
10774.67 10769.88 10873.87
1583.933 1592.400 1581.066
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
tt2
ft2
192
195 08/08/10
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: 1 0 0 7 1 5 9 - 0 6 RUN TIME: 0 8 / 0 8 / 1 0 1 9 : 1 8 : 4 9 COMMENT: SDG:MY71S4 CLIENTID :MY71T4 MODE: CONC CORR. FACTOR: 1
0 7 : 2 5 : 4 6 PM
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .1563930 .5063876 323.7916
AL3082 UG/LITER 54.19408 2.98261 5.503579
BA4934 UG/LITER 30.98491 .08328 .2687797
BE3130 UG/LITER .1072679 .0282505 26.33639
CA3179 UG/LITER 106680.4 860.7 .7974728
CD2265 UG/LITER .3253075 ,1306841 40.17249
C02286 UG/LITER 105.5754 ,4339 ,4110141
#1 ft2 ft3
-.322187 ,1047370 .6866287
57.53693 51.80504 53.24026
30.98356 31,06886 30.90231
.1299354 ,1162499 .0766184
106842,6 106656,1 107543.5
.3473921 .1849881 .4435421
105,3133 105.3367 106.0763
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000,000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000,00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .0584676 .1246665 213.2597
CU3247 UG/LITER .7164176 .2345993 32,74617
FE2714 UG/LITER 16971.63 23.53 .1386662
K_7664 UG/LITER 10521.05 4.00 .0376427
MG2790 UG/LITER 214839.9 270.6 .1259600
MN2576 UG/LITER 2493.307 2.717 .1089832
NA3302 UG/LITER 111399.2 138.2 .1241003
#1 tt2 ft3
-.035571 .1998683 .0110755
.7599566 .9261975 .4630988
16945.77 16991.78 16977.35
10621.06 10625.04 10617.05
214692,3 214798.6 216128.8
2490.993 2492,629 2496.299
111263.7 111415,1 111528.8
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 257,0764 .6767 .2243387
TL1908 UG/LITER -1.66647 .97983 62.54994
V_2924 UG/LITER .0845316 .2560933 301.7725
ZN2138 UG/LITER 66.76462 .27182 ,4789372
PB2203 UG/LITER 1.296329 .888714 68.55624
SE1960 UG/LITER -.339841 1.968273 579,1740
SB2068 UG/LITER 1.972238 .956030 48,47435
ttl ft2 ft3
267,7373 256,6753 256,8166
-1.18856 -2.67898 -.831876
.3731446 -.110761 -.008789
66.72881 56.49662 57.03842
1.025093 .5748373 2.289056
1.698879 -.489262 -2.22915
3.074444 1.474514 1.367766
ERRORS HIGH LOW
LC PASS 60000.00 -40,0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.689634 1.596429 231,4893
22031 UG/LITER 2.560089 1.541311 60.20536
22032 UG/LITER .6500506 .8218613 126.4303
20681 UG/LITER 2.130609 2.465583 115.7220
20682 UG/LITER 1.883002 .600484 31.88972
19601 UG/LITER -7.16473 6.48278 90.48180
19602 UG/LITER 3.067317 .481966 15.76400
ttl ft2 tt3
-1.98063 -1.18369 1.095418
1.202211 2.242652 4.2354 04
.9214147 -.273176 1.301914
4.781828 -.093541 1.703539
2.211864 2.247220 1.189923
-.088117 -8.58938 -12.8167
2.580866 3.544595 3.046492
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10,0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1.460419 .485735 33.26001
BI2230 UG/LITER 1.657232 1.510068 91.11990
MO2020 UG/LITER .3866338 .1507208 38.98283
TI3349 UG/LITER 4.613530 1.279470 27.73239
B_2496 UG/LITER 3750.681 1.711 .0456056
Y_3710 PPM 1204.333 2.802 .2326954
ttl ft2 ft3
1.066014 2.002621 1.313621
-.083866 2.446529 2.610022
.5606386 .3025498 .2967131
3.431732 4.436867 5.972290
3752.564 3750.255 3749.224
1204.467 1207.067 1201.467
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
193
196 ANALYSIS REPORT
QC STAMDARD
08/08/10 07:32:46 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CRI RUN TIME: 08/03/10 19:25:49 COMMENT: CRI MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 8.007548 .373957 4.670055
AL3082 UG/LITER 1.142459 6.523539 571.0086
BA4934 UG/LITER -.468812 .019006 4.054035
BE3130 UG/LITER 5.101401 .067298 1.319205
CA3179 UG/LITER -528.456 180.673 34.18890
CD2265 UG/LITER 5.241036 .053656 1.023776
C02286 UG/LITER 51.02347 .25405 .4979079
#1 #2 *3
8.142486 8.295309 7.584851
-4.67316 -.095866 8.196407
-.486415 -.448660 -.471369
5.033113 5.103427 5.167664
-319.835 -631.779 -633.753
6.198165 5.301209 5.223734
50.99668 50.78387 51.28985
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS .OOOOOOO 400.0000
QC PASS .OOOOOOO 400.0000
QC PASS 6.000000 1.500000
QC PASS .OOOOOOO 2000.000
QC PASS 5.000000 1.600000
QC PASS 50.00000 15.00000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 9.833951 .488507 4.967553
CU3247 UG/LITER 25.43084 .19917 .7831773
FE2714 UG/LITER 3.177685 6.700127 210.8559
K_7 664 UG/LITER .4229038 3.016502 713.2832
MG2790 UG/LITER 9.463387 1.642216 17.35335
MN2576 UG/LITER 14.50515 .09134 .6296917
NA33 02 UG/LITER -34.3337 21.9386 63.89808
ftl «2 fl3
9.570502 10.39763 9.533720
25.66041 25.32793 25.30418
-4.55174 7.333561 6.750934
-2.20435 3.717045 -.243986
9.191032 11.22475 7.974376
14.41192 14.50906 14.69447
-56.7457 -12.9014 -33.3540
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS 25.00000 7.500000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 2000.000
QC PASS .OOOOOOO 2000.000
QC PASS 15.00000 4.500000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 38.58888 .48499 1.256825
TLI908 UG/LITER 21.99168 .84796 3.855799
V_2924 UG/LITER 50.69337 .13293 .2622265
ZN2138 UG/LITER 54.08145 .41726 .7716472
PB2203 UG/LITER 10.04689 .72707 7.236761
SE1960 UG/LITER 35.17668 2.45029 6.965669
SB2068 UG/LITER 62.48565 .67064 1.073265
ftl ft2 »3
38.10714 38.58244 39.07706
22.90780 21.23434 21.83288
50.81105 50.54918 50.71988
53.95691 53.74138 54.54708
10.31362 9.224123 10.60292
37.43754 35.51945 32.57305
62.08456 63.25986 62.11253
ERRORS VALUE RANGE
QC PASS 40.00000 12.00000
QC PASS 25.00000 12.50000
QC PASS 50.00000 16.00000
QC PASS 60.00000 18.00000
QC PASS 10.00000 6.000000
QC PASS 35.00000 10.50000
QC PASS 60.00000 30.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 9.048584 1.538028 16.99744
22031 UG/LITER 10.53252 .66737 6.336300
22032 UG/LITER 9.739658 1.408988 14.39275
20681 UG/LITER 61.90017 1.61470 2.608548
20682 UG/LITER 62.76804 1.30988 2.086864
19601 UG/LITER 33.76918 3.10358 9.190558
19602 UG/LITER 35.86946 2.42944 6.772994
ftl ft2 ft3
7.276498 10.03618 9.833075
10.54112 11.19566 9.860893
10.18515 8.225071 10.95848
60.33890 61.79814 63.56346
62.94615 63.97975 61.37822
37.31491 32.44687 31.54576
37.48883 37.04356 33.07600
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
10.00000 3.000000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 51.64996 1.38634 2.584100
BI2230 UG/LITER 52.43116 2.26178 4.313813
MO2020 UG/LITER 51.81135 .55446 1.070144
TI3349 B_2496 UG/LITER UG/LITER 51.89629 Q66.67232 2.72025 2.53896 5.241705 3.808100
Y_3710 PPM 1233.178 3.705 .3004795
ftl ft2 ft3
63.22161 50.60075 51.12751
62.38676 54.71530 50.19242
51.29809 51.73655 52.39941
49.97327 Q69.45557 55.00867 Q66.07841 50.70692 64.48296
1231.667 1237.400 1230.467
ERRORS VALUE RANGE
NOCHECK
QC PASS 50.00000 15.00000
NOCHECK
NOCHECK
QC FAIL 50.00000 15.00000
NOCHECK
194
197 ANALYSIS REPORT
QC STANDARD
08/08/10 07:39:46 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSA RUN TIME: 08/08/10 19:32:49 COMMENT: ICSA MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.007348 .228790 3113.618
AL3082 UG/LITER 257899.3 1826.0 .7080275
BA4934 UG/LITER 2.530862 .040098 1.524132
BE3130 UG/LITER .9189331 .0149115 1.622699
CA3179 UG/LITER 257066.4 1163.9 .4527457
CD2265 UG/LITER 1.821983 .096870 5.316726
C02286 UG/LITER 5.520071 .236296 4.280664
ftl «2 ft3
.1404992 .1083355 -.270879
256638.0 257066.7 259993.2
2.600654 2.615578 2.676354
.9360738 .9117777 .9089479
256410.0 256379.0 258410.2
1.899644 1.862868 1.713436
5.792469 5.397489 6.370256
ERRORS VALUE RANGE
QC PASS .OOOOOOO 20.00000
QC PASS 243900.0 49997.06
QC PASS 2.000000 400.0000
QC PASS .OOOOOOO 10.00000
QC PASS 234100.0 47990.00
QC PASS .OOOOOOO 10.00000
QC PASS 3.000000 100.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 46.64870 .38402 .8232244
CU3247 UG/LITER 24.27507 .20198 .8320466
FE2714 UG/LITER 103335.6 702.3 .6796604
K_7664 UG/LITER 4.787579 2.477749 61.75369
MG2790 UG/LITER 271548.2 1879.1 .6920087
MN2576 UG/LITER 18.06820 .14846 .8216760
NA3302 UG/LITER 874.2454 37.3575 4.273112
#1 tt2 ft3
46.25310 47.01999 46.67302
24.42548 24.04550 24.35424
102811.4 103061.8 104133.5
7.377943 2.440375 4.544419
270158.4 270800.1 273686.2
17.95223 18.01687 18.23552
869.3187 913.8218 839.5958
ERRORS VALUE RANGE
QC PASS 36.00000 20.00000
QC PASS 15.00000 50.00000
QC PASS 94900.00 19454.00
QC PASS .OOOOOOO 2000.000
QC PASS 248800.0 51003.00
QC PASS 19.00000 30.00000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 20.54065 .17005 .8278467
TL1908 UG/LITER .1721656 2.046510 1188.687
V_2924 UG/LITER 1.350376 .126634 9.377719
ZN2133 UG/LITER 28.46075 .42372 1.488773
PB2203 UG/LITER 12.79107 .38499 3.009798
SE1960 UG/LITER -5.31155 .64582 12.15874
SB2068 UG/LITER 2.528624 .766721 30.32167
#1 tt2 *3
20.70345 20.55431 20.36418
2.082359 -1.98774 .4218807
1.249782 1.308766 1.492580
28.07100 28.39949 28.91177
12.34705 12.99449 13.03167
-6.00007 -5.21536 -4.71923
2.898360 3.040414 1.647098
ERRORS VALUE RANGE
QC PASS 10.00000 80.00000
QC PASS .OOOOOOO 50.00000
QC PASS 1.000000 100.0000
QC PASS 39.00000 120.0000
QC PASS 5.000000 20.00000
QC PASS .OOOOOOO 70.00000
QC PASS .OOOOOOO 120.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1.741657 1.950966 112.0178
22031 UG/LITER -5.91212 .61698 10.43587
22032 UG/LITER 22.11418 .88153 3.986272
20681 UG/LITER 6.921077 2.735356 46.19693
20682 UG/LITER .8245004 .2446185 29.66870
19601 UG/LITER -11.0103 3.0099 27.33752
19602 UG/LITER -2.47692 .83270 33.61843
ftl ft2 #3
.8657056 .3821897 3.977076
-5.21989 -6.11237 -6.40411
21.10292 22.51917 22.72043
6.972186 7.974971 2.816075
.8540956 .5664307 1.052975
-13.0882 -12.3840 -7.55855
-2.47171 -1.64683 -3.31221
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 20.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -2.79858 .95765 34.21902
BI2230 UG/LITER 5.906715 1.200299 17.37873
MO2020 UG/LITER .2397181 .2606995 108.7525
TI3349 UG/LITER 3.698330 2.047577 56.90364
B_2496 UG/LITER 4.865386 .641290 13.18066
Y_3710 PPM 1175.400 6.697 .5697847
ftl tt2 tt3
-1.93706 -2.62898 -3.82969
8.201680 6.687040 5.831427
.4599954 -.048108 .3072664
1.293938 4.292374 5.208679
5.433630 4.992455 4.170075
1179.267 1179.267 1167.667
ERRORS VALUE RANGE
NOCHECK
NOCHECK
NOCHECK
NOCHECK
QC PASS .OOOOOOO 200.0000
NOCHECK
195
198 ANALYSIS REPORT
QC STANDARD
08/08/10 07:46:46 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSAB RUN TIME: 08/08/10 19:39:49 COMMENT: ICSAB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 205.4485 .5656 .2753130
AL3082 UG/LITER 256495.0 584.8 .2280073
BA4934 UG/LITER 626.6891 .9434 .1791163
BE3130 UG/LITER 504.4356 1.1640 .2307591
CA3179 UG/LITER 256531.8 940.8 .3667408
CD2265 UG/LITER 1014.987 2.394 .2358436
C02286 UG/LITER 514.4737 1.6320 .3172098
ftl #2 #3
204.8332 205.5665 205.9458
255919.5 256476.9 257088.7
525.7605 526.6602 627.6466
503.4528 504.1330 505.7211
257332.4 256495.6 256767.6
1013.152 1014.114 1017.695
612.7352 514.7134 515.9727
ERRORS VALUE RANGE
QC PASS 210.0000 43.00000
QC PASS 248400.0 50922.00
QC PASS 475.0000 400.0000
QC PASS 482.0000 98.00001
QC PASS 234300.0 48031.00
QC PASS 916.0000 187.0000
QC PASS 455.0000 100.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 555.2875 2.4786 .4453567
CU3247 UG/LITER 540.2698 .7038 .1302676
FE2714 UG/LITER 103071.9 341.0 .3308833
K_7664 UG/LITER 3.237045 2.358189 72.85003
MG2790 UG/LITER 270930.5 729.6 .2692888
MN2576 UG/LITER 527.2399 1.2035 .2282567
NA3302 UG/LITER 983.1145 96.2981 9.795201
ftl #2 ft3
562.9561 555.0174 557.8901
539.5098 540.8991 540.4004
102775.2 102996.1 103444.5
5.428581 .7416589 3.640897
270240.9 270866.1 271694.4
526.2149 526.9397 528.5650
1090.561 904.5965 954.1862
ERRORS VALUE RANGE
QC PASS 506.0000 103.0000
QC PASS 537.0000 110.0000
QC PASS 95100.00 19495.00
QC PASS .OOOOOOO 2000.000
QC PASS 254100.0 52090.00
QC PASS 483.0000 99.00000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1057.733 4.558 .4309039
TL1908 UG/LITER 99.40144 2.74641 2.762944
V_2924 UG/LITER 519.8368 1.5865 .3051824
ZN2138 UG/LITER 1052.778 3.176 .3016316
PB2203 UG/LITER 64.39046 1.22150 1.897025
SE1960 UG/LITER 46.10171 2.30500 4.999809
SB2068 UG/LITER 631.4792 4.8740 .7718323
ftl ft2 #3
1053.772 1056.714 1062.715
96.95108 98.88318 102.3701
519.2872 518.5982 521.6249
1049.662 1052.663 1066.010
63.11429 64.60834 66.54875
47.93643 46.85418 43.51451
626.7456 631.2077 636.4832
ERRORS VALUE RANGE
QC PASS 930.0000 190.0000
QC PASS 96.00000 50.00000
QC PASS 481.0000 99.99999
QC PASS 976.0000 199.0000
QC PASS 51.00000 20.00000
QC PASS 51.00000 70.00000
QC PASS 585.0000 120.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 103.0937 1.1897 1.154002
22031 UG/LITER 49.51447 3.31111 6.687162
22032 UG/LITER 71.80637 .47970 .6680456
20681 UG/LITER 629.5228 3.0957 .4917612
20682 UG/LITER 632.4499 5.7628 .9111901
19601 UG/LITER 40.65949 1.47040 3.616387
19602 UG/LITER 48.80823 2.72217 5.577282
#1 #2 ft3
104.4672 102.3812 102.4328
46.68182 48.85638 53.10621
71.35721 72.31167 71.75024
626.4795 629.4206 632.6685
626.8737 632.0935 638.3827
41.78909 41.19247 38.99692
50.99499 49.67030 45.75940
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
97.00000 20.00000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER 1007.641 1.133 .1124241
BI2230 UG/LITER 1050.262 2.957 .2815906
MO2020 UG/LITER 1011.536 6.773 .6695505
TI3349 UG/LITER 1029.017 4.641 .4510561
B_2496 UG/LITER 1037.853 5.481 .5280663
Y_3710 PPM 1169.911 1.038 .0887071
ttl #2 tt3
1008.948 1006.940 1007.035
1046.869 1051.622 1052-295
1005.788 1009.818 1019-003
1025.096 1027.812 1034.142
1032.487 1037.631 1043.441
1169.800 1171.000 1168.933
ERRORS VALUE RANGE
QC PASS 1000.000 205.0000
QC PASS 1000.000 205.0000
QC PASS 1000.000 206.0000
QC PASS 1000.OOO 206.0000
QC PASS 1000.000 200.0000
NOCHECK
196
199 ANALYSIS REPORT
QC STANDARD
08/08/10 07:53:47 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCVl RUN TIME: 08/08/10 19:46:50 COMMENT: CCV CVSl MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 101,4251 .8401 .8283016
AL3082 UG/LITER 50796,35 21.56 .0424419
BA4934 UG/LITER 1022,586 .606 .0592298
BE3130 UG/LITER 1016.995 .825 .0811176
CA3179 UG/LITER 49688.40 248.08 .4992669
CD2265 UG/LITER 1008.491 .593 .0587604
C02286 UG/LITER 1003.911 .926 .0922060
ftl «2 #3
100.6645 101.2839 102.3268
50811.04 50771.60 50806.41
1023.212 1022.003 1022.544
1016.645 1016.403 1017,937
49595.35 49500.30 49969.55
1009.134 1007.966 1008.374
1004.923 1003.702 1003,107
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1017.052 .376 .0369328
CU3247 UG/LITER 1020.032 .475 .0465872
FE2714 UG/LITER 25646.07 24.54 .0956853
K_7664 UG/LITER 49127.27 66.18 .1347154
MG2790 UG/LITER 51508.30 29.69 .0576427
MN2676 UG/LITER 999.1033 .4267 .0426037
NA3302 UG/LITER 50622.30 103.86 .2051708
ttl «2 tf3
1017.343 1017.184 1016.628
1020.015 1020.515 1019.565
25673.71 25637.68 25626.83
49202.71 49100.12 49078.98
51532.67 51475.23 51517.00
999.2971 998.6153 999.3977
50562.34 50562.33 50742.23
ERRORS VALUE RANGE
QC PASS 1000.OOO 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 60000.00 5200.000
QC PASS 1000,000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1017.474 1.705 .1675571
TLI908 UG/LITER 1018.324 4.966 .4876250
V_2924 UG/LITER 1025.822 ,532 .0518669
ZN2138 UG/LITER 1090,512 .663 .0607656
PB2203 UG/LITER 1007.040 .831 .0824883
SE1960 UG/LITER 1011,631 1.614 .1595403
SB2068 UG/LITER 1033.650 1.404 .1358048
ftl ft2 #3
1018.967 1017.837 1015.616
1024.021 1014.913 1016.038
1026.406 1025.366 1025.693
1090.718 1089.771 1091.048
1006.084 1007.448 1007.587
1012,413 1012,704 1009.774
1032,851 1032.828 1035.271
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114,0000
QC PASS 1000.000 104,0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104,0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1023.931 1.648 ,1609166
22031 UG/LITER 997.1768 2.3816 .2388367
22032 UG/LITER 1011.948 .362 .0358170
20681 UG/LITER 1028,010 1,881 ,1830041
20682 UG/LITER 1036,462 1,392 ,1343122
19601 UG/LITEK 1004.720 4,259 .4239109
19602 UG/LITER 1015.071 ,308 .0303034
ftl #2 ft3
1025,220 1022.074 1024.497
994.4881 999.0216 998.0205
1011.858 1011.640 1012.348
1026.111 1028.046 1029.873
1036,213 1035.211 1037.962
1006.966 1007.386 999.8081
1015.123 1015.349 1014.740
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1012.243 3.804 .3768441
BI2230 UG/LITER 1019.615 5.898 .5784330
MO2020 UG/LITER 1029.694 .675 .0655207
TI3349 UG/LITER 1022.755 1.666 .1629363
B_2496 UG/LITER 1036.107 1.571 .1516344
Y_3710 PPM 1216.378 1.776 .1469712
ftl ft2 «3
1008.275 1015.859 1012,594
1016.922 1015.545 1026.379
1029.380 1030.468 1029.233
1020.043 1023.899 1023.624
1036.973 1034.294 1037.055
1216,933 1218,333 1214.867
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
197
200 ANALYSIS REPORT
QC STANDARD
08/08/10 08:00:48 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCBl RUN TIME: 08/08/10 19:53:51 COMMENT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.064890 .495286 763.2720
AL3082 UG/LITER -2.93622 7.67663 261.4116
BA4934 UG/LITER -.305800 .025703 8.405281
BE3130 UG/LITER .1669345 .0462185 27.68663
CA3179 UG/LITER -653.066 329.585 50.46740
CD2265 UG/LITER .3818133 .1067039 27.94663
C02286 UG/LITER .3074343 .0565117 18,38170
ttl #2 #3
-.533796 .4531187 -.113992
1.906796 -11.7861 1.070663
-.333811 -.283296 -.300295
.2150007 .1228170 .1629857
-987.356 -328.396 -643.445
.2862141 .4969280 ,3622977
.2484672 ,3127162 ,3611197
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS ,0000000 5000,000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .3794213 .2502646 65.95956
CU3247 UG/LITER .3958108 .1856096 46.89351
FE2714 UG/LITER 1.586792 6.438947 405.7839
K_7664 UG/LITER 3.255306 2.041442 62.71122
MG2790 UG/LITER 15,82502 1.61327 10.19445
MN2576 UG/LITER -.000555 .033139 5972.669
NA3302 UG/LITER -39.7409 69.0303 148,5379
ftl #2 #3
.1527660 .6480001 .3374980
.2256120 .5937162 .3681042
-5.83014 6.744614 4.846007
4.182872 4.568276 .9147701
14.10008 17,29667 16,07830
-.004440 ,0343554 -.031580
-104.236 -26.5946 11.60792
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 6000.000
QC PASS .OOOOOOO 6000.000
QC PASS .OOOOOOO 10,00000
QC PASS .OOOOOOO 5000,000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER .4423564 .0704286 15.92123
TL1908 UG/LITER 3.649344 3,657803 100.2318
V_2924 UG/LITER -.103853 .344672 331.8852
ZN2138 UG/LITER .0795255 .0127817 16.07250
PB2203 UG/LITER .2395099 .7547510 315.1231
SE1960 UG/LITER .2059933 1.653266 754.0366
SB2068 UG/LITER .4087967 .8540993 208.9306
ftl #2 #3
.4253326 .6197365 .3820001
2.288390 .8671091 7.792534
-.247789 .2894574 -.353227
.0719440 .0942827 .0723498
-.354475 1.088803 -.015798
1.120476 -1.58744 1.084949
-,062458 -,106862 1,394706
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS ,0000000 10,00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.456076 .646193 138.6464
22031 UG/LITER .7231701 1.226569 169.6100
22032 UG/LITER -.011822 1.035937 8752.543
20681 UG/LITER 2.064677 .879166 42.58128
20682 UG/LITER -.427768 .843302 197.1398
19601 UG/LITER -2.74064 4.62645 168.8090
19602 UG/LITER 1,567239 1,998339 119,8692
ftl #2 tt3
.0236116 -1.19851 -.223229
1.257901 1.591594 -.679986
-1.16939 .8280864 .3058411
1.646269 1.472860 3.074901
-.925480 -.903737 .5459117
-4.60129 -6.14709 2.526449
3,967130 .6792630 .3553234
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1.123612 2.116559 188.2819
BI2230 UG/LITER .8811096 2.469091 280.2252
MO2020 UG/LITER 2.454969 .802422 32.68563
TI3349 UG/LITER 2.100188 4.447256 211.7551
B_24 96 UG/LITER 4.188875 .597505 14.26408
Y_3710 PPM 1238.911 18.003 1.453106
#1 #2 ft3
-1.31909 2.322510 2.367414
-.429248 -.656671 3.729148
3.376243 2.079909 1.908757
-2.32032 6.573714 2.047174
4.809046 4.140616 3.616964
1229.533 1259.657 1227,533
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 60.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
198
201
Maintenance:
Daily Instrument Profile Nebulizer pressure: ^ Peak position: - . O C > o 3 < ^ Peak intensity: • = ^ ^ f o R « r ^ Vernier position: I'gjC*
H^ts^g
Printed: 8/11/2010 9:09:55 AM Method{s) (circle one): ULM05.4 ) 6010B 0perator(s):
RR RR#X #X
6010C
/^^^Kr\
Otiier
Datemme O f t . \ o . i o lo.^CtfT
Specified element(s) fail(s) high Specified elementfs) fail(s) low Re-run sample(s) neat Re-run ata #-fold dilution Sample run at a #-fold dilution (aliquot of sample diluted with acidified water) Matrix = leachate Vlatrix = water Vlatrix = solid Vlatrix = biological tissue
SDG 1007182 MC0022 MG68M3
Matrix
MY71N3 MY71S3 MY71S4
O^.loi^ 7 ^ ( 1 ^
COPY '^a.13.
Comments
MPt^lvsr
7^U
^
"
TAL-
TAU t^L.
E Z ^ £ ^.>1 1A i\CA.,fe,yu,icVN^^
H
(M
^
rt^_A-fey^^^ \'^0'^^^^ C^HP{.¥y]^ GL
cyoH^^y^jS.
ICP Run Log (P3) File Name: P30810 Seq
Client ID
DF
Date
1
08/10/10
10:35:39
CALIB STD
08/10/10
10:42:40
S RSTD-3
CALIB STD
08/10/10
10:49:40
CAL3
S RSTD-2
CALIB STD
08/10/10
10:55:07
5
CALS
S RSTD-4
CALIB STD
08/10/10
11:00:35
6
ICVl
ICVl
ICV
08/10/10
11:07:36
7
ICBI
ICB
ICB
08/10/10
11:14:37
8
CRLI
CRI
CRI
08/10/10
11:21:37
9
IFA1
ICSA
ICS
08/10/10
11:28:37
10
IFB1
ICSAB
ICS
08/10/10
11:35:38
11
CCVl
CCV
CCV
08/10/10
11:42:39
12
CCB1
CCB
CCB
08/10/10
11:49:40
13
LRS
LRS
LRS
08/10/10
11:59:09
14
1007156-02RE1
MY71N4
SAMPLE
08/10/10
12:06:10
Sample ID
Sample Type
1
CALI
SO BLANK
CALIB STD
2
CAL2
S RSTD-1
3
CAL4
4
10
Time
SDG
Action Needed
MY71N3
The presence of the Chemisfs/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP fias occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials of the lab supervisor and a QA department representafive, signifying approval of the deviation.
Reviewed By :
^ . OtQ^>-wt>
Date:
Y-11-/0
Page 1 of 4
199
202
ICP Run Log (P3) File Name: P30810 Seq
Client ID
Sample ID
Sample Type
DF
Date
Time
SDG
15
1007156-05RE1
MY71N7
SAMPLE
3
08/10/10
12:14:48
MY71N3
16
1007159-O7RE1
MY71T6
[SAMPLE
2
08/10/10
12:21:49
MY71S4
17
0080607-DUPl
MY71T6D
SAMPLE
2
08/10/10
12:28:49
MY71S4
18
SRD1
MY71T6L
SAMPLE
19
1007159-lOREl
MY71W0
SAMPLE
2
08/10/10
12:45:12
MY71S4
20
1007159-12RE1
MY71X0
SAMPLE
2
08/10/10
12:52:12
MY71S4
21
1007159-13RE1
MY71X2
SAMPLE
2
08/10/10
12:59:12
MY71S4
22
1007157-lOREl
MY71W1
SAMPLE
2
08/10/10
13:06:12
MY71S3
23
CCV2
CCV
CCV
1
08/10/10
13:13:13
24
CCB2
CCB
CCB
1
08/10/10
13:20:15
25
1007157-12RE1
MY71W9
SAMPLE
2
08/10/10
13:28:50
MY71S3
26
1007157-13RE1
MY71X1
SAMPLE
2
08/10/10
13:35:50
MY71S3
27
CRL2
CRI
CRI
08/10/10
13:42:50
28
IFA2
ICSA
ICS
08/10/10
13:49:51
29
IFB2
ICSAB
ICS
08/10/10
13:56:51
30
CCV3
CCV
CCV
08/10/10
14:03:52
31
CCB3
CCB
CCB
08/10/10
14:10:53
32
0080620-BLK1
PBS
PBS
08/10/10
14:17:54
1007182
33
0080620-BS1
LCSS
LCS
08/10/10
14:24:55
1007182
34
1007182-04
Q4-SB3-S 5
SAMPLE
08/10/10
14:33:15
1007182
35
0080620-DUP1
Q4-SB3-S 5D
SAMPLE
08/10/10
14:40:15
1007182
36
0080620-MS1
Q4-SB3-S 5S
SAMPLE
08/10/10
14:47:16
1007182
37
SRD2
Q4-SB3-S 5L
SAMPLE
08/10/10
14:54:16
1007182
38
0080620-PS1
Q4-SB3-S 5A
SAMPLE
08/10/10
15:01:16
1007182
39
1007182-01
Q4-SB1-S 8
SAMPLE
08/10/10
15:10:41
1007182
[40
1007182-02
Q4-SB2-S 6
SAMPLE
08/10/10
15:17:42
1007182
41
1007182-03
Q4-SB2A-S 6
SAMPLE
08/10/10
15:24:42
1007182
42
CCV4
CCV
CCV
08/10/10
15:31:43
43
CCB4
CCB
CCB
08/10/10
15:38:44
44
0080327-BLKl
PBS
PBS
08/10/10
15:45:45
MG68M3
45
0080327-BSl
LCSS
LCS
08/10/10
15:52:45
MG68M3
46
1008002-07
MG68M9
SAMPLE
08/10/10
15:59:45
MG68M3
1 Action Needed
1 10 08/10/10 12:38:12 MY71S4
5
:
R«L \
i
The presence of the Chemist's/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials of the lab sup>ervisor representative, signifying approval of the deviation. sup>ervisor and and a a QA QA department depart
Reviewed By :
^-
,40"MVS
Date:
J-^/v^
Page 2 of 4
200
203 ICP Run Log (P3) File Name: P30810 Seq
Sample ID
47 p080327-DUP1
1 48
|0080327-MS1
I Client ID
1 ^^
1 Sample Type
|MG68M9D
SAMPLE
|MG68M9S
1 SAMPLE
Date
Time
SDG
08/10/10
16:06:45
MG68M3
08/10/10
16:13:45
MG68M3
08/10/10
16:20:45
MG68M3 MG68M3
Action Needed
L?.»^
49
SRD3
MG68M9L
SAMPLE
50
0080327-PSl
MG68M9A
SAMPLE
08/10/10
16:27:46
51
CRL3
CRI
CRI
08/10/10
16:34:46
52
IFA3
ICSA
ICS
08/10/10
16:41:46
53
IFB3
ICSAB
ICS
08/10/10
16:48:47
54
CCV5
CCV
CCV
08/10/10
16:55:48
55
CCB5
CCB
CCB
08/10/10
17:02:49
56
1008002-01
MG68M3
SAMPLE
08/10/10
17:09:50
MG68M3
57
1008002-02
MG68M4
SAMPLE
08/10/10
17:16:51
MG68M3
58
1008002-03
MG68M5
SAMPLE
08/10/10
17:23:51
MG68M3
59
1008002-04
MG68M6
SAMPLE
08/10/10
17:30:51
MG68M3
60
1008002-05
MG68M7
SAMPLE
08/10/10
17:37:52
MG68M3
61
1008002-06
MG68M8
SAMPLE
08/10/10
17:44:52
MG68M3
62
1008002-08
MG68N0
SAMPLE
08/10/10
17:51:52
MG68M3
63
0080337-BLKl
PBS
PBS
08/10/10
17:58:52
MC0022
64
0080337-BSl
LCSS
LCS
08/10/10
18:07:54
MC0022
65
1008009-03
MC0024
SAMPLE
08/10/10
18:14:54
MC0022
66
CCV6
CCVl
CCV
08/10/10
18:21:55
67
CCB6
CCBl
CCB
08/10/10
18:28:56
0080337-DUPl
MC0024D
SAMPLE
08/10/10
18:35:56
MC0022
69
0080337-MSl
MC0024S
SAMPLE
08/10/10
18:42:56
MC0022
70
SRD4
MC0024L
SAMPLE
08/10/10
18:49:56
MC0022
0080337-PSl
MC0024A
SAMPLE
08/10/10
18:56:57
MC0022
72
1008009-01
MC0022
SAMPLE
08/10/10
19:03:57
MC0022
73
1008009-02
MC0023
SAMPLE
08/10/10
19:10:58
MC0022
1008009-04
MC0025
SAMPLE
08/10/10
19:17:58
MC0022
CRL4
CRI
CRI
08/10/10
19:32:36
h
1 68
1 ^^ [74 75 76
IFA4
5
-|
ICSA
ICS
08/10/10
19:39:36
1 ^^
IFB4
ICSAB
ICS
08/10/10
19:46:36
I 78
CCV7
CCVl
CCV
08/10/10
19:53:37
-L
11
1
1
The presence of the Chemisfs/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP has occun'ed. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemisfs/analysf s initials and the initials of the lab supervisor and a QA department representative, signifying approval of the deviation.
Reviewed By:
Jc^ . jtP^wWQ-
Date:
T'nyi7
Page 3 of 4
201
204 ICP Run Log (P3) File Name: P30810 Seq 79
CCB7
Sample ID
Client ID CCBl
Sample Type CCB
80
1008009-05
MC0026
SAMPLE
DF 1
Date Time 08/10/10 20:00:38
SDG
1
08/10/10 20:20:26 MC0022
Action Needed
The presence of the Chemisfs/Analyst's employee ID number, or signature, on this mn log attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analysfs initials and fhe initials of the lab supervisor grid a QA department representative, signifying approval of the deviation.
Reviewed By:
Jl-
^s
Date:
t/yo
Page 4 of 4
202
205 CO
o
CM
D a i l y S t a n d a r d s / Q C P r e p a r a t i o n L o g f o r T r a c e I C P ( P 3 & P 4 ) 1 ofS CompuChem a division of UbertyAnaiyticalCorp. worksheet l P(6) 2
STANDARDS and REAGENTS TRACEABILITY
Seq. File Name: Refr
HNOs [Baker Instra-analyzed Trace-Metals grade] HCI [Baker Instra-analyzed Trace-Metals grade] SM-770-027 multi-element standard mix (RSTD-1) SM«770-028 partA multi-element standard mix (RSTD-2A) SM-770-028 part B multi-element standart mix (RSTD-2B) SM«770-029 piart A multi-element standanj mix (RSTD-3A) SM-770-029.part B multi-element standard mix (RSTD-3B) SM-770-030 multi-element standard mix (RSTD-4) SPEX-R muttl-element standard mix ICP-AES-CRQL-R multi-element standard mix ICV1 multi-element standard mix ICSA multi-element standard mix ICSB multi-element standard mix SM-770-031 multi-element standard mix (PDS-R) ARSENIC (As) 1,000 PPM single-element standard Intemat Mix SM-770-040 multi-element CCV mix (Soln A) SM-770-040 multi-element CCV mix (Soln B) $M.770-042 (LRS 601 OB)
O C3^ { 2 O I O
0F12002 9J22002 9J22001 0D14008 9G08005 OFI2003 OF12001 9104002 0B04003 OB04002 0BO4001 9122001 9F17001 OB04004 0E03001 0E03001 0B23007
'Y'^O^ I Q
Manufacturer Manufact JT Baker Caledon HlQh Purity High Puritv High Purity High Puritv High Puritv High Purity High Purity High Puritv EPA EPA EPA High Puritv High Puritv High Puritv High Purity High Purity High Purity
Lot# " ^ ^ 0
3-*^
1015827 0928011 0928012 0925430 0906204 1015830 1015828 0923808 0307 1206 0203 0926418 0911221 0934101 1010910 1010911 1004021
Expiration Date OPr .
Multi-Element Stock Standard Concentrations: RSTD-1 multi-element standard mix RSTD-2A/2B multi-element standard mix RSTD-3/\/3B multi-element standard mix RSTD-4 multi-element standard mix SPEX-R multi-element standard mix ICP-AES-GRQL-R multi-element standard mix PDS-R multi-element standard mix Intemal Mix LRS 601 OB multi-element standard mix
Al:20 Sbri As:1 Ba:20 Be:0.5 Bl:2 B:2 Cd:0.5 Ca:500 Cni Co:0.5 Cu:0.5 FerlO PbrO.3 MgrSOO Mnri Mo:2 Nl:0,5 KrSOO SerO.5 TIrO.5 Vr2 Znr2
IrUvjtJt^
Entered By: Revievyed By
Cd:1.000 CrI.OOO Cu:1.000 Pb:1,000 Nl:1,000 Se:1,000 Ag:l00 Tl:1.000 2n:1.000 PartA:/\8:1,000 Ba:1.000 Be:1,000 Co:1,000 Mn:1.000 Mo:1,000 V:1,000 Part B: Fe:25,000 PartA: Ca:10,000 MgrlO.OOO K:10,000 Na:10,000 Part B:A1:10.000 Sb:1.000 Bhl.lJOO 8:1,000 Snrl.OOO Tlr1,000 Mo:1,000 Snrl.OOO Bin,000 Tl:1,000 BrI.OOO AgrlO BerS CdrS CorSO Cr10 Cur25 Mn:15 N1.40 Tlr25 VrSO Zrir60 PbrlO Ser35 AsrIO SbrOO Al:400 Ba:400 Agr20 Be:10 CdrlO CorlOO Cr:20 Cu:50 Fe:200 Mn:30 Nl:80 Tl;20 V:100 Zn:40 Pb:6 Se:10 As:20 Sbri 20 Llr50,000 Yr250
_
*Ref# « Logbook 10, Page number, and Item number from Materials Receipt Log "High Purity is abbreviated "HP* on reporting fonns
: ^-//-/J
Date
03/25/1 Or Jcf
206 o CM
Dally Standards/QC ^ r e p a r a t i o n L o g f o r T r a c e I C P ( P 3 & P 4 ) 3 of 3 CompuChem a division ofLiberty Analytical Corp. Worksheet 1 P(6) 2
AS-
o&.cegjo^^g^H
ICSA- O f c . t P C * . .
ICSAB-
l O - ^ ^ H
Ogj.pW.jO-ej^V^
c:>i^o<:p
C>M-C3(pOl-4-
OW
EPA-CRI- O & . o C p . l O - ^ Z i e f ^
CH-hoCeoo ^
P3RINSE- C?g>.|C?.| -
OH-
^
H
P4RINSE- C?gp^
l O . l o ^ n
P5R1NSE-
H^
l o o o ^
CPHlQ 0 0 ^
HA
In a 100 mL volumetric flask, combine 50 mL delonlzed water, 1 mL concentrated HNO3, 5 mL concentrated HCI, and 0.1 mL 1000-ppm As standard. Bring to final 100 mL volume Iri a 500-mL volumetric flask, combine 350 mL deionized water, 5 mL concentrated HNO3, and 25 mL concentrated HCI. Pipet 50.0 mL ICSA Into flask. Bring up to volume with delonlzed water and transfer to a SOOmL Teflon bottle. Final volume 500 mL.
As:1,000 Al:244.100 Ba:2 Car234,900 Co:4 Cr:43 Cu:23 Fe:95,600 Mg:247,500 Mn;19 Nl;21 Zn:28 PbrlO
In a 500-mL volumetric flask, combine 350 mL deionized water, 5 mL concentrated HNO3, and 25 mL concentrated HCI. Pipet 50.0 mL ICSA and 50.0 mL ICSB Into flask. Add 0,5 mL Compuchem SPEX-R. Bring up to volume with deionized water and transfer to a 500mL Teflon bottle. Final volume 500 mL.
Agr206 Al:241,100 Ba:495 Be:475 Ca:231,100 Cd:940 Co:461 Crr511 Cur548 Fe:94,800 Mg:251,100 Mn;502 Ni:984 Tl:103 V:494 Zn:1028 Pb:61 Se:53 Sbr589 AsilOI Sn:1,000 81:1,000 Mo:1,000 Till,000 BrI.OOO
In a 500 mL volumetric flask, combine 300 mL deionized vrater, 5 mL concentrated HNO3, and 25 mL concentrated HCI. Pipet 0.50 mL ICP-AESCRQL-R and 25 pL Compuchem SPEX-R into flask. Bring up to volume with delonlzed water and transfer to a SOOmL Teflon bottle, Final volume 500 mL. Prepare as needed.
AgrlO Mnri5 Ser35 BIrSO
BerS CdrS CorSO Cr:10 Cur25 Nl:40 Tl:25 VrSO Znr60 PbrlO AsrIO Sbr60 Snr50 BrSO MorSO TIrSO
In a IOL container, combine 8 L deionized water and 400 mL concentrated HNO3 Fill with deionized water. Final volume 10 L.
N/A
In a 10 L container, combine 8 L deionized water and 400 mL concentrated HNO3 Fill with deionized water. Final volume 10 L.
N/A
In a 10 L container, combine 8 L deionized water and 400 mL concentrated HNO3 Fill with deionized water. Final volume 10 L.
N/A
P3INTSTD- (J^ X - ^ \ 0 - ^ ( ^ \ - \ O C ^ ^ ' ^ O O ^
In a 10 L container, combine 8 L deionized vrater, 400 mL concentrated HNOs, and 200 mL Internal Mix. Fill with delonlzed water. Final volume 10 L.
Ll:1,000,000
Yr5,000
P4INTSTO- e ? 5 . \ O . \ 0 - 5 ^ U , 0 K \ 0 O O q —
In a 10 L container, combine 8 L delonlzed vrater, 400 mL concentrated HNO3, and 200 mL Internal Mix. FIII with delonlzed vrater. Final volume 10 L.
Ll:1,000,000
Y:5,000
In a 10 L container, combine 8 L deionized water, 400 mL concentrated HNO3, and 200 mL Intemal Mix. Fill w/lth deionized water. Final volume IOL.
Li:1,000,000
YrS.OOO
P5INTSTD-
U
N ^
Standard Solutions Pn Entered By: _
f P/VK-^J
Reviewed By: •Standard Lot Number consists of standard ID, date prepared, and initials of preparer.
Date
: y / -/6 ~ 03/25/10: jcf
207
o CM
D a i l y S t a n d a r d s / Q C P r e p a r a t i o n L o g f o r T r a c e I C P (P3 & P4) 2of3 compuChem a division of Liberty Analytical corp. worksheet i p(6) 2
SO/ICB/CCB-e^,Olp.|£,.^,l
RSTD-1-
^ ^ ^ . o ^ . \ o - ' 5 ^ v ^ ^H-^C^! tpcfS.
RSTD.2-0£>.
(D^oica \ : ^
OH-0^(003
^r^&.oS^.io-fxs^K/^O-H-ofpCJo^
RSTD-4- C3^,0«5 . I O - S ^ ^ \ O H T O ^ O O S "
ICV1-
ogp.o^jo ' ^ t \
CCV/CVS1- o e 7 . < p ^ . l c y ^ t J \
LRS- c ? : f . 5 \ . l O ' - ' ^ « - A
C>\+-o<^oa \
Entered By:
N/A
In a 200 mL volumetric flask, cornbine 150 mL deionized vrater, 2 mL concentrated HNO3, and 10 mL concentrated HCI. Pipet 0.4 mL RSTD-1 Into flask. Bring up to 200 mL volume with delonlzed vrater. Prepare as needed,
Cd:2,000 Cr:2,000 Cu:2,000 Pb:2,000 Nl:2,000 Ser2,000 Agr200 Tl:2,000 Znr2,000
In a 200 mL volumetric flask, combine 150 mL deionized water, 2 mL concentrated HNO3. and 10 mL concentrated HCI, Pipet 0.4 mL each RSTD-2A and RSTD-2B into flask. Bring up to 200 mL volume with delonlzed water. Prepare as needed. In a 200 mL volumetric flask, combine 150 mL deionized vrater, 2 mL concentrated HNO3. and 10 mL concentrated HCI. Pipet 2,0 mL each RSTD-3A and RSTD-3B into flask. Bring up to 200 mL volume with deionized vrater. Prepare as needed. In a 200 mL volumetric flask, combine 150 mL deionized water, 2 mL concentrated HNO3, and 10 mL concentrated HCI. Pipet 0.4 mL RSTD-4 into flask. Bring up to 200 mL volume virtth deionized vrater. Prepare as needed.
Place in a 500 m l volumetric flask: 300 mL deionized vrater, 5 mL concentrated HN03,and 25 mL concentrated HCI. Pipet 50.0 mL 1CV1 Info flask and 0.55 mL Compuchem SPEX-R. Bring up to volume vwth deionized vrater. Transfer to a SOOmL Teflon bottle. Final volume 500 mL. Prepare as needed.
Place In a 500-mL volumetric flask; 300 mL deionized water, 20 mL concentrated HNOs.and 100 mL concentrated HCI. Add 50 ml of SM-770-40 Soln A and Soln B, Bring up to volume with deionized vrater. Transfer to a 2000mL Teflon bottle and add 1.5 L of delonlzed water. Prepare as needed.
OhV-C>(cO|
C7
Standard Solutions Prepared By:
Place In a 500 mL volumetric flask: 100 mL deionized vrater, 20 mL concentrated HNO3, and 100 mL concentrated HCI. Bring up to volume with delonlzed vrater. Transfer to a 2L Teflon bottle and add 1.5L deionized water. Final volume 2 L. Prepare as needed.
In a 500 mL volumetric flask, combine 200 mL deionized vrater, 5 mL concentrated HNOsand 25 mL concentrated HCI. Pipet S.OmL of LRS 601 OB. Bring up to volume with deionized water and transfer to a SOOmL Teflon bottle. Final volume SOO mL. Prepare as needed.
f^-.2.00Q Bar2,000 Be:2,000 Co;2,000 FerSO.OOO Mn:2,000 Mo:2,000 V:2.000 KrIOO.OOO Na:100,000 AlrlOO.OOO Mg: 100,000 Ca: 100,000 Sn:2,000 Bi:2,000 Tl:2,000 Sb:2,000 B:2,000
Al:2,521 Ba:497 K:10,021 Mg:6,074 Narl 0,097 Ca:10,026 AgrSOl Be:495 Cd:498 Co:499 Cr:490 Cu:492 Fe:5,082 Mnr499 NlrS03 Tl:1,028 V:S01 2n:1,025 Pb:1002 Se:1,029 As:999 Sb:994 Mo:1,100 Sn:1,100 Bl:1,100 Tl:1,100 B:1,100 AlrSO.OOO Ba:1,000 KrSO.OOO MgrSO.OOO NarSO.OOO Ca:50,000 Ag:100 Be;1,000 Cdrl.OOO Corl.OOO CrI.OOO Cu:1,000 Fe;25,000 Mn:1,000 Nlrl.OOO Tl:1,000 Vr1,000 Zn:1,100 Pbr1,000 Se:1,000 AsrI.OOO Mon.OOO Sn;1,000 BIrl.OOO Tlrl.OOO Sb:1,000 Br1,000 Al:200 Bar200 KrS.OOO Mg:5,000 NarS.OOO Car5,000 AgrS BerS CdrS Co:10 CrrlO Cu:5 FerlOO Mn:10 NIrS TIrlO Vr20 Zn:20 Pb:3 SerS AsrIO Mor20 Snr20 Blr20 Tlr20 Sbr10 Br20
f^M
.Vh^Oru-^^^u
Reviewed By: ^ ^Standard Lot Number consists of standard ID. date prepared, and initials of preparer.
Date:
^-My^ 03125110: ]c1
208 08/10/10 10:42:36 AM
STANDAPtDIZATION RPT.
PAGE 1
METHOD: ALT-P3Q3 STANDARD: SO BLANK RUN TIME: 08/10/10 10:35:39 ELEM AVGE SDEV %RSD
AG3280 -.26465 .00611 2.3086
AL3082 9.1549 .2382 2.6018
BA4934 .37974 .00724 1.9080
BE3130 1.9868 .0305 1.5329
CA3179 -.00012 .00046 397.42
CD2255 -.14023 .02202 15.701
C02286 -.01050 .01697 161.71
ttl »2 »3
-.25799 -.26999 -.26599
8.9248 9.4004 9.1395
.37861 .38749 .37313
1.9908 2.0151 1.9546
-.00038 -.00038 .00042
-.16090 -.14272 -.11708
.00267 -.00450 -.02966
ELEM AVGE SDEV %RSD
CR2677 -.00080 .00368 460.11
CU3247 .66230 .00723 1.0922
FE2714 .01502 .00962 64.043
K_7664 .42318 .05466 12.917
MG2790 .01249 .00281 22.526
MN2576 .00831 .00234 28.179
NA3302 -.39307 .02090 5.3163
#1 #2 #3
.00322 -.00161 -.00400
.66697 .66597 .65397
.01930 .02175 .00400
.38111 .48496 .40346
.01124 .01571 .01052
.00965 .00967 .00560
-.39478 -.37138 -.41307
ELEM AVGE SDEV %RSD
NI2316 -.00414 .00407 98.214
TL1908 -.03455 .00793 22.947
V_2924 -.02406 .00298 12.378
ZN2138 .01071 .00246 22.984
AS1890 -.11715 .08261 70.516
22031 .18352 .10727 58.451
22032 -.04805 .11839 246.41
#1 #2 #3
-.00831 -.00394 -.00018
-.02573 -.04109 -.03682
-.02441 -.02093 -.02685
.00804 .01289 .01121
-.19699 -.12245 -.03202
.23317 .06042 .25697
.07638 -.06122 -.15930
ELEM AVGE SDEV %RSD
20681 .00027 .00674 2496.0
20682 -.01458 .08274 567.53
19601 -.22409 .03509 15.660
19602 .22796 .03202 14.046
SNI899 -.01231 .02218 180.22
BI2230 -.08398 .05037 59.986
MO2020 .02316 .02834 122.35
#1 #2 #3
.00804 -.00403 -.00320
.04181 -.10956 .02402
-.24684 -.18367 -.24176
.23799 .25376 .19212
-.03538 .00886 -.01041
-.06593 -.04511 -.14089
.02434 -.00575 .05089
ELEM AVGE SDEV %RSD
T13349 .79051 .60653 76.727
B_2496 .24314 .02271 9.3393
#1 #2 #3
1,3170 .92723 .12728
.26614 .22073 .24256
206
209 0 8 / 1 0 / 1 0 1 0 : 4 9 : 3 6 AM
STANDARDIZATION R P T . METHOD: A L T - P 3 Q 3 RUN T I M E : 0 8 / 1 0 / 1 0
PAGE 1
STANDARD: S RSTD-1 10:42:40
ELEM AVGE SDEV %RSD
AG3280 24.602 .026 .10397
CD2265 652.06 .90 .13743
CR2677 35.304 .025 .06950
CU3247 170.28 .13 .07680
NI2316 31.755 .047 .14906
TL1908 13.309 .024 .17747
ZN2138 29.843 .020 .06708
#1 #2 #3
24.576 24.627 24.605
652.95 652.07 651.16
35.329 35.302 35.280
170.13 170.37 170.33
31.804 31.709 31.752
13.282 13.325 13.320
29.849 29.859 29.820
ELEM AVGE SDEV %RSD
22031 197.66 .02 .01071
22032 179.81 .13 .07353
19601 43.653 .133 .30581
19602 78.022 .147 .18787
#1 02 113
197.66 197.64 197.68
179.84 179.92 179.66
43.785 43.656 43.518
77.929 77.947 78.191
207
210 STANDARDIZATION RPT.
08/10/10 10:55:04 AM
PAGE 1
METHOD- AI.T-P3Q3 STANDARD: S RSTD-3 RUN TIME: 08/10/10 10:49:40 ELEM AVGE SDEV %RSD
AL3082 1845.0 21.9 1.1864
CA3179 .11914 .00126 1.0557
K_7664 687.39 6.41 .93212
MG2790 275.85 3.28 1.1903
NA3302 40.115 .381 .95052
#1 «2 tt3
1827.7 1837.8 1869.6
.11808 .11881 .12053
682.34 685.23 694.59
273.20 274.82 279.52
39.822 39.978 40.546
208
211 STANDARDIZATION RPT.
08/10/10 11:00:31 AM
PAGE 1
METHOD: ALT-P3Q3 STANDARD: S RSTD-2 RUN TIME: 08/10/10 10:55:07 ELEM AVGE SDEV %RSD
BA4934 359.64 .01 .00207
BE3130 1701.1 2.2 .13042
C02286 113.35 .13 .11222
FE2714 61.337 .052 .08448
MN2576 57.463 .044 .07635
V_2924 16.948 .020 .11939
AS1890 172.27 .07 .03916
#1 #2 #3
359.64 359.65 359.65
1698.5 1702.6 1702.0
113.38 113.47 113.22
61.334 61.391 61.287
57.457 57.509 57.422
16.948 16.969 16.928
172.21 172.34 172.27
ELEM AVGE SDEV %RSD
MO2020 136.21 .23 .16921
#1 #2 #3
135.95 136.32 136.37
209
212 STANDARDIZATION RPT.
08/10/10 11:07:32 AM
PAGE 1
METHOD: ALT-P3Q3 STANDARD: S RSTD-4 RUN TIME: 08/10/10 11:00:35 ELEM AVGE SDEV %RSD
20681 18.080 .066 .36483
20682 72.981 .102 .14008
SN1899 26.260 .064 .24515
BI2230 161.01 .17 .10509
TI3349 242.91 .28 .11477
B_2496 147.76 .29 .19475
#1 #2 #3
18.073 18.149 18.018
72.977 73.085 72.880
26.324 26.262 26.195
160.97 161.20 160.87
243.14 242.98 242.60
147.52 148.08 147.69
210
213 ANALYSIS REPORT
QC STANDARD
08/10/10 11:14:33 AM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICVl RUN TIME: 08/10/10 11:07:36 COMMENT: ICVl MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 504.0743 1.2619 .2503417
AL3082 UG/LITER 2547.653 15.636 .6137572
BA4934 UG/LITER 505.0473 2.4596 .4870020
BE3130 UG/LITER 491.1705 1.9014 .3871162
CA3179 UG/LITER 10223.87 626.67 6.129518
CD2265 UG/LITER 501.3218 1.8278 .3645928
C02286 UG/LITER 505.3174 2.1640 .4282539
ftl #2 #3
502.6290 504.6360 504.9577
2554.975 2558.285 2529.699
505.7289 507.0942 502.3188
490.9055 493.1905 489.4155
9584.372 10250.35 10836.88
501.3813 503.1191 499.4650
505.2500 507.5144 503.1879
ERRORS VALUE RANGE
QC PASS 501.0000 10.40000
QC PASS 2521.000 10.40000
QC PASS 497.0000 10.40000
QC PASS 495.0000 10.40000
QC PASS 10026.00 10.40000
QC PASS 496.0000 10.40000
QC PASS 499.0000 10.40000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 500-6569 3.1560 .6303750
CU3247 UG/LITER 508.2271 .4567 .0898621
FE2714 UG/LITER 5039.582 27.651 .5486752
K_7 664 UG/LITER 9680.185 46.964 .4851544
MG2790 UG/LITER 5897.994 24.350 .4128562
MN2576 UG/LITER 491.8404 2.1334 .4337581
NA3302 UG/LITER 10054.32 100.81 1.002609
ttl #2 #3
501.2844 503.4521 497.2343
507.7004 508.5140 508.4668
5047.331 5062.531 5008.883
9707.303 9707.295 9625.955
5905.842 5917.452 5870.687
492.1146 493.8234 489.5831
9943.722 10141.05 10078.18
ERRORS VALUE RANGE
QC PASS 490.0000 10.40000
QC PASS 492.0000 10.40000
QC PASS 5082.000 10.40000
QC PASS 10021.00 10.40000
QC PASS 6074.000 10.40000
QC PASS 499.0000 10.40000
QC PASS 10097.00 10.40000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 507.7484 1.2575 .2476582
TL1908 UG/LITER 1040.102 4.334 .4166982
V_2924 UG/LITER 504.7283 1.5871 .3144370
ZN2138 UG/LITER 982.2358 4.6993 .4784267
PB2203 UG/LITER 1008.627 5.614 .5565682
SE1960 UG/LITER 1003.316 3.914 .3900697
SB2068 UG/LITER 1013.915 4.248 .4189275
ttl tt2 #3
506.9641 509.1988 507.0823
1041.867 1043.274 1035.164
504.6135 506.3696 503.2017
982.9478 986.5386 977.2213
1010.096 1013.359 1002.424
1002.768 1007.475 999.7050
1013.216 1018.469 1010.061
ERRORS VALUE RANGE
QC PASS 503.0000 10.40000
QC PASS 1028.000 10.40000
QC PASS 501.0000 10.40000
QC PASS 1025.000 10.40000
QC PASS 1002.000 10.40000
QC PASS 1029.000 10.40000
QC PASS 994.0000 10.40000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1005.746 5.380 .5349234
22031 UG/LITER 1010.972 5.255 .5197479
22032 UG/LITER 1007.441 6.250 .6203893
20681 UG/LITER 1010.993 3.098 .3064279
20682 UG/LITER 1015.371 5.213 .5134228
19601 UG/LITER 996.2794 3.0015 .3012671
19602 UG/LITER 1006.819 4.472 .4442204
ttl #2 tt3
1009.477 1008.182 999.5790
1009.319 1016.855 1006.743
1010.470 1011.600 1000.254
1012.707 1012.856 1007.417
1013.467 1021.268 1011.377
994.7859 999.7346 994.3175
1006.744 1011.329 1002.385
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
999-0000 10.40000
ELEM UNITS AVGE SDEV 1RSD
SNI899 UG/LITER 1103.855 1.922 .1741105
BI2230 UG/LITER 1098.627 7.643 .6956625
MO2020 UG/LITER 1086.127 4.028 .3708942
TI3349 UG/LITER 1096.701 3.903 .3559159
B_2496 UG/LITER 1101.284 5.700 .5175921
Y_3710 PPM 1270.289 5-235 .4120821
#1 #2 #3
1104.361 1105.473 1101.730
1104.167 1101.807 1089-908
1084.610 1090.693 1083.076
1093.643 1101.097 1095.363
1104.289 1104.852 1094.710
1267.267 1267.267 1276.333
ERRORS VALUE RANGE
QC PASS 1100.000 10.40000
QC PASS 1100.000 10-40000
QC PASS 1100.000 10-40000
QC PASS 1100.000 10.40000
QC PASS 1100.000 10-40000
NOCHECK
211
214 ANALYSIS REPORT
QC STANDARD
08/10/10 11:21:34 AM
METHOD: ALT-P3Q3 SAMPLE NAME: ICB RUN TIME: 08/10/10 11:14:37 COMMENT: ICB MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.214746 .427902 199.2601
AL3082 UG/LITER -3.64484 2.27815 62.50330
BA4934 UG/LITER -.372348 .145849 39.17005
BE3130 UG/LITER .0463411 .0760262 164.0579
CA3179 UG/LITER 100.3920 .2248 .2239517
CD2265 UG/LITER .1844070 .2251961 122.1190
C02286 UG/LITER .1747937 .1799194 102.9324
#1 #2 #3
--485309 -.437510 .2785821
-6.27519 -2.29910 -2.36025
-.490586 -.417087 -.209370
-.032474 .0522651 .1192320
100.3232 100.2097 100.6433
.0287864 .0818013 -4426333
.0228528 .1280594 .3734689
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS -OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.106942 .465815 435-5769
CU3247 UG/LITER .4991480 .2305516 46.18904
FE2714 UG/LITER -1.57210 8.26731 525.8767
K_7664 UG/LITER 7.392122 1.968514 26.62989
MG2790 UG/LITER 7.842254 3.246772 41.40100
MN2576 UG/LITER -.107387 .143794 133.9027
NA3302 UG/LITER 139.5359 116.4991 83.49043
#1 «2 tt3
-.499223 -.229504 .4079003
-2790512 .4794962 .7388965
-9.01050 -3.03470 7.328898
6.606377 5.937834 9.632155
6.518045 5.466862 11.54185
-.217546 -.159896 .0552816
185.4961 7.067031 226.0445
ERRORS VALUE RANGE
QC PASS -OOOOOOO 5-000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.COO
QC PASS .OOOOOOO 5000.000
OC PASS .OOOOOOO 10-00000
QC PASS -OOOOOOO 5000-000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER .3977589 .3357601 84.41297
TL1908 UG/LITER 2.038730 2.727755 133.7968
V_2924 UG/LITER -.111585 .092408 82.81365
ZN2138 UG/LITER .1541409 .0819860 53.18898
PB2203 UG/LITER .2186377 .3119362 142.6727
SE1960 UG/LITER -.946999 1.819161 192.0976
SB2068 UG/LITER .3537458 1.571654 444.2890
ttl #2 #3
.4329848 .0457746 .7145173
3.049516 4.116819 -1.05015
-.034190 -.213896 -.086670
.0853963 .1321454 .2448811
.5702546 --024835 -1104931
-3.04216 .2312477 -.030084
-.918093 2-110788 -.131457
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS -OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1.447611 1.019763 70.44451
22031 UG/LITER 2.115404 .451002 21.31988
22032 UG/LITER -.737958 .499310 67.66099
20681 UG/LITER -2.11597 1.25658 59.38541
20682 UG/LITER 1.577117 1.862990 118.1262
19601 UG/LITER 1.088812 7.299410 670-4011
19602 UG/LITER -1.97292 1.68348 85.32931
#1 #2
tt3
.2708079 2.071598 2.000428
2.051506 1.699759 2.594947
-.178870 -.895535 -1.13947
-2.40097 -.741371 -3.20557
-.187377 3.525033 1.393696
-6.73926 2.296858 7.708837
-1.20571 -.809705 -3.90334
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SNI 899 UG/LITER -1.14540 .64835 56.60488
BI2230 UG/LITER 2.380585 1.009638 42.41133
MO2020 UG/LITER 1-993881 -962889 48-29220
TI3349 UG/LITER -4.56434 3.35324 73.46602
B_2496 UG/LITER 2.291569 .737826 32.19740
Y_3710 PPM 1267.667 6.860 .5411151
#1 tt2 #3
-.773271 -1.89404 -.768875
1.879061 3.542788 1.719907
2.936393 2.033418 1.011833
-5.83571 -7.09597 -.761332
2.620915 2.807363 1.446429
1270.800 1259.800 1272.400
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS -OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
212
215 ANALYSIS REPORT
QC STANDARD
08/10/10
1 1 : 2 8 : 3 4 AM
METHOD: A L T - P 3 Q 3 SAMPLE NAME: CRI RUN T I M E : 0 8 / 1 0 / 1 0 1 1 : 2 1 : 3 7 COMMENT: CRI MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 tX3/LITER 8.005695 .207288 2.589258
AL3082 UG/LITER -9.56832 4.74923 49.63496
BA4934 UG/LITER -.430747 .051022 11.84504
BE3130 UG/LITER 4.947470 .053864 1.088712
CA3179 UG/LITER 119.3017 330.6978 277.1946
CD2265 UG/LITER 5.213320 .100127 1.920602
C02286 UG/LITER 50.36095 .15825 .3142322
ttl tt2 tt3
7.933668 7.844029 8.239389
-13.9368 -10.2550 -4.51313
-.483323 -.427483 -.381435
4.901595 4.934036 5.006779
-206.595 454.6005 109-8991
5.260635 5.098304 5-281022
50.53931 50.23738 50.30615
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS -OOOOOOO 400.0000
QC PASS .OOOOOOO 400.0000
QC PASS 5.000000 1.500000
QC PASS .OOOOOOO 2000.000
QC PASS 5.000000 1.500000
QC PASS 50.00000 15.00000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 9.568513 .243550 2.545324
CU3247 UG/LITER 25.24432 .21430 .8489053
FE2714 UG/LITER -.535431 7.064723 1319-447
K_7664 UG/LITER 1.606766 2.583449 160.7856
MG2790 UG/LITER 4.121679 1.781327 43-21849
MN2576 UG/LITER 14.40805 .02330 -1616972
NA3302 UG/LITER 55.65066 42.25235 75.92424
#1 #2 #3
9.828167 9.345138 9.532235
25.31113 25.00457 25.41725
1.486649 -8.39072 5.297775
3.534413 -1.32869 2.614576
6.019437 2.485769 3.859831
14.40310 14.38763 14.43343
63.90192 93.16875 9.881334
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS 25.00000 7.500000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 2000.000
QC PASS .OOOOOOO 2000-000
QC PASS 15.00000 4.500000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 39-65611 -62805 1.583737
TLI908 UG/LITER 26-33096 .94833 3-601566
V_2924 UG/LITER 50.04606 .28063 .5607417
ZN2138 UG/LITER 53.10621 .18666 .3514858
PB2203 UG/LITER 9.994963 -140869 1.409404
SEI960 UG/LITER 35.85115 1.15863 3.231771
SB2068 UG/LITER 61.87915 1.21810 1.968507
#1 #2 #3
39.78083 38.97506 40.21244
27.12527 26-58658 25.28102
50.18570 49.72301 50.22948
53.19456 53.23228 52-89177
9.833021 10-06269 10.08918
35.36093 35.01821 37.17430
61.44285 63.25531 60.93929
ERRORS VALUE RANGE
QC PASS 40.00000 12-00000
QC PASS 25.00000 12-50000
QC PASS 50.00000 15.00000
QC PASS 60.00000 18-00000
QC PASS 10.00000 5.000000
QC PASS 35.00000 10.50000
QC PASS 60.00000 30.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 10.55911 .89953 8.519013
22031 UG/LITER 11.28853 1.81301 16.06065
22032 UG/LITER 9.334714 -760898 8.151274
20681 UG/LITER 60.02023 2-51589 4.191733
20682 UG/LITER 62.79760 1-61941 2.578771
19601 UG/LITER 36.99021 2.49219 6.737431
19602 UG/LITER 35.27285 2.07695 5.888233
ttl #2 #3
10.15409 11.58994 9.933287
9.604096 13-20733 11-05417
9.932829 8.478288 9.593024
57.17733 61.95948 60-92389
63.56276 63.89264 60.93739
34.25573 39.13397 37.58093
35.90305 32.95380 36.96172
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
10.00000 3.000000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 50.87080 2.18056 4.286461
BI2230 UG/LITER 49.16674 2.82175 5.739139
MO2020 UG/LITER 51.07673 .30076 .5888392
TI3349 UG/LITER 48.41533 3.81302 7.875651
B_24 96 UG/LITER 51.70816 .68127 1.317534
Y_3710 PPM 1269-156 4.459 .3513655
#1 #2 #3
50.14417 49.14632 53.32189
51.64204 46.09417 49.75400
51.21195 51.28614 50.73209
47.81232 44-93975 52-49393
51.39861 52.48925 51-23663
1265.000 1268.600 1273-867
ERRORS VALUE RANGE
NOCHECK
QC PASS 50.00000 15.00000
NOCHECK
NOCHECK
QC PASS 50.00000 15-00000
NOCHECK
213
216 ANALYSIS REPORT
QC STANDARD
08/10/10 11:35:34 AM
METHOD: ALT-P3Q3 SAMPLE NAME: ICSA RUN TIME: 08/10/10 11:28:37 COMMENT: ICSA MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.031655 .099547 314.4746
AL3082 UG/LITER 251586.5 504.5 -2005078
BA4934 UG/LITER 2.573750 -095698 3.718236
BE3130 UG/LITER .7910559 .0412611 5.215952
CA3179 UG/LITER 252344.7 1312.2 .5199950
CD2265 UG/LITER 1.686348 .181935 10.78867
C02286 UG/LITER 5.078364 .197014 3.879486
ttl #2 tt3
.0414048 -.145038 -0086677
251489.8 252132-4 251137-5
2.629114 2.463248 2.628889
.8386649 .7688363 .7656664
251445.2 253850.4 251738.4
1-611268 1.553968 1.893806
5.292564 5.037623 4.904906
ERRORS VALUE RANGE
QC PASS .OOOOOOO 10.00000
QC PASS 244100.0 48820.00
QC PASS 2.000000 400.0000
QC PASS .OOOOOOO 10.OOOOO
QC PASS 234900-0 46980.00
QC PASS -OOOOOOO 10.00000
QC PASS 4.000000 10.00000
ELEM LTNITS AVGE SDEV %RSD
CR2677 UG/LITER 45.22913 .57070 1-261801
CU3247 UG/LITER 23.35778 .16008 .6853557
FE2714 UG/LITER 99992.54 214.60 .2146198
K_7664 UG/LITER 7.923087 10.84794 136.9155
MG2790 UG/LITER 260101-2 399.3 .1535111
MN2576 UG/LITER 18.03399 .02341 .1298145
NA3302 UG/LITER 1007.538 152.560 15.14184
ttl #2 #3
45.88809 44.89457 44-90472
23.25952 23.54250 23-27131
100063-2 100162-9 99751.52
19.66393 -1.72783 5.833164
259817-9 260557.9 259927.9
18.01248 18.03057 18.05892
1156.609 851.7134 1014-294
ERRORS VALUE RANGE
QC PASS 43.00000 20.00000
QC PASS 23-00000 10.00000
QC PASS 95600.00 19120.00
QC PASS .OOOOOOO 2000.000
QC PASS 247500.0 49500-00
QC PASS 19-00000 20.00000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 22.17113 .58304 2-629714
TL1908 UG/LITER 1-844182 3-542668 192-0997
V_2924 UG/LITER 1.260371 .292063 23.17279
ZN2138 UG/LITER 28.45664 .20319 .7140270
PB2203 UG/LITER 14.31928 .62010 4.330524
SE1960 UG/LITER -3.89377 2-41464 62.01299
SB2068 UG/LITER 1-661626 .698683 42.04814
#1 #3
22.74567 22.18779 21.57995
-2779942 5.900010 -.645458
1.528072 .9488890 1-304152
28.62089 28.51961 28.22942
14.08895 15.02158 13.84730
-1.10753 -5.19649 -5.37728
2.254117 1-839590 .8911721
ERRORS VALUE RANGE
QC PASS 21.00000 10.00000
QC PASS .OOOOOOO 20-00000
QC PASS 1.000000 40.00000
QC PASS 28.00000 40.00000
QC PASS 10.00000 6.000000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1.061333 2.074955 195.5046
22031 UG/LITER -.214973 1.874734 872.0768
22032 UG/LITER 21.56138 1.37495 6.376931
20681 UG/LITER 6.685167 2.755243 41.21427
20682 UG/LITER -.856580 1.354409 158.1182
19601 UG/LITER -8.38078 1.09279 13.03929
19602 UG/LITER -1.66383 4.10344 246.6266
ttl f»3
-1.14035 1.343710 2-980638
1-887169 --818413 -1-71368
20,.16656 22,.91557 21,.60202
5-643307 9-809414 4.602781
.5518646 -2.14956 -.972043
-9-50064 -7.31723 -8.32449
3.072529 -4.14794 -3.91608
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 20.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER .5239312 3.572728 681.9078
BI2230 UG/LITER 4.893574 3.856149 78.80027
MO2020 UG/LITER 1.271363 .397352 31.25400
TI3349 UG/LITER -1.28509 2.67391 208.0728
B_2496 UG/LITER -3-49141 .11773 3-372021
Y_3710 PPM 1202-289 1.260 .1048195
#1 #2 tt3
-.056710 4.351415 -2.72291
8-546489 .8621114 5.272120
.8216683 1.417348 1.575074
.0151787 -4.36046 .4900246
-3.40361 -3.62519 -3-44542
1202.733 1200.867 1203.267
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS -OOOOOOO 100.0000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 100.0000
QC PASS -OOOOOOO 100-0000
NOCHECK
tt2
tt2
214
217 ANALYSIS REPORT
QC STANDARD
08/10/10
1 1 : 4 2 : 3 5 AM
METHOD: ALT-P3Q3 SAMPLE NAME: ICSAB RUN T I M E : 0 8 / 1 0 / 1 0 1 1 : 3 5 : 3 8 COMMENT: ICSAB MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 199.6669 .4393 .2199942
AL3 082 UG/LITER 248715.5 1670.3 .6715532
BA4934 UG/LITER 507.1974 3.5115 .6923433
BE3130 UG/LITER 486.7356 3.5763 .7347437
CA3179 UG/LITER 248278.7 1786.7 .7196270
CD2265 UG/LITER 983.7699 6.9024 .7016267
C02286 UG/LITER 499.5670 3.5600 .7126108
ttl tt2 #3
199.1606 199.8936 199.9465
246786.9 249681.7 249678.0
503.1426 509-2396 509.2098
482.6169 489.0537 488.5363
246219.2 249414.2 249202.7
975.8812 988.6990 986.7294
495.5235 502.2295 500.9481
ERRORS VALUE RANGE
QC PASS 206.0000 41.20000
QC PASS 241100-0 48220.00
QC PASS 495.0000 400.0000
QC PASS 475.0000 95.00000
QC PASS 231100.0 46220.00
QC PASS 940.0000 188.0000
QC PASS 461.0000 92.20000
ELEM UNITS AVGE SDEV %RSD
CR2577 UG/LITER 53 8,5129 3,8944 .7231719
FE2714 CU3247 UG/LITER UG/LITER 523.6810 98829.78 741.37 1.1089 .2117443 .7501455
K_7664 UG/LITER 4.792633 2.490673 51.96877
MG2790 UG/LITER 258024.2 1987.9 .7704190
MN2576 UG/LITER 513.1858 3.7356 -7279320
NA3302 UG/LITER 1062.506 128.870 12-12891
#1 #2 (13
534,0204 540,5884 540,9299
522.5098 523.8186 524.7147
97973.73 99256.08 99259.54
7-661607 3.531915 3.184378
255729.0 259143.3 259200.2
508.8782 515.5349 515.1445
1204.148 1031.190 952.1793
ERRORS VALUE RANGE
QC PASS 511,0000 102,2000
QC PASS 548-0000 109.6000
QC PASS 94800.00 18960.00
QC PASS .OOOOOOO 2000.000
QC PASS 251100.0 50220.00
QC PASS 502.0000 100.4000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1028.973 7.520 -7308440
TL1908 UG/LITER 100-9332 1-6914 1-675758
V_2924 UG/LITER 503.0996 3.5926 .7140995
ZN2138 UG/LITER 1026.831 7.196 -7008273
PB2203 UG/LITER 63.67939 .83750 1.315187
SE1960 UG/LITER 46.31426 1.96836 4.250014
SB2068 UG/LITER 621.0368 3.6282 .5842162
#1 #2 #3
1020.320 1033.930 1032.668
100.3185 102-8460 99.63506
499.0215 505.7972 504.4802
1018-533 1031.356 1030.606
62.94160 64.58973 63.50686
45.69472 48.51786 44.73020
617.1680 624.3634 621.5790
ERRORS VALUE RANGE
QC PASS 984.0000 196,8000
QC PASS 103.0000 20-60000
QC PASS 494.0000 98.80000
QC PASS 1028.000 205-6000
QC PASS 61.00000 12.20000
QC PASS 53.00000 10.60000
QC PASS 589.0000 117.8000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 98.90888 2-17083 2.194782
22031 UG/LITER 48.95384 3-23591 6.610122
22032 UG/LITER 71.01540 2.62094 3.690664
20681 UG/LITER 623.8207 7.5451 1.209503
20682 UG/LITER 619.6408 1-6777 .2707587
19601 UG/LITER 39.18034 2.43649 6.218658
19602 UG/LITER 49.86566 1.77308 3.555711
#1 tt2 #3
98.43091 101.2789 97.01686
49.02706 45.68194 52.15251
69.87277 74.01366 69-15974
615.6822 630.5831 625.1970
617.9037 621.2521 619.7665
37.90572 41.98974 37.64555
49.57322 51.76678 48.25698
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
101.0000 20.20000
ELEM UNITS AVGE SDEV %RSD
SNI 8 9 9 UG/LITER 987.6367 5-5361 .5605441
BI2230 UG/LITER 1023.894 10.185 .9946973
MO2020 UG/LITER 979.4838 11.5246 1.176600
TI3349 UG/LITER 999.4612 9.1361 .9140984
B_2496 UG/LITER 1008.419 8.014 .7947373
y_3710 PPM 1201.844 4.949 .4117647
ttl tt2 tt3
981.2764 991-3731 990.2605
1012-161 1030.456 1029.065
966.4413 983.7169 988.2933
989-0142 1005.955 1003.414
999.1874 1012.473 1013.596
1207.533 1198.533 1199-467
ERRORS VALUE RANGE
QC PASS 1000-000 200.0000
QC PASS 1000.000 200.0000
QC PASS 1000.000 200.0000
QC PASS 1000.000 200.0000
QC PASS 1000.000 200.0000
NOCHECK
215
218 ANALYSIS REPORT
QC STANDARD
08/10/10 11:49:36 AM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCV RUN TIME: 08/10/10 11:42:39 COMMENT: CCV CVSl MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 99.78887 .20072 .2011427
AL3082 UG/LITER 49706.83 68.33 .1374622
BA4934 UG/LITER 996.2067 .7993 .0802335
BE3130 UG/LITER 999.0322 .3267 .0327007
CA3179 UG/LITER 49127.18 519.64 1.057734
CD2265 UG/LITER 996.1175 1.1634 .1167966
C02286 UG/LITER 994.1396 .3731 .0375349
ttl
S2 #3
99-59602 99.99663 99.77396
49785.72 49668.35 49666.42
997.1149 995.8948 995.6103
999.2926 999.1384 998.6657
49099.90 49659.92 48621.73
997.0615 996.4733 994.8177
994.5689 993.8934 993.9564
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000-00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1005-414 1.390 -1382806
CU3247 UG/LITER 997.9385 .8344 .0836168
FE2714 UG/LITER 25120.38 26.18 .1042295
K_7664 UG/LITER 48117.90 133.43 .2772975
MG2790 UG/LITER 49966.07 50.32 .1007102
MN2576 UG/LITER 987.8174 .5681 .0575123
NA3302 UG/LITER 50026.16 67.89 .1357013
#1 #2 #3
1006.710 1003.946 1005.585
996.9756 998.3905 998.4495
25150.27 25109.38 25101.50
48267.88 48073.46 48012.36
50023.79 49931.41 49943.02
988.1081 988.1813 987.1627
50022.61 49960.12 50095.76
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1007.621 .820 .0813482
TL1908 UG/LITER 1007.187 1.498 .1487494
V_2924 UG/LITER 1008.589 1.462 .1449992
ZN2138 UG/LITER 1080.691 1.151 .1065466
PB2203 UG/LITER 1000.130 1.012 .1012309
SE1960 UG/LITER 1000.712 1.879 .1877308
SB2068 UG/LITER 1031.343 3.001 .2909991
ttl #2 #3
1008.120 1008.068 1006.675
1007.611 1008.427 1005.522
1009.713 1009.118 1006.936
1081.784 1080.799 1079.489
1001.268 999.7956 999.3276
1002.869 999-4377 999.8278
1034.766 1030.097 1029.165
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1006.300 2.539 .2523371
22031 UG/LITER 998.8356 2.8686 .2871918
22032 UG/LITER 1000.762 .247 .0246622
20681 UG/LITER 1029.384 2.920 .2836783
20682 UG/LITER 1032.317 3.309 .3205346
19601 UG/LITER 998.3315 4.2505 .4257581
19602 UG/LITER 1001.890 .927 -0924757
ttl tt3
1003.405 1008.148 1007.349
1002.138 997.4023 996.9661
1000.818 1000.976 1000.492
1032.026 1029.877 1026.249
1036.130 1030-204 1030.617
1003.186 996.5289 995-2794
1002-701 1000.880 1002.089
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
1000-000 104.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1014.868 3.854 .3797821
BI2230 UG/LITER 1013.571 5.761 .5684336
MO2020 UG/LITER 1014.571 1.546 .1523476
TI3349 UG/LITER 1012.659 1.459 .1441004
B_2496 UG/LITER 1024.642 1.798 .1755121
Y_3710 PPM 1249.400 2.254 .1803985
#1 tt2 tt3
1019.269 1012-091 1013.246
1018.202 1015.391 1007.119
1016.165 1014.469 1013.078
1011.180 1012-699 1014.098
1026.525 1024.459 1022.942
1246.800 1250.800 1250.600
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
#2
216
219 ANALYSIS REPORT
QC STANDARD
08/10/10 11:56:37 AM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCB RUN TIME: 08/10/10 11:49:40 COMMENT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.125642 .116632 92.82911
AL3082 UG/LITER 58.05686 52.28412 90.05674
BA4934 UG/LITER -.012378 .311484 2516.517
BE3130 UG/LITER .5004976 .3229135 64.51849
CA3179 UG/LITER 438-3375 333.1902 76.01224
CD2265 UG/LITER .5797743 .4153565 71.64107
C02286 UG/LITER .1795999 .3476792 193.5853
(fl
It2 #3
-.067049 -.049923 -.259953
21.20343 117.8961 35.07105
-.189868 .3472826 -.194547
.2976632 .8728701 .3309595
100.5164 447.8009 766.6951
.2536033 1.047376 .4383432
.0451665 .5744240 --080791
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5-000000
QC PASS -OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5-000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.288195 .366795 127.2730
CU3247 UG/LITER .1807936 .2256758 124.8251
FE2714 UG/LITER 27.76304 21.51169 77.48318
K_7664 UG/LITER 7.333461 3.438621 46.88947
MG2790 UG/LITER 78-12363 52.67322 67.42291
MN2576 UG/LITER .1677701 .2870878 171.1198
NA3302 UG/LITER 24.24767 4.80048 19.79771
ttl »2 ft3
-.680728 .0458272 -.229684
-.027512 .4205416 -1493514
8.698197 51.08501 23.50593
3.726538 10.57452 7.699322
42.40765 138.6166 53.34661
-.026953 -4974710 .0327924
27.42116 26.59682 18-72502
ERRORS VALUE RANGE
QC PASS -OOOOOOO 5.000000
QC PASS -OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER .4883697 .1311293 26.85041
TL1908 UG/LITER 1.263558 .798174 63.16877
V_2924 UG/LITER .1400947 -2254253 160-9093
ZN2138 UG/LITER .8454278 .3374586 39.91573
PB2203 UG/LITER .2529325 -5890552 232-8903
SE1960 UG/LITER 1.904025 .714665 37.53445
SB2068 UG/LITER -8808757 1.775963 201.6134
ttl tt2 #3
.4915079 .3556995 .6179017
1.487605 .3773030 1.925765
-.011463 .3991473 .0325993
.6666496 1.234662 .6349718
-.310807 .8643991 .2052057
2.648230 1.840736 1-223109
2.854492 -.588295 .3764301
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS -OOOOOOO 3-000000
QC PASS -OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .2989719 1.412327 472-3945
22031 UG/LITER 1.854436 .895457 48.28728
22032 UG/LITER -.556286 .444522 79.90877
20681 UG/LITER 1.860571 1.981671 106.5088
20682 UG/LITER -3820949 1-684453 440.8469
19601 UG/LITER 3.157191 3.316942 105.0599
19602 UG/LITER 1.268713 .947016 74.64381
ttl tt2 #3
--306063 -.710042 1.913022
.9262493 2.713111 1.923949
-.938020 -.068251 -.662589
4.121098 .4228435 1.037772
2-212528 -1.10279 -0365435
5.182006 4.960311 -.670744
1.373630 .2736078 2.158902
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -1.53447 .85328 55.60771
BI2230 UG/LITER 1-729235 1.393496 80.58455
MO2020 UG/LITER 2.502985 1.132128 45.23112
TI3349 UG/LITER -4.57973 1.52159 33.22434
B_2496 UG/LITER 1.970503 .841326 42.69598
Y_3710 PPM 1263.489 6.585 .5211729
#1 #2 #3
-1.74010 -.597162 -2.26615
3.321329 1.135073 .7313016
3.258391 3.049259 1.201304
-3.06665 -4.56286 -6.10969
1.899066 2.845269 1-167173
1270.733 1261-867 1257-867
ERRORS VALUE RANGE
QC PASS -OOOOOOO 100.0000
QC PASS .OOOOOOO 50-00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
217
220 08/10/10 12:06:06 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: LRS RUN TIME: 08/10/10 11:59:09 COMMENT: SDG:LRS CLIENTID:LRS MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 3.671387 .290869 7.922597
AL3082 UG/LITER 219.7225 21.8124 9.927271
BA4934 UG/LITER 192.9218 .3817 .1978394
BE3130 UG/LITER 5.131500 .150421 2.931335
CA3179 UG/LITER 5181.045 363.966 7.024947
CD2265 UG/LITER 5.166673 .059595 1.153456
C02286 UG/LITER 5.060225 .168833 3.336480
#1 tt2 #3
3.464967 3.545146 4.004049
201.8406 244.0244 213.3023
193.2731 192.9766 192.5157
5.025692 5.303694 5.065114
4760.774 5391.509 5390-852
5.098115 5-195811 5.206093
4.892567 5.230209 5.057897
ERRORS HIGH LOW
LC PASS 7.500000 2.500000
LC PASS 300.0000 100.0000
LC PASS 300-0000 100.0000
LC PASS 7-500000 2.500000
LC PASS 7500.000 2500.000
LC PASS 7.500000 2.500000
LC PASS 7.500000 2.500000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 9.373298 .231533 2.470138
CU3247 UG/LITER 4.394075 .047163 1.073337
FE2714 UG/LITER 100.8946 8.1739 8.101424
K_7664 UG/LITER 3975.759 7.582 .1907157
MG2790 UG/LITER 4830.532 19.155 .3965333
MN2576 UG/LITER 9.436164 .159508 1.690387
NA3302 UG/LITER 4777.842 43.268 .9056045
ttl tt2 tt3
9.111305 9.550421 9.458167
4.394075 4.346912 4.441239
92.84802 109.1901 100-6457
3983.474 3975.487 3968.316
4822.293 4852.427 4816.874
9.289259 9.605829 9.413403
4823.723 4737.773 4772-030
ERRORS HIGH LOW
LC PASS 15.00000 5.000000
LC PASS 7-500000 2.500000
LC PASS 150.0000 50.00000
LC PASS 7500.000 2500.000
LC PASS 7500.000 2500.000
LC PASS 15.00000 5.000000
LC PASS 7500.000 2500.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 5.325868 .506360 9.507562
TL1908 UG/LITER 10.73716 1.30853 12.18694
V_2924 UG/LITER 19.58416 -09634 .4919149
ZN2138 UG/LITER 16.90211 .03231 .1911671
PB2203 UG/LITER 4.374526 .673133 15.38757
SE1960 UG/LITER 3.807509 .466087 12-24126
SB2068 UG/LITER 10.30844 1.36458 13.23747
#1 #2 tt3
4.998245 5.909082 5.070277
10.12095 9.850489 12.24003
19.58428 19.48775 19.68043
16.87590 3.732606 16.93821 H5.075042 16.89221 4.315930
3.494842 3.584478 4.343206
10.82733 8.760538 11.33747
ERRORS HIGH LOW
LC PASS 7.500000 2.500000
LC PASS 15-00000 5.000000
LC PASS 30-00000 10-00000
LC PASS 30.00000 10.00000
LC PASS 4.500000 1.500000
LC PASS 7.500000 2.500000
LC PASS 15-00000 5.000000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 9.718045 .221445 2.278703
22031 UG/LITER 6.016498 .339601 5.644502
22032 UG/LITER 3.542719 .841939 23.76532
20681 UG/LITER 9.648639 .422105 4.374765
20682 UG/LITER 10-62827 1.95616 18-40527
19601 UG/LITER 5-862868 1.197409 20.42360
19602 UG/LITER 2-771728 .215297 7.767621
ttl tt2 #3
9.655697 9.963981 9.534457
5.663428 6.340800 6.045266
2.756536 4.431086 3.440535
9.316927 9.505223 10.12377
11.57177 8.379187 11.93386
4.766866 5.680889 7.140850
2.850099 2.528223 2.936862
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
15.00000 5.000000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER 21.30519 1.05027 4.929640
BI2230 UG/LITER 21.41277 1.49197 6.967664
MO2020 UG/LITER 20.76624 .51204 2.465733
TI3349 UG/LITER 16.37344 3.90346 23.84022
B_2496 UG/LITER 19-17920 -15220 -7935616
Y_3710 PPM 1267.133 4.908 .3873701
ttl tt2 tt3
22.35889 20.25839 21.29828
20.97141 20.19128 23.07563
20.42909 21-35545 20.51419
12.49786 16.31824 20.30420
19.23500 19-29562 19-00698
1261.467 1269-867 1270.066
ERRORS HIGH LOW
LC PASS 30.00000 10.00000
LC PASS 30.00000 10.00000
LC PASS 30-00000 10.00000
LC PASS 30-00000 10.00000
LC PASS 30.00000 10.00000
NOCHECK
218
221 0 8 / 1 0 / 1 0 1 2 : 1 3 : 0 7 PM
ANALYSIS REPORT
METHOD: A L T - P 3 Q 3 SAMPLE NAME: 1 0 0 7 1 5 6 - 0 2 R E 1 RUN T I M E : 0 8 / 1 0 / 1 0 1 2 : 0 6 : 1 0 COMMENT: SDG:MY71N3 CLIENTID:MY71N4 1 10 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0588915 -1055172 179.1722
AL3082 UG/LITER 3034.751 93-208 3.071341
BA4934 UG/LITER 5.533710 .235715 4.259611
BE3130 UG/LITER .1862894 .0522165 28.02979
CA3179 UG/LITER 2475.043 364.937 14.74466
CD2265 UG/LITER .6664985 .0871809 13.08044
C02286 UG/LITER 82.83139 2.78833 3.366267
ttl tt2 tt3
.1303746 -.062299 .1085987
2985.164 2976.819 3142.270
5.418507 5.377753 5.804871
.1583983 .1539410 .2465289
2222.826 2893.501 2308.800
.7607152 .6500971 .5886831
81.41675 81.03395 86.04348
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1224.389 34.767 2.839569
CU3247 UG/LITER 8.084627 .198353 2.453464
FE2714 UG/LITER 48482.12 1323.25 2.729361
K_7664 UG/LITER 21.15890 3.66655 17.32864
MG27 90 UG/LITER 205756.9 5639.8 2.741017
MN2576 UG/LITER 684.1121 18.7356 2.738669
NA3302 UG/LITER 202.0295 31.1363 15.41177
#1 #2 #3
1204.618 1204.017 1264.534
8.013882 7-931345 8.308654
47715.00 47721.30 50010.08
20.80312 17.68321 24.99037
202446.1 202555.7 212268.9
673.1968 673.3938 705.7458
169.9152 204.0877 232.0857
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 2175.668 59.611 2.739889
TL1908 UG/LITER -1.09942 1.77094 161.0792
V_2924 UG/LITER 21.11632 -50102 2.372685
ZN2138 UG/LITER 19.50451 .74910 3.840668
PB2203 UG/LITER 4.650127 .896943 19.28857
SE1960 UG/LITER -1.69137 1.70360 100.7234
SB2068 UG/LITER .2887356 .2291750 79.37192
ttl tt2 tt3
2141.481 2141.022 2244.500
.7215104 -2.81573 -1.20404
20.76199 20.89743 21.68954
19.05802 19.08616 20.36935
4.384583 5.649860 3.915938
-.513628 -3.64477 -.915699
.0722722 .5287962 .2651383
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS . LC PASS lOOOO.OO 60000.00 -20-0000 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .5953128 .7720915 129.6951
22031 UG/LITER 8.272656 1.295357 15.65830
22032 UG/LITER 2.828551 .708885 25.06179
20681 UG/LITER .7731524 1.316162 170.2332
20682 UG/LITER .0369765 .9997558 2703.760
19601 UG/LITER -6.18763 3-25631 52-62619
19602 UG/LITER .5434761 2-401846 441.9414
#1 tt2 #3
1.037862 -.296214 1.044290
8.081924 9.652805 7.083240
2.525828 3.638537 2.321286
2-090787 --541531 -7702007
-.945264 1.053372 -0028210
-2.51861 -7.30990 -8-73438
.4775677 -1.82474 2-977598
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.318233 2.741669 861.5298
BI2230 UG/LITER 2.439028 1.625310 66.63759
MO2020 UG/LITER .2392787 .2058630 86.03483
TI3349 UG/LITER 8.789231 3.179744 36.17773
B_2496 UG/LITER 11.74200 -60349 5.139565
Y_3710 PPM 1232.400 27.312 2-216175
#1 tt2 tt3
2.815047 -2.27688 -1.49287
.8092225 4.059804 2.448058
.0214625 .2657449 .4306288
7.130581 6.781757 12.45536
11.28328 11.51706 12.42565
1247-733 1248.600 1200-867
ERRORS HIGH LOW
LC PASS 40000-00 -20.0000
LC PASS 40000-00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
219
222 08/10/10 12:21:45 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 1007156-05RE1 RUN TIME: 08/10/10 12:14:48 COMMENT: SDG:MY71N3 CLIENTID:MY71N7 1:3 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .2608879 .1516154 58.11514
AL3082 UG/LITER 17447.93 79.99 .4584761
BA4934 UG/LITER 912.8013 4.4927 .4921850
BE3130 UG/LITER .7668133 .0082990 1.082271
CA3179 UG/LITER 59926.39 198.59 .3313956
CD2265 UG/LITER 1.963527 -107724 5.486264
C02286 UG/LITER 70.76940 .39271 .5549138
#1 *2 #3
.4352589 .1872411 .1601638
17408.49 17539.98 17395.30
911.7686 917.7205 908.9150
.7761685 .7603372 .7639344
60016.41 60064.04 59698.73
1.996825 1.843085 2.050671
71.02966 70.96086 70.31768
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200-000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1010.094 4.455 .4410700
CU3247 UG/LITER 60.91965 .25535 .4191555
FE2714 UG/LITER 76979.98 313.54 .4073039
K_7664 UG/LITER 2385.585 14.667 .6148270
MG2790 UG/LITER 164215.9 726.3 .4422999
MN2576 UG/LITER 2143.254 8.938 .4170138
NA3302 UG/LITER 12071.97 12.04 .0997555
ttl tt2 tt3
1008.047 1015.205 1007.031
60.88428 61.19084 60-68383
76864.84 77334-82 76740.30
2391.596 2396.291 2368.867
163886.8 165048.5 163712.3
2140.121 2153.336 2136.304
12070.84 12084.53 12060.53
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000-0 -100-000
LC PASS 400000-0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1320.913 5.247 .3972585
TLI908 UG/LITER -1.73631 2.74886 158.3168
V_2924 UG/LITER 77.53414 .58334 -7523675
ZN2138 UG/LITER 143.4808 .5143 .3584317
PB2203 UG/LITER 25.57728 .33723 1-318488
SE1960 UG/LITER 7.933329 1.248322 15.73516
SB2068 UG/LITER 1.092081 2-224814 203.7224
ttl tt2 tt3
1320.130 1326-508 1316-101
-2.17561 -4.23906 1.205754
77.58144 78-09239 76-92859
143.4765 143-9973 142.9687
25.70180 25.83454 25.19549
6.606780 8.108232 9.084976
2.894846 -1.39433 1.775729
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 24.47378 1.12275 4.587555
22031 UG/LITER 30.37541 2.03837 6.710579
22032 UG/LITER 23.17196 .51211 2.210059
20681 UG/LITER 3.511179 1.718028 48.93024
20682 UG/LITER -.125091 2.589920 2070.425
19601 UG/LITER 1.156324 3.943389 341.0279
19602 UG/LITER 11.30690 2.62942 23.25496
ttl #2 tt3
24.27158 25.68389 23.46587
31.11202 31.94308 28.07113
22.99088 22.77499 23.75002
4.153398 1.564558 4.815581
2.257884 -2.88143 .2482715
2.669887 -3.31962 4.118705
8.562413 13.80372 11.55458
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10-0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 6.480973 1-251917 19.31681
BI2230 UG/LITER 4.633990 .733183 15.82186
MO2020 UG/LITER 3.596574 .086543 2.406253
TI3349 UG/LITER 548.9239 2.3300 .4244636
B_2496 UG/LITER 167.7235 1.1979 .7141853
Y_3710 PPM 1242.533 4.068 .3274203
ttl tt2 #3
7.675724 5-178811 6.588385
4.432870 4.022356 5.446745
3.578142 3.520731 3.690847
549.0740 551.1753 546.5226
167.0608 169.1062 167.0033
1240.667 1239.733 1247.200
ERRORS HIGH LOW
LC PASS 40000-00 -20-0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10-0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
220
223 ANALYSIS REPORT
08/10/10 12:28:45 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 1007159-07RE1 RUN TIME: 08/10/10 12:21:49 COMMENT: SDG:MY71S4 CLIENTID:My71T6 1:2 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
AG3280 UG/LITER -.587248 .053419 9.096557
AL3082 UG/LI'TER 304.8245 8.4728 2.779559
BA4934 UG/LITER 11.42997 .22113 1.934620
BE3130 UG/LITER .3141167 .0260026 8.278015
CA3179 UG/LITER 60032.32 1185.07 1.974046
CD2265 UG/LITER .0066484 .2483164 3734.977
C02286 UG/LITER 31.41416 -34197 1.088582
.541472 .574331 .645942
295.0412 309.6599 309.7725
11.17809 11.59214 11.51969
.2849874 .3349861 .3223765
60177.99 58781.15 61137.82
-.279467 .1659769 .1334348
31.14131 31.30339 31.79778
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.263340 .658397 250.0176
CU3247 UG/LITER -.117909 .178947 151.7669
FE2714 UG/LITER 205.3436 19.2171 9.358508
K_7664 UG/LITER 5318.526 33.370 .6274329
MG2790 UG/LITER 163066.8 1372.6 .8417425
MN2576 UG/LITER 1031.758 8.899 .8624858
NA3302 UG/LITER 63746.01 478.32 .7503531
ttl #2 tt3
-1.01936 .1840111 .0453319
-.310494 .0432329 -.086467
183.6030 212.3660 220.0617
5301.602 5297.010 5356.968
162079.5 162486.8 164634.2
1025.411 1027.934 1041.930
63516.02 63426.12 64295.88
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000-00
ELEM ITOITS AVGE SDEV %RSD
NI2316 UG/LITER 98.16219 .95903 .9769825
TL1908 UG/LITER -1.75515 2.34275 133.4790
V_2924 UG/LITER -.058643 .169186 288.4997
ZN2138 UG/LITER 43.68221 .40252 .9214709
PB2203 UG/LITER .7334853 .6650214 90.66595
SE1960 UG/LITER 3.014551 1.383627 45.89829
SB2068 UG/LITER 1.257605 .703755 55.95997
ffl #2 ff3
97.08285 98.48737 98.91634
-1.24116 -4.31222 .2879336
.0272648 -.253547 .0503523
43.41082 43.49114 44.14468
.1965774 .5264912 1-477387
1.486481 4.182537 3.374636
1.324865 1.925315 .5226341
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
ASI890 UG/LITER -.071161 .068188 95.82207
22031 UG/LITER 5.049282 1-032834 20-45507
22032 UG/LITER -1.43429 -77922 54.32779
20681 UG/LITER .2876178 .7102321 246.9361
20682 UG/LITER 1.732037 .743260 42.91244
19601 UG/LITER 2.384203 3.291875 138.0702
19602 UG/LITER 3.319416 2.062943 62.14777
ttl #2 tt3
-.017411 -.147864 -.048208
3.860928 5.730682 5.556236
-1.64510 -2.08640 -.571352
.0251107 1.091736 -.253994
1.963966 2.331679 .9004675
-.096874 1.130823 6.118660
2.267166 5.696301 1.994782
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.428343 .321205 13.22734
BI2230 UG/LITER 1.399240 1.340939 95.83342
MO2O20 UG/LITER 1.025568 .448681 43-74953
TI3349 UG/LITER -2.48982 2.02530 81.34316
B_2496 UG/LITER 1869.463 14.253 .7623892
Y_3710 PPM 1243.911 6.853 .5508866
ttl tt2 tt3
2.380490 2.133748 2.770790
1.624027 -.039887 2.613580
1.527080 .8874126 .6622114
-4.78356 -1.73780 -.948103
1858.918 1863.793 1885.678
1247.733 1248.000 1236.000
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
ELEM UNITS AVGE SDEV %RSD ttl tt2 tt3
221
224 08/10/10 12:35:46 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0080607-DUPl RUN TIME: 08/10/10 12:28:49 COMMENT: SDG:MY71S4 CLIENTID:MY71T6D 1:2 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.063854 .311588 487.9681
AL3082 UG/LITER 282.5652 3.3634 1.190322
BA4934 UG/LITER 11.05387 .01916 .1733426
BE3130 UG/LITER .2081423 .0240629 11.56077
CA3179 UG/LITER 59706.09 825.26 1.382209
CD2265 UG/LITER .1720667 .0410244 23.84213
C02286 UG/LITER 31.02395 .18183 .5860815
ttl tt2 tt3
-.259493 .2954631 -.227533
286.3590 281.3879 279.9486
11.07125 11.03332 11.05705
.2327989 .2069071 .1847207
60642.54 59085.03 59390.70
.2182363 .1581624 .1398016
30.99991 31.21660 30.85534
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.448300 .148832 33.19922
CU3247 UG/LITER .3576571 .0476524 13.32348
FE2714 UG/LITER 190.0632 2.0883 1.098732
K_7664 UG/LITER 5214.148 13.724 .2632093
MG2790 UG/LITER 160395.2 188.0 .1172283
MN2576 UG/LITER 1014.493 1.167 .1150743
NA3302 UG/LITER 63204.18 209.77 .3318863
ttl #2 tt3
-.511181 -.278348 -.555372
.3497964 .4087510 .3144238
190.4880 191.9063 187.7951
5228.889 5201.739 5211.816
160554.0 160187.6 160444.1
1015.801 1013.557 1014.122
63177.03 63009.32 63426.21
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000-0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 96.27490 .71158 .7391120
TL1908 UG/LITER .8004047 1.445282 180.5690
V_2924 UG/LITER -1911683 .0518429 27.11901
ZN2138 UG/LITER 41.92126 .18886 .4505141
PB2203 UG/LITER .2938986 1.078222 366.8687
SE1960 UG/LITER 3.036953 3.225171 106.1976
SB2068 UG/LITER .3668824 .2433648 66.33319
ttl #2 tt3
97.07980 96.01541 95.72948
1.569518 1.698497 -.866802
.2142608 .2274524 .1317917
42.13025 41.76282 41.87070
1.076630 -.935955 .7410209
-.340086 6.085043 3.365904
-0908681 .4591897 .5505896
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.123827 .422341 341.0734
22031 UG/LITER 1.628484 2.824161 173.4227
22032 UG/LITER -.384636 .564104 146.6591
20681 UG/LITER -.230301 .991721 430-6194
20682 UG/LITER .6552239 .8515525 129.9636
19601 UG/LITER .2358017 4-928192 2089.972
19602 UG/LITER 4.425627 2-415881 54.58845
ttl #2 #3
-.162127 .3163591 -.525713
2.686401 -1.57190 3.770947
.2607021 -.630706 -.783905
.9096805 -.894325 -.706258
-.327749 1.125136 1.168284
-5.18926 4-436139 1-460531
2.071044 6.898463 4.307375
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.253564 .321541 14.26812
BI2230 UG/LITER 2.164069 1.170146 54.07156
MO2020 UG/LITER 1.215544 .433191 35.63763
TI3349 UG/LITER 2.400206 1.973721 82.23132
B_2496 UG/LITER 1835.728 2-811 .1531464
Y_3710 PPM 1247.822 2.397 .1920621
ttl tt2 #3
2.069112 2.066734 2.624845
3-395299 2.030425 1.066483
1.668389 1.173112 .8051301
3.942434 3.082270 .1759148
1837-047 1832.500 1837.639
1245.133 1248.600 1249-733
ERRORS HIGH LOW
LC PASS 40000-00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
222
225 08/10/10
ANALYSIS REPORT
1 2 : 4 5 : 0 9 PM
METHOD: A L T - P 3 Q 3 SAMPLE NAME: S D I 1 0 0 7 1 5 9 - 0 7 RUN TIME: 0 8 / 1 0 / 1 0 1 2 : 3 8 : 1 2 COMMENT: SDG:MY71S4 CLIENTID:MY71T6L 1:10 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 OG/LITER -.332570 .210248 63.21912
AL3082 UG/LITER 54.04365 .91083 1.685358
BA4934 UG/LITER 1.908211 .034735 1.820292
BE3130 UG/LITER .1172127 .0041157 3.511275
CA3179 UG/LITER 12050.74 386.13 3.204172
CD2265 UG/LITER .0562472 .0758100 134.7801
C02286 UG/LITER 6.175538 .106777 1.729024
#1 #2 #3
-.130609 -.550225 -.316875
53.07490 54.88253 54.17344
1.880125 1.897456 1.947051
.1217334 .1136830 .1162216
11838.70 12496.43 11817.09
.1432035 .0214929 .0040452
6.298622 6.107759 6.120233
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.490291 .161343 32.90756
CU3247 UG/LITER -.279052 .083652 29.97714
FE2714 UG/LITER 17.95723 5.01102 27.90532
K_7664 UG/LITER 871.0158 4.4005 .5052102
MG2790 UG/LITER 31946.53 39.32 .1230694
MN2576 UG/LITER 206.9233 .3063 .1480138
NA3302 UG/LITER 12813.13 33-54 .2617837
ttl tt3
-.505867 -.643281 -.321725
-.204376 -.369448 -.263330
20.18360 12.21881 21.46928
875.6166 866.8477 870.5828
31956.07 31980.19 31903-31
206.9963 207.1865 206-5871
12850.55 12785.76 12803-07
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000-0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 33.06300 2.64506 8.000060
TL1908 UG/LITER -.473542 2.334721 493.0335
V_2 924 UG/LITER -.060078 .308884 514.1423
ZN2138 UG/LITER 8.352556 .151429 1-812968
PB2203 UG/LITER .6159678 1.058407 171.8282
SE1960 UG/LITER .0745674 1.089509 1461.105
SB2068 UG/LITER -.087281 1.058876 1213-178
ttl tt2 tt3
•30.28138 35.54619 33.36142
2.148587 -2.32706 -1.24216
.2955126 -.261878 -.213867
8.186129 8.389323 8.482216
-.577807 .9861380 1.439572
-.335291 1.309565 -.750572
-1.02489 1.061147 -.298105
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM tJNITS AVGE SDEV %RSD
AS1890 UG/LITER -.155042 1.030211 664.4705
22031 UG/LITER .8066309 1.624429 201.3844
22032 UG/LITER .5098450 .7780042 152.5962
20681 UG/LITER -.279166 1.214424 435.0191
20682 UG/LITER -.001204 1.618423 134421.1
19601 UG/LITER -7666124 2.507958 327.1482
19602 UG/LITER -.280658 2.417914 861.5172
#1 #2 #3
1.010086 -.945433 -.529779
-1.04373 1.465559 1.998064
-.356142 .7358587 1.149818
.4620645 .3811213 -1.68068
-1.77698 1.390930 .3824344
-1.37877 -1547066 3.523898
.1759348 1.876408 -2.89432
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.707146 .254063 35.92799
BI2230 UG/LITER .1399306 2.214291 1582.421
MO2020 UG/LITER .2942613 .4352259 147.9046
TI3349 UG/LITER -5.90292 3.51976 59.62742
B_2496 UG/LITER 373.8095 .5106 .1366060
Y_3710 PPM 1257.044 1.174 .0934286
ttl #2 #3
-.422768 -.786924 -.911746
2.093180 -2.26557 .5921843
-.030066 .7888861 .1239635
-3-59927 -9.95450 -4.15499
374.3565 373.7265 373.3453
1255.800 1257.200 1258.133
ERRORS HIGH LOW
LC PASS 40000.00 -20-0000
LC PASS 40000.00 -10-0000
LC PASS 40000.00 -10-0000
LC PASS 40000.00 -30-0000
LC PASS 40000.00 -50-0000
NOCHECK
#2
223
226 ANALYSIS REPORT
0 8 / 1 0 / 1 0 1 2 : 5 2 : 0 9 PM
IffiTTHOD: ALT-P3Q3 SAMPLE NAME: 1 0 0 7 1 5 9 - l O R E l RUN T I M E : 0 8 / 1 0 / 1 0 1 2 : 4 5 : 1 2 COMMENT: SDG:MY71S4 CLIENTID :MY7 IWO 1:2 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.155197 .147499 95.04022
AL3082 UG/LITER 167.8629 3.8126 2.271284
BA4934 UG/LITER 9.596407 .046454 .4840756
BE3130 UG/LITER .2320659 .0555426 23.93398
CA3179 UG/LITER 84697.22 466.47 .5507541
CD2265 UG/LITER .0526353 .0206783 39.28603
C02286 UG/LITER 7.176604 .205007 2.856605
ttl tt2 tt3
-.090776 -.050866 -.323948
166.1379 165.2176 172.2332
9.649748 9.564837 9.574635
.1951062 .2051534 .2959381
85174.02 84241.80 84675.83
.0586149 .0696648 -0296261
7.407418 7-106710 7-015683
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50-0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.435939 .194546 44.62693
CU3247 UG/LITER .0943270 .2299475 243.7769
FE2714 UG/LITER -48.7609 1.6237 3.329932
K_7664 UG/LITER 5381.674 17.622 .3274426
MG2790 UG/LITER 180737.9 355.0 .1964290
MN2576 UG/LITER 311-0993 .6836 .2197377
NA3302 UG/LITER 104850.7 363.4 .3465596
ttl tt2 #3
-.654094 -.373277 -.280445
.2554692 .1965147 -.169003
-47.0439 -48.9672 -50.2716
5400.992 5366.480 5377.551
180967.7 180329.0 180917.1
311.6621 310.3386 311.2973
105267.7 104682.1 104602.2
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15-0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 17.32937 .28603 1-650553
TL1908 UG/LITER 2.442087 2.086119 85-42361
V_2924 UG/LITER .1139045 .0757593 66.51126
ZN2138 UG/LITER 2.899338 .064805 2.235161
PB2203 UG/LITER .8193024 .7089714 86.53353
SE1960 UG/LITER 2.437717 1.852942 76-01135
SB2068 UG/LITER 1.324489 1.515041 114.3868
ttl tt2 tt3
17.43511 17-54747 17-00552
4.205026 2.982212 .1390243
.1460886 .0273666 .1682581
2.843368 2.970337 2.884308
1.021771 1.405015 .0311219
1.344889 4.577143 1.391119
2.678627 1.606630 -.311789
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM IWJITS AVGE SDEV %RSD
AS1890 UG/LITER --437565 .531544 121.4777
22031 UG/LITER 1.952177 2.440242 125.0010
22032 UG/LITER .2426210 .1910846 78.75845
20681 UG/LITER .6918388 2.820909 407.7408
20682 UG/LITER 1.630890 .960573 58.89872
19601 UG/LITER 2.511569 1.005574 40.03770
19602 UG/LITER 2-390986 3-151059 131.7891
ttl tt2 tt3
.1639807 -.632763 -.843912
2.379119 4.150774 -.673361
.3330055 .0231121 .3717455
3.627171 .4470367 -1.99869
2.195190 2.175707 .5217724
3.638618 1.706176 2.189912
-1898687 6.000625 .9824632
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER .7120003 .6609718 92.83308
BI2230 UG/LITER 2.122803 1.362580 64.18776
MO2020 UG/LITER 1.405592 .712385 50.68220
TI3349 UG/LITER 1.752651 1.370393 78.18971
B_2496 UG/LITER 2691.377 4-780 .1776216
Y_3710 PPM 1241-000 1-665 .1341900
#1 #2 #3
1.382938 .6915950 .0614674
1.692581 1.027263 3.648565
1.044147 2.226245 .9463854
.8160248 3.325512 1.116417
2691.966 2686.330 2695.836
1239.133 1242-333 1241.533
ERRORS HIGH LOW
LC PASS 40000-00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000-00 -50.0000
NOCHECK
224
227 08/10/10 12:59:09 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 1007159-12RE1 RUN TIME: 08/10/10 12:52:12 COMMENT: SDG:MY71S4 CLIENTID:MY71X0 1:2 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.512817 .266135 51.89673
AL3082 UG/LITER 24.54553 6.20865 25.29443
BA4934 UG/LITER 11.41154 .06214 -5444936
BE3130 UG/LITER .3498164 .0435403 12.44662
CA3179 OG/LITER 99042.77 873.16 .8815964
CD2265 UG/LITER .1107089 .1093558 98.77773
C02286 UG/LITER .5306264 .2581246 48.64525
ttl tt2 tt3
-.619816 -.708800 -.209835
31.71040 21.17734 20.74886
11.40425 11.35336 11.47699
.4000554 .3263671 .3230267
98841.05 98288.12 99999.12
.0620939 .0340902 .2359427
.5870912 .2489437 .7558444
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000-00
LC PASS 10000.00 -5-00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1.866048 .107541 5.763019
CU3247 UG/LITER 4.162188 .044639 1.072497
FE2714 UG/LITER 6.460264 6.036898 93.44662
K_7664 UG/LITER 2973.041 26.929 .9057611
MG2790 UG/LITER 154685.6 964.5 .6235537
MN2 576 UG/LITER 297.7114 1.6830 .5653189
NA33 02 UG/LITER 323419.4 1303.7 .4030845
ttl «2 «3
1-815315 1-793259 1.989571
4.111094 4.193630 4.181839
-.139589 11.70328 7.817102
2997.513 2944.192 2977-418
155600.3 153677.9 154778.6
299.3370 295.9763 297.8209
324216.3 321915.0 324127.1
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000-0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000-00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 8.986041 .375166 4.174985
TL1908 UG/LITER -.284385 3.348947 1177.610
V_2924 UG/LITER .7469315 .1038282 13.90064
ZN2138 UG/LITER 1.287973 .101696 7-895787
PB2203 UG/LITER .9341021 .6894218 73.80584
SE1960 UG/LITER 41.69189 2.06870 4.961866
SB2068 UG/LITER 1-453429 .507862 34.94234
ttl #2 tt3
9.21Q425 9.194766 8-552931
2.593603 -3.96019 .5134339
.8386599 .6342113 .7679234
1.328937 1.172184 1.362799
1.710207 .6995052 .3925942
39.68528 41.57287 43.81753
1.959043 1.457895 .9433480
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM LINITS AVGE SDEV %RSD
AS1890 UG/LITER .3660580 1.327486 362.6437
22031 UG/LITER 3.882162 .211891 5.458060
22032 UG/LITER -.548745 1.074101 195.7375
20681 UG/LITER 1.024030 1.171175 114.3692
20682 UG/LITER 1.658004 .906260 54.65972
19601 UG/LITER 39.23517 2.28899 5.834016
19602 UG/LITER 42.90860 1.96965 4.590335
ttl #2 #3
.0169454 1.833213 -.751984
3.749942 4.126559 3.769986
.6807721 -1.02241 -1.30460
1.836148 -.318512 1.554453
2.010534 2.335027 .6284513
36.87087 39.39407 41.44056
41-08050 42.65089 44.99443
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1.428749 1.801147 126.0647
BI2230 UG/LITER 3.590314 1.750340 48.75173
MO2020 UG/LITER 10.79874 .63548 5.884733
TI3349 UG/LITER 3.048903 3.732230 122.4122
B_24 96 UG/LITER 3632.179 21.825 .6008858
Y_3710 PPM 1248.867 7.601 .6086200
ttl tt2 »3
-.310165 3.286268 1.310143
1.643058 5.032810 4.095073
11.23122 10.06912 11.09587
-.257481 2.308268 7.095923
3654.522 3610.911 3631.105
1241.333 1256.533 1248.733
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
225
228 08/10/10 01:06:09 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 1007159-13RE1 RUN TIME: 08/10/10 12:59:12 COMMENT: SDG:MY71S4 CLIENTID:MY71X2 1:2 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.206517 .083168 40.27153
AL3082 UG/LITER 172.3225 5.5889 3.243298
BA4934 UG/LITER 11.51028 .11410 .9913157
BE3130 UG/LITER .2383778 .0392825 16.47909
CA3179 UG/LITER 59137.81 303.63 .5134249
CD2265 UG/LITER -1163345 .1325252 113.9173
C02286 UG/LITER 31.39028 .36550 1.164377
#1 #2 #3
-.114715 -.276834 -.228002
176.4843 165.9701 174.5130
11.62289 11.39474 11.51319
.2802426 .2325654 .2023253
59480.08 58900.89 59032.45
.1938866 .1918046 -.036688
31.67988 30.97960 31.51135
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5-00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.138322 .287467 207.8249
CU3247 UG/LITER .1061179 .1516098 142.8692
FE2714 UG/LITER -50.4799 4.0472 8.017532
K_7664 UG/LITER 5241.533 30.370 .5794154
MG2790 UG/LITER 160682.4 848.6 .5281107
MN2576 UG/LITER 1038.456 5.353 .5155234
NA3302 UG/LITER 63245.83 195.54 .3091725
#1 #2 #3
.1842776 -.367330 -.231913
.2790512 .0432329 -.003930
-45.9979 -51.5746 -53.8672
5266.602 5207.761 5250.234
161120.1 159704.3 161222.7
1042.056 1032.304 1041.007
63368.20 63020.31 63348.97
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000-0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 94.16803 .79452 .8437263
TL1908 UG/LITER -2.02786 2.61232 128.8219
V_2924 UG/LITER -.038017 .251198 660.7457
ZN2138 UG/LITER 23.36427 .13779 .5897592
PB2203 UG/LITER 1.533928 .452149 29.47653
SE1960 UG/LITER 2.805921 .995800 35.48924
SB2068 UG/LITER 1.812787 .983823 54.27134
#1 #2 tt3
95.07925 93.80478 93.62007
-4.75104 .4573191 -1.78985
.2204421 -.281262 -.053232
23.44114 23.20519 23.44647
1-365249 1.190366 2.046168
3.948336 2.347781 2.121647
2.157367 .7030227 2.577970
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3-00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .2094352 .8429309 402.4782
22031 UG/LITER 1.959938 1-861627 94.98399
22032 UG/LITER 1.309036 1.294338 98.87714
20681 UG/LITER 2.267562 .566964 25.00323
20682 UG/LITER 1.575975 1.317932 83.62643
19601 UG/LITER -.864385 3.222014 372.7524
19602 UG/LITER 4.628558 1.277516 27.60074
ttl tt2 tt3
.5725390 -.754197 .8099633
4.107293 .8007940 .9717263
-.015970 1.372725 2.570355
2.879794 1.760630 2.162262
1.786893 .1653041 2.775729
1.902610 -4.40176 -.094005
4.959864 5.707784 3.218026
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1.056846 3.476936 328.9917
BI2230 UG/LITER .1210304 2-355710 1946-378
MO2020 UG/LITER .4987139 .3034976 60-85605
TI3349 UG/LITER .9798158 4.078330 416.2343
B_2496 UG/LITER 1842.092 9.132 .4957394
Y_3710 PPM 1252.600 6.300 .5029193
#1 #2 tt3
2.747280 -2.94208 3.365343
2.812462 -.883343 -1.56603
.2165783 .4597529 -8198106
4.239439 -3.59345 2.293457
1848-832 1831.699 1845.746
1247.800 1259.733 1250.267
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
226
229 08/10/10
ANALYSIS REPORT
01:13:09
METHOD: ALT-P3Q3 SAMPLE NAME: 1 0 0 7 1 5 7 - l O R E l Rinj TIME: 0 8 / 1 0 / 1 0 1 3 : 0 6 : 1 2 COMMENT: SDG:MY71S3 CLIENTID:MY71W1 1:2 MODE: CONC CORR. FACTOR: 1
PM
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0372086 .1145112 307.7548
AL3082 UG/LITER 2452.880 3.569 .1454872
BA4934 UG/LITER 13.29366 .03528 .2653945
BE3130 UG/LITER .3481256 .0090284 2.593435
CA3179 UG/LITER 90208.20 420.34 .4659685
CD2265 UG/LITER .1858592 .1681204 90.45580
C02286 UG/LITER 13.84059 .35967 2.598651
ttl #2 #3
-.040397 -.016702 .1687251
2455.706 2454.065 2448.870
13.33327 13.26562 13.28209
.3417216 .3584517 .3442032
89884.52 90056.80 90683.27
.3673244 .0354000 .1548532
14.04049 13.42538 14.05591
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000-0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM ITOITS AVGE SDEV %RSD
CR2677 UG/LITER 1.926365 .545561 28-32077
CU3247 UG/LITER 1.281278 .085025 6.635982
FE2714 UG/LITER 5642.308 2.486 .0440671
K_7664 UG/LITER 5462.542 15.173 .2777666
MG2790 UG/LITER 184690.4 241.2 .1305921
MN2576 UG/LITER 391.9536 .3762 .0959836
NA3302 UG/LITER 106537.5 205.8 .1931932
#1 tt2 tt3
1.296930 2-218803 2.263361
1.352023 1.186950 1.304860
5639.549 5644.375 5643.000
5476.560 5464.635 5446.431
184767.1 184883.9 184420.2
392.2412 392.0919 391.5279
106614.2 106693.9 106304.3
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 40-68980 .22728 .5585644
TL1908 UG/LITER .2654388 1.485987 559.8227
V_2924 UG/LITER .9303137 .1009136 10.84726
ZN2138 UG/LITER 83.35792 .06724 .0806595
PB2203 UG/LITER .7447317 .9614691 129.1027
SE1960 UG/LITER .4338813 .6361182 146.6111
SB2068 UG/LITER .2670404 .6926275 259.3718
#1 #2 #3
40.92039 40.46598 40.68304
-1.32982 .5157768 1.610357
.9844229 .8138852 .9926330
83.42101 83.28719 83.36556
1.839385 -3577900 -0370201
1.135311 -.105629 .2719623
.9676633 -.417305 .2507628
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .2287163 .8498415 371.5701
22031 UG/LITER 2.980033 .967979 32.48214
22032 UG/LITER -.382286 .978497 255.9591
20681 UG/LITER -.574141 1.582755 275.6737
20682 UG/LITER .6772035 .3880545 57.30250
19601 UG/LITER .2396634 1.578158 658.4892
19602 UG/LITER .5210464 .7769088 149.1055
#1 #2 #3
.4500123 .9460186 -.709882
4.007077 2.84 8439 2.084584
.7461237 -.896748 -.996235
1.226356 -1.74600 -1.20278
.8286973 .2362531 .9666600
.8869630 -1.55923 1.391254
1.249481 .6102872 -.296629
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.520009 .992891 39.40029
BI2230 UG/LITER 2.036425 1.732853 85.09291
MO2020 UG/LITER 1.144592 .564276 49.29925
TI3349 UG/LITER 2.771432 2.451897 88.47039
B_2496 UG/LITER 2754.077 2.984 .1083331
Y_3710 PPM 1249.133 1.943 .1555110
ttl »2 tt3
1.507564 2.560346 3.492116
1.977745 3.797873 .3336570
1.571171 1.357835 .5047709
.0456314 3.471531 4-797134
2752.946 2757.461 2751.825
1247.000 1249.600 1250.800
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
227
230 ANALYSIS REPORT
QC STANDARD
0 8 / 1 0 / 1 0 0 1 : 2 0 : 1 1 PM OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCV RUNTIME: 0 8 / 1 0 / 1 0 1 3 : 1 3 : 1 3 COMMENT: CCV CVSl
MODE: CONC
PAGE 1
CORR:. FACTOR: 1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 99.43311 .26313 .2646257
AL3082 UG/LITER 49641.61 170.00 .3424553
BA4934 UG/LITER 996.4407 3.5332 .3545774
BE3130 UG/LITER 991.5111 3.1942 .3221509
CA3179 UG/LITER 48987.33 72.47 .1479451
CD2265 UG/LITER 989.1603 3.6522 .3692254
C02286 UG/LITER 984.8475 2.6963 .2636238
tfl #2 #3
99.71795 99.19912 99.38226
49678.57 49456.16 49790.08
997.2655 992.5682 999.4886
992.8183 987.8707 993.8443
48968.48 49067.37 48926.14
991.0049 984.9536 991.5222
985.8265 981.9040 986-8119
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1000.813 2.631 .2628890
CU3247 UG/LITER 997.2507 1.8671 .1872260
FE2714 UG/LITER 24942.38 83.49 .3347489
K_7664 UG/LITER 48113.06 152.68 .3173440
MG2790 UG/LITER 50113.79 172.86 .3449285
MN2576 UG/LITER 979.4709 3.0492 .3113133
NA3 302 UG/LITER 49855.19 149.61 .3000847
ttl tt2 #3
1001.993 997.7980 1002.646
996.0913 996.2563 999.4046
24982.65 24846.38 24998.11
48164.08 47941.40 48233.70
50165.35 49921.02 50255.00
980.6498 976.0082 981.7546
49912.06 49685.49 49968.03
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1003.479 3.694 .3680831
TLI908 UG/LITER 1001.963 6.519 .6506169
V_2924 UG/LITER 1002.555 3.036 .3028123
ZN2138 UG/LITER 1076.346 3.962 .3681334
PB2203 UG/LITER 996.0139 1.5953 .1601670
SE1960 UG/LITER 994.2469 6.9484 .6988603
SB2068 UG/LITER 1026.060 .906 .0882937
ttl tt2 tt3
1003.749 999.6578 1007.030
994.4998 1004.843 1006.546
1003.879 999.0815 1004.703
1077.875 1071.847 1079.316
997.4069 994.2736 996.3614
998.0330 986.2277 998.4800
1027.059 1025.290 1025.833
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000-000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1003.606 6.578 .6554120
22031 UG/LITER 988.3875 2-0836 -2108098
22032 UG/LITER 999.8068 1.6331 .1633417
20681 UG/LITER 1016.201 2.293 .2266478
20682 UG/LITER 1030.979 .253 .0245805
19601 UG/LITER 991.7667 5.8610 .5909609
19602 UG/LITER 995.4763 7.5876 .7622132
#1 tt2 tt3
1002.622 997.5750 1010.620
990.7751 986.9368 987.4506
1000.703 997.9218 1000.795
1018.799 1014.459 1015.345
1031.179 1030.694 1031.065
996.1793 985-1166 994.0041
998.9486 986.7728 1000.705
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHEiTK
VALUE RANGE
1000.000 104.0000
ELEM imiTS AVGE SDEV %RSD
SN1899 UG/LITER 1002.507 5.219 .5206331
BI2230 UG/LITER 1014.368 3.707 .3654772
MO2020 UG/LITER 1007.055 4.922 .4887825
TI3349 UG/LITER 1004.632 3.382 .3366450
B_24 96 UG/LITER 1025.233 3.089 -3013199
Y_3710 PPM 1252.955 2.986 -2383266
ttl tt2 #3
1005-012 996-5074 1006.002
1017.164 1010.163 1015.778
1003.545 1004.938 1012.682
1007.963 1001.201 1004.731
1025.268 1022.126 1028.304
1250-667 1256.333 1251.867
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
228
231 ANALYSIS REPORT
QC STANDARD
08/10/10 01:27:12 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCB RUN TIME: 08/10/10 13:20:15 COMMENT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.254878 .262616 103.0362
AL3082 UG/LITER 25.48952 6.58868 25.84859
BA4934 UG/LITER -.405683 .026022 6.414420
BE3130 UG/LITER .4081742 .0660866 16.19077
CA3179 UG/LITER -224.962 580.422 258.0086
CD2265 UG/LITER .1709078 .1367259 79.99983
C02286 UG/LITER .0104283 .1176805 1128.474
ttl «2 #3
-.285005 .0215032 -.501131
18.60259 26.13328 31.73270
-.381936 -.401611 -.433501
.3390402 .4147627 .4707198
-562.110 445.2469 -558.024
.0137291 .2623475 .2366467
.0859240 .0705272 -.125166
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.182126 .276391 151.7580
CU3247 UG/LITER -.620988 .085297 13.73577
FE2714 UG/LITER 2.365358 6.074757 256.8219
K_7664 UG/LITER 3.851597 1.143355 29.68521
MG2790 UG/LITER 13.79480 1.52612 11.06301
MN2676 UG/LITER -.226824 -062554 27.57814
NA3302 UG/LITER 65.17943 32.35775 49.64412
ttl tt2 tt3
-.319636 -.362791 .1360485
-.676012 -.522730 -.664221
-1.74966 -.496749 9.342484
3.009092 5.153133 3.392566
12.04053 14.52723 14.81665
-.299054 -.190607 -.190810
77.60744 89-48070 28.45013
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.446975 .218632 48.91368
TL1908 UG/LITER 1.270256 1.183078 93.13700
V_2924 UG/LITER -.080119 .219615 274.1103
ZN2138 UG/LITER .3348663 .0448893 13.40514
PB2203 UG/LITER .2936684 .6449549 219.6201
SE1960 UG/LITER -.033865 3.162015 9337.203
SB2068 UG/LITER .5129029 .6917435 134.8683
ttl tt2 tt3
-.660807 -.223840 -.456279
2.067810 -.089044 1.832002
-.332253 .0224480 .0694472
.3808639 .2911741 .3325608
.6689573 -.451054 .6631016
-2.66103 -.916156 3.475589
-.018294 .2618959 1.295107
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS -OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1.006913 1.238328 122.9826
22031 UG/LITER 1.754441 1-133382 64.60078
22032 UG/LITER -.445244 1.003526 225.3881
20681 UG/LITER -1.32090 .85168 64.47711
20682 UG/LITER 1.418810 .697085 49.13163
19601 UG/LITER 3.377371 2.394880 70.90961
19602 UG/LITER -1.74655 4.69329 268.7179
ttl tt2 »3
.2845285 .2994261 2.436786
3-004931 1.463502 .7948888
-.506935 -1.41650 .5877050
-1.53486 -2.04519 -.382643
.7291936 1.404107 2.123130
1.154065 5.913150 3.064897
-4.57537 -4.33529 3.671022
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.203287 1.275808 627.5879
BI2230 UG/LITER 2.867633 1.866236 65.07931
MO2020 UG/LITER 1.737551 .352161 20.26767
TI3349 UG/LITER -1.92443 3.40803 177.0936
B_2496 UG/LITER 3.150470 .453494 14.39447
Y_3710 PPM 1269.555 3.890 .3063918
ttl #2 tt3
-1.33051 1.181733 -.461088
4.899397 2.473672 1.229830
2.006412 1.867323 1.338918
-5.83686 .3983499 -.334771
3.666619 2.815913 2.968879
1265.066 1271.667 1271.933
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS -OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
229
232 ANALYSIS REPORT
08/10/10 01:35:47 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-12RE1 RUN TIME: 08/10/10 13:28:50 COMMENT: SDG:MY71S3 CLIENTID:MY71W9 1:2 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM tJNITS AVGE SDEV %RSD
AG3280 UG/LITER -.343353 .289162 84.21712
AL3082 UG/LITER 49.90254 .79588 1.594863
BA4934 UG/LITER 11.33962 .03176 .2800505
BE3130 UG/LITER .4447157 .0813347 18.28914
CA3179 UG/LITER 94697.92 880.41 .9297081
CD2265 UG/LITER .2150106 .1830389 85.13017
C02286 UG/LITER .5841720 .3760427 64.37192
#1 tt2 #3
-.603749 -.394155 -.032157
50.80250 49.29140 49.61371
11.32906 11.37531 11.31448
.3909298 .4049332 .5382843
95281.58 95126.95 93685.23
.1280675 .0916472 .4253172
.1856293 .6341754 .9327113
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 3.093283 .443819 14.34782
CU3247 UG/LITER .7310357 .3452403 47.22619
FE2714 UG/LITER 251.5813 1.8781 .7465371
K_7664 UG/LITER 2825.592 30.059 1.063808
MG2790 UG/LITER 147710.1 1650.8 1.117575
MN2576 UG/LITER 283.5778 2.8853 1.017459
NA3302 UG/LITER 311087.4 2449.1 .7872643
ttl tt2 #3
2.615594 3.171393 3.492861
-3615878 1.045459 .7860597
249.4450 252.3263 252.9726
2850.456 2834.132 2792.187
148892.7 148413.4 145824.1
285.5566 284.9095 280.2671
312897.2 312064.4 308300.6
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 8.653359 .267496 3.091233
TL1908 UG/LITER .9652438 2.238531 231.9136
V_2924 UG/LITER .9735501 .1239572 12.73249
ZN2138 UG/LITER 1.338010 .117362 8.771405
PB2203 UG/LITER .1199563 1.105814 921.8473
SE1960 UG/LITER 39.33668 3.38670 8.609532
SB2068 UG/LITER 2.360352 .462326 19.58716
ttl tt2 tt3
8.413830 8.942012 8.604237
1.140722 3.110872 -1.35586
.8319446 1.026289 1.062417
1.232884 1.316510 1.464636
.5296857 -1.13225 .9624288
35.90615 39.42610 42.67778
2.894137 2.100545 2.086373
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1.329095 .543544 40.89583
22031 UG/LITER 2.355882 1.571495 66.70515
22032 UG/LITER -1.00617 2.05887 204.6249
20681 UG/LITER .6186321 .4906337 79.30944
20682 UG/LITER 3.220887 .455567 14.14416
19601 UG/LITER 39.16135 3.30528 8.440160
19602 UG/LITER 39.41437 3.43254 8.708843
ttl tt2 #3
1.401742 1.832663 .7528807
3.778790 2.619669 .6691867
-1.10233 -3.01527 1.099096
1.176015 .2521084 .4277727
3.743251 3.013497 2.905913
35.70196 39.49486 42.28723
35.99819 39.38189 42.86303
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000-00 -10-0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.697767 .450824 16.71100
BI2230 UG/LITER .6812662 1.789897 262.7310
MO2020 UG/LITER 10.65783 .18019 1.690678
TI3349 UG/LITER 7.371908 4.311498 58.48562
B_2496 UG/LITER 3477.722 37.070 1.065927
Y_3710 PPM 1244.355 11.163 .8970697
ttl #2 #3
3.086754 2.203676 2.802872
2.466051 -1.11370 .6914477
10.45245 10.78938 10.73165
2.612760 11.01714 8.485817
3505.554 3491.970 3435.642
1237.000 1238.867 1257.200
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10-0000
LC PASS 40000.00 -30.0000
LC PASS 40000-00 -50-0000
NOCHECK
230
233 08/10/10 01:42:47 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-13RE1 RUN TIME: 08/10/10 13:35:50 COMMENT: SDG:MY71S3 CLIENTID:MY71X1 1:2 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.342313 .207336 60.56901
AL3082 UG/LITER 12251.18 26.25 .2142669
BA4934 UG/LITER 20.62450 .02387 .1157562
BE3130 UG/LITER .9966130 .0067676 .6780575
CA3179 UG/LITER 62343.39 153.33 .2459521
CD2265 UG/LITER .7391496 .0816212 11.04258
C02286 UG/LITER 62.25427 .30157 .4844174
#1 #2 #3
-.111877 -.401295 -.513768
12260.82 12271.25 12221.48
20.63939 20.63714 20.59696
1.003746 .9957890 .9903052
62199.04 62504.36 62326.77
.7552754 .6506692 .8115044
62.23099 62.56681 61.96502
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 6.486177 .083966 1.294544
CU3247 UG/LITER 8.946362 .112478 1.257390
FE2714 UG/LITER 23147.42 51.22 .2212979
K_7664 UG/LITER 5261.818 10.057 .1911356
MG2790 UG/LITER 161792.0 303.4 .1875122
MN2576 UG/LITER 1258.653 2.769 .2199803
NA3302 UG/LITER 63230.84 131.66 .2080692
ttl tt2 tt3
6.390464 6.520632 6.547435
9.004317 9.016108 8.815662
23174.85 23179.10 23088.33
5267.393 5267.853 5250.208
161935.2 161997.2 161443.5
1260.663 1259.801 1255.495
63162.48 63382.60 63147.53
ERRORS HIGH LOW
LC PASS 60000-00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 181.6164 .7365 .4055489
TL1908 UG/LITER 1.754306 3.136727 178.8016
V_2924 UG/LITER 1.383760 .044748 3.233766
ZN2138 UG/LITER 695.8387 1.7722 .2974366
PB2203 UG/LITER 2.101083 1.635322 77.83234
SE1960 UG/LITER -.072509 1.318652 1818.606
SB2068 UG/LITER 1.180357 .452063 38.29882
ttl tt2 #3
182.4493 181.0506 181.3494
-.833930 5.242695 .8541509
1.339820 1.382186 1.429274
597.3348 596.2997 593.8816
1.105325 1.209492 3.988432
-1.22659 1.364712 -.355644
1.637079 1-170889 .7331022
ERRORS HIGH LOW
LC PASS 60000-00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.611720 .766748 125.3430
22031 UG/LITER 2.732674 2.836070 103.7837
22032 UG/LITER 1.773686 1.122376 63.27928
20681 UG/LITER 2.377510 .307832 12.94766
20682 UG/LITER .5731615 .8272213 144.3261
19601 UG/LITER --465075 2.449893 538.3495
19602 UG/LITER .1089711 .7591745 696.6749
ttl #2 tt3
.2726893 -1.08963 -1.01831
1.693255 .6629606 5.941807
.7996171 1.520369 3.001071
2.121059 2.292581 2.718891
1.385922 .6013620 -.267800
-2.48951 2.264428 -1.14014
-.605611 .9060063 .0265183
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000-00 -10-0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1.027374 .665891 64.81488
BI2230 UG/LITER 3.021467 2.311594 76.50568
MO2020 UG/LITER .6872029 .1054755 17.96236
TI3349 UG/LITER -1.64335 2.24159 136.4039
B_2496 UG/LITER 1879.498 3.661 .1947598
Y_3710 PPM 1284.911 2.432 .1892454
#1 #2 #3
1.350046 1.470457 .2616181
3.915821 4.752263 -3963178
.6442703 .7073742 -6099642
-1.16926 .3232803 -4.08405
1881.531 1881.690 1876.272
1283.066 1284.000 1287.667
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
231
234 ANALYSIS REPORT
QC STANDARD
08/10/10 01:49:47 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CRI RUN TIME: 08/10/10 13:42:50 COMMENT: CRI MODE: CONC CORR. FACTOR: 1 AG3280 UG/LITER 7.455729 .418608 5.614576
AL3082 UG/LITER 13.22722 1.14548 8.660035
BA4934 UG/LITER -.419634 .015604 3.718393
BE3130 UG/LITER 5.141676 .028220 .5488389
CA3179 UG/LITER 119.2965 331.9590 278.2639
CD2265 UG/LITER 5.146954 .102021 1.982162
C02286 UG/LITER 50.10839 .35825 .7149520
Q6.976129 7.747685 7.643373
12.75741 12.39134 14.53292
-.436643 -.416277 -.405982
5.136665 5.116362 5.172103
109.3367 456.1233 -207.671
5.163822 5.037551 5.239490
49.72938 50.44144 50.15436
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS .OOOOOOO 400.0000
QC PASS .OOOOOOO 400.0000
QC PASS 5.000000 1.500000
QC PASS .OOOOOOO 2000.000
QC PASS 5.000000 1.500000
QC PASS 50.00000 15.00000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 9.620118 .215196 2.236938
CU3247 UG/LITER 24.18314 .13041 .5392695
FE2714 UG/LITER 5.300899 8.255015 155.7286
K_7664 UG/LITER 1.329093 2.093232 157.4932
MG2790 UG/LITER 9.555736 5.667919 59.31432
MN2576 UG/LITER 14.30548 .03939 .2763797
NA3302 UG/LITER 37.48706 14-78464 39.43931
ttl #2 tt3
9.390673 9.652225 9.817457
24.06130 24.32070 24.16742
-2.36880 14.03749 4.234002
1.650470 3.243052 -.906242
5.464066 7.177886 16.02526
14.26732 14.30311 14.34600
30.98240 54.40879 27.06999
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS 25.00000 7.500000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 2000.000
QC PASS .OOOOOOO 2000.000
QC PASS 15.00000 4.500000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 40.14023 .21410 .5333804
TL1908 UG/LITER 26.15460 .11100 .4243812
V_2924 UG/LITER 49.88592 .10067 .2017982
ZN2138 UG/LITER 53.11613 .26510 .4991006
PB2203 UG/LITER 9.702647 .277025 2.855151
SE1960 UG/LITER 34.04257 .93058 2.733567
SB2068 UG/LITER 61.70251 .84128 1.363447
ttl tt2 tt3
40.02801 40.00558 40.38712
26.07772 26.28185 26.10424
49.98865 49.78745 49.88166
52.86590 53.08581 53.39366
9.387269 9.906656 9.814015
34.38975 32.98831 34.74964
62.55169 60.86926 61.68669
ERRORS VALUE RANGE
QC PASS 40.00000 12.00000
QC PASS 25.00000 12.50000
QC PASS 50.00000 15.00000
QC PASS 60.00000 18.00000
QC PASS 10-00000 5.000000
QC PASS 35.00000 10.50000
QC PASS 60.00000 30.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 10.97089 .27257 2.484504
22031 UG/LITER 10.79563 1.08491 10.04950
22032 UG/LITER 9.142460 .809394 8.853131
20681 UG/LITER 60.33104 .65125 1.079456
20682 UG/LITER 62.37754 1.22623 1.965821
19601 UG/LITER 33.20559 2.02247 6.090753
19602 UG/LITER 34.45075 .83499 2.423709
ttl tt2 tt3
11.24698 10.70198 10.96370
11.12504 9.584202 11.67766
8.505176 10.06315 8.869054
60.84072 60.55505 59.59736
63.39607 61.01646 62.72010
32.60283 31.62825 35.48570
35.32212 33.65766 34.37248
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
10.00000 3.000000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 47.89597 2.48453 5.187348
BI2230 UG/LITER 50.95968 2.01899 3.961946
MO2020 UG/LITER 50.10846 .28520 .5691683
TI3349 UG/LITER 49.24743 3.13404 6.363869
B_2496 UG/LITER 55.52453 .91047 1.639767
Y_3710 PPM 1262.400 1.842 .1458761
#1
49.25995 46.02821 49.39974
53,.26051 60,.13479 49,.48373
50.09693 49.82920 50.39925
45-62858 51.04486 51.06885
56 .53717 55 .26289 54,.77352
1262.60 1264.13 1260.46
NOCHECK
QC PASS 50..00000 15..00000
NOCHECK
NOCHECK
QC PASS 50,,00000 15,.00000
NOCHECK
ELEM VtUTS AVGE SDEV %RSD ttl tt2 tt3
#2 tt3 ERRORS VALUE RANGE
232
235 ANALYSIS REPORT
QC STANDARD
08/10/10 01:56:47 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSA RUN TIME: 08/10/10 13:49:51 COMMENT: ICSA MODE: COHC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.444883 .205226 46.13030
AL3082 UG/LITER 250379.0 382.0 .1525882
BA4934 UG/LITER 2.551969 .027476 1.076659
BE3130 UG/LITER 1.079984 .005026 .4663754
CA3179 UG/LITER 250971.8 495.9 -1975830
CD2265 UG/LITER 1.402966 .088908 6-337159
C02286 UG/LITER 5.004919 .140561 2.808459
ttl #2 #3
-.208576 -.547641 -.578432
249972.6 250730.8 250433.5
2.551480 2-524742 2.579687
1.082680 1.083086 1.074185
250894.5 251501.9 250519.2
1.327598 1-501019 1.380281
5.070874 4.843509 5-100373
ERRORS VALUE RANGE
QC PASS .OOOOOOO 20.00000
QC PASS 243900.0 49997.06
QC PASS 2.000000 400.0000
QC PASS .OOOOOOO 10.00000
QC PASS 234100.0 47990-00
QC PASS .OOOOOOO 10.00000
QC PASS 3.000000 100.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 45.01523 .50056 1.111980
CU3247 UG/LITER 22.87042 .21256 .9294260
FE2714 UG/LITER 100253.4 93.5 .0932277
K_7664 UG/LITER 2.432014 3.224236 132.5747
MG2790 UG/LITER 263101.8 227.0 .0862646
MN2576 UG/LITER 17.74021 .09243 .5210069
NA3302 UG/LITER 938.7248 52.7725 5.621720
ttl tt2 #3
44.47348 45.11163 46.46058
22.69355 22.81146 23.10623
100165.0 100243.8 100351.2
6.003362 -.264594 1.557273
262839.8 263229.2 263236.5
17.71861 17.66050 17.84153
941.3289 990.1470 884.6985
ERRORS VALUE RANGE
QC PASS QC PASS 3 6.00000 15.00000 20.00000 50.00000
QC PASS 94900.00 19454.00
QC PASS .OOOOOOO 2000.000
QC PASS 248800.0 51003.00
QC PASS 19.00000 30.00000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 21.76116 .34659 1.592721
TL1908 UG/LITER -1.32112 2.46096 186.2775
V_2924 UG/LITER 1.107688 .304102 27.45374
ZN2138 UG/LITER 28.09572 .01642 .0584305
PB2203 UG/LITER 14.00172 .60228 4.301492
SE1960 UG/LITER -2.64369 1.61796 61.20072
SB2068 UG/LITER 5.209396 1.230329 23.61750
#1 #2 #3
21.50862 21.61856 22.15631
1.472326 -3.16926 -2.26643
1.264588 .7571819 1.301296
28.11348 28.08110 28.09258
13.62618 13.68256 14.69642
-3.88416 -.813616 -3.23330
6.605904 4.285235 4.737049
ERRORS VALUE RANGE
QC PASS 10.00000 80.00000
QC PASS .OOOOOOO 50.00000
QC PASS 1.000000 100.0000
QC PASS 39.00000 120.0000
QC PASS 5.000000 20.00000
QC PASS .OOOOOOO 70.00000
QC PASS .OOOOOOO 120.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.486383 1-738066 357.3431
22031 UG/LITER .2937775 .9842969 335.0485
22032 UG/LITER 20.83140 .60179 2.408795
20681 UG/LITER 4.564910 2.799168 61.31924
20682 UG/LITER 5.521043 .720701 13.05370
19601 UG/LITER -.207294 5.012365 2418.000
19602 UG/LITER -3.87018 .34902 9.018057
ttl tt2 tt3
1.138348 -.278443 -2-31905
-.665512 .2455368 1.301308
20.74730 20.37698 21.36992
7.750925 3.443411 2.500393
6.024132 4.695404 6.843595
-3.41686 5.568559 -2.77358
-4.12758 -4.01003 -3.47293
ERRORS
OC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
-OOOOOOO 20.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -2.60397 3.51345 134.9268
BI2230 UG/LITER 5.568434 .827119 14.85371
MO2020 UG/LITER .8729466 .7383622 84.58285
TI3349 UG/LITER -3.66181 1.84094 50.27412
B_2496 UG/LITER -1.31648 .54857 41.66972
y_3710 PPM 1212.955 .870 .0717299
ttl tt2 tt3
1.277542 -3.52259 -5.56686
6.350202 4.702413 5.652688
1.694757 .6586312 .2654484
-2.72458 -5.78278 -2.47808
-.697542 -1.74265 -1.50925
1212.133 1212-867 1213.867
ERRORS VALUE RANGE
NOCHECK
NOCHECK
NOCHECK
NOCHECK
QC PASS .OOOOOOO 200.0000
NOCHECK
233
236 ANALYSIS REPORT
QC STANDARD
08/10/10 02:03:48 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSAB RUN TIME: 08/10/10 13:56:51 COMMENT: ICSAB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 198.4106 .1042 .0524973
AL3082 UG/LITER 249506.0 856.4 .3432571
BA4934 UG/LITER 511.7964 2.1271 .4156085
BE3130 UG/LITER 486.9876 1.3584 .2789354
CA3179 UG/LITER 250203.4 830.6 .3319586
CD2265 UG/LITER 991.7410 2.6203 .2642126
C02286 UG/LITER 500.5153 1.5657 -3128254
ttl #2
tt3
198.3537 198.3472 198.5308
250490.4 248931.9 249095.8
514.2178 510.2296 510.9417
488.5517 486.3075 486.1036
249949.7 251131.2 249629.2
994.6713 990.9287 989.6231
502.0737 500.6297 498.9423
ERRORS VALUE RANGE
QC PASS 210.0000 43.00000
QC PASS 248400.0 50922.00
QC PASS 475.0000 400.0000
QC PASS 482.0000 98.00001
QC PASS 234300.0 48031.00
QC PASS 916.0000 187.0000
QC PASS 465.0000 100.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 543.7832 1.2624 .2321507
CU3247 UG/LITER 524.1252 .7521 .1435003
FE2714 UG/LITER 100278.9 267.1 .2663564
K_7664 UG/LITER 4.289472 2.246292 52.36756
MG2790 UG/LITER 262612.5 765.7 .2877769
MN2 576 UG/LITER 513.2823 1.5588 .3036981
NA3302 UG/LITER 964.8978 52.3242 5.422771
ttl #2 #3
545.2357 542.9501 543.1639
524.2077 623.3352 524-8326
100586.2 100102.6 100147.9
4.184070 6.586609 2.097736
263484.7 262151.0 262201.9
515.0701 512.5694 512.2073
904.8861 988.8396 1000.968
ERRORS VALUE RANGE
QC PASS 506.0000 103.0000
QC PASS 637.0000 110.0000
QC PASS 95100.00 19495.00
QC PASS .OOOOOOO 2000.000
QC PASS 254100.0 52090.00
QC PASS 483.0000 99.00000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1041.966 3.638 .3491117
TL1908 UG/LITER 103.2550 1.6766 1.623720
V_2924 UG/LITER 505.5879 1.6735 .3309946
ZN2138 UG/LITER 1030.398 3.016 .2927098
PB2203 UG/LITER 63.42813 1.47767 2.329679
SE1960 UG/LITER 48.16845 2.70040 5.606160
SB2068 UG/LITER 622.2918 1.1363 .1825967
ttl tt2 #3
1046.163 1039.735 1039.999
104.8131 103.4709 101.4809
507.4953 604.9018 504.3664
1033.840 1029.141 1028.214
64.05808 61.73988 64.48644
51.17517 45.94963 47-38055
623.5663 621.3845 621.9246
ERRORS VALUE RANGE
QC PASS 930.0000 190.0000
QC PASS 96.00000 50.00000
QC PASS 481.0000 99.99999
QC PASS 975.0000 199.0000
QC PASS 51.00000 20.00000
QC PASS 51.00000 70.00000
QC PASS 585.0000 120.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 101.8991 .4342 .4261169
22031 UG/LITER 46.78883 1.53354 3.277587
22032 UG/LITER 71.71963 2.90381 4.048832
20681 UG/LITER 617.6440 1.3241 .2143752
20682 UG/LITER 624.6062 1.0480 .1677881
19601 UG/LITER 45.61214 7.61429 16.73024
19602 UG/LITER 49.48445 2.68930 5.434629
ttl tt2 tt3
101.4261 101.9914 102.2797
47.04538 48.17792 45.14319
72.53693 68.49504 74.12792
619.0848 616.4807 617-3663
625.7976 623.8267 624.1943
50.52029 36-74977 49-26637
51.49193 60-53250 46-42892
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
97.00000 20-00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 995-9232 4.8001 .4819751
BI2230 UG/LITER 1030.197 5.876 .5703909
MO2020 UG/LITER 986.9152 2.2334 .2263009
TI3349 UG/LITER 1001.439 4.190 .4184348
B_2496 UG/LITER 1023.763 1.992 .1945348
Y_3710 PPM 1207.378 3.754 .3108951
ttl tt2 #3
1000.980 991.4296 995.3597
1036.688 1025.239 1028.665
989.0738 984-6139 987.0578
1006.140 1000.083 998.0947
1025.853 1021.887 1023.548
1203.200 1208-467 1210-467
ERRORS VALUE RANGE
QC PASS 1000.000 205.0000
QC PASS 1000-000 205-0000
QC PASS 1000.000 205.0000
QC PASS 1000.000 205.0000
QC PASS 1000.000 200.0000
NOCHECK
234
237 ANALYSIS REPORT
QC STANDARD
08/10/10 02:10: 49 PM
PAGE
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCV RUN TIME: 08/10/10 14:03:52 COMMENT: CCV CVSl MODE: CONC CORR:. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 98.45142 .29285 .2974570
AL3082 UG/LITER 49318.07 240.64 .4879371
BA4934 UG/LITER 992.8649 4.2983 .4329222
BE3130 UG/LITER 983.8823 4.1844 .4252972
CA3179 UG/LITER 49083.45 685.84 1.397293
CD2265 UG/LITER 984.8550 4.1143 .4177523
C02286 UG/LITER 976.6477 3.2966 .3375470
#1 #2 tt3
98.12594 98.69358 98.53474
49040.84 49472.97 49440.41
987.9020 995.2935 995.3993
979-0794 985.8269 986.7405
48614.71 48765.02 49870.62
980-1448 986.6734 987.7467
972.8708 978.1252 978.9472
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 996.2576 4.6484 .4665850
CU3247 UG/LITER 991.7719 3.0777 .3103184
FE2714 UG/LITER 24959.29 95.21 .3814582
K_7664 UG/LITER 48069.84 255.53 .5315906
MG2790 UG/LITER 49993.66 226.07 .4522003
MN2576 UG/LITER 972.5200 4.2529 .4373046
NA3302 UG/LITER 49219.27 295.01 .5993763
ttl #2 #3
990.9543 998.1926 999.6259
989.1229 995.1480 991.0448
24849.50 25019.02 25009.37
47797.92 48305.01 48106.59
49733.32 50107.19 50140.46
967-6097 974.9134 975.0369
48880.15 49416.74 49360.91
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000-000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1000.330 4.334 .4332351
TLI908 UG/LITER 997.5687 2.7723 .2779042
V_2924 UG/LITER 997.0618 4.9729 .4987562
ZN2138 UG/LITER 1070.359 3.853 .3599593
PB2203 UG/LITER 990.9872 3.0101 .3037437
SE1960 UG/LITER 985-6877 2.0629 .2092855
SB2068 UG/LITER 1019.762 1.510 .1480377
ttl tt2 #3
996.3476 1002.413 1003.228
994.9102 997.3536 1000.442
991.3379 999.5263 1000.321
1065.911 1072.648 1072.520
987.5116 992-7086 992.7416
983.5168 985.9239 987.6223
1018.394 1019.510 1021.382
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
OC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104-0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1000.610 4.530 .4527244
22031 UG/LITER 981.4704 3.4302 .3494985
22032 UG/LITER 995.7247 3.1426 .3156140
20681 UG/LITER 1005.222 2.830 .2815026
20682 UG/LITER 1027.017 1.632 .1588830
19601 UG/LITER 978.8907 3.8938 .3977793
19602 UG/LITER 989.0714 4.2001 -4246519
ttl tt2 tt3
996.2995 1000.199 1005.332
978.0224 984.8826 981.6063
992.2369 996.6011 998.3362
1001.983 1007.212 1006.471
1026.584 1025.646 1028.822
982.0835 974.5527 980.0358
984.2228 991.5913 991.4001
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALlrt: RANGE
1000-000 104.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 996.6476 4.9965 -5013276
BI2230 UG/LITER 1009.727 5-725 .5670232
MO2020 UG/LITER 1004-854 6-517 .6485079
TI3349 UG/LITER 998.4072 5.2024 .5210722
B_2496 UG/LITER 1020.583 5.562 .5450235
Y_3710
#1 #2
tt3
992-6140 1002.237 995.0920
1003-740 1015-149 1010.293
997-3389 1008.279 1008.943
992-6050 999-9607 1002.656
1014-171 1023.468 1024.111
1259.533 1255-867 1253-467
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000-000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000-000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
PPM 1256.289 3.055 .2431991
235
238 ANALYSIS REPORT
QC STANDARD
08/10/10 02:17:51 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCB RUN TIME: 08/10/10 14:10:53 COMMENT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.449791 .316037 70.26311
AL3082 UG/LITER 47.25583 15.73329 33.29386
BA4934 UG/LITER --270726 .117457 43.38612
BE3130 UG/LITER .5505418 .0629169 11.42817
CA3179 UG/LITER 448.4104 1.2162 .2712314
CD2265 UG/LITER .2941605 .0531440 18.06633
C02286 UG/LITER .1580367 .0202066 12.78599
ttl tt2 #3
-.267150 -.257504 -.814720
33.93393 43.21951 64.61406
-.320760 -.354882 -.136536
.5077249 .5211213 .6227790
449.5725 448.5122 447.1465
.3223682 .2328599 .3272532
.1355001 .1640720 .1745378
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS -OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS -OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .0456923 .4202826 919.8096
CU3247 UG/LITER -.707454 .027230 3.848972
FE2714 UG/LITER 7.534563 7.560309 100.3417
K_7664 UG/LITER 5.805206 2.784130 47.95920
MG2790 UG/LITER 29.26556 17.40327 59.46672
MN2576 UG/LITER -.179050 .040494 22.61605
NA33 02 UG/LITER -46.8786 16.4307 35.04957
ttl #2 tt3
.4130497 -.412620 .1366478
-.723175 -.676012 -.723175
4.957673 1.599573 16.04644
7.662033 2.604013 7.149572
15.57795 23.36728 48.85146
-.214459 -.187792 -.134899
-45.4341 -31.2178 -63.9838
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS -OOOOOOO 5000.000
QC PASS -OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER .1595886 .1570158 98.38782
TL1908 UG/LITER 3.493390 3.350584 95.91212
V_2924 UG/LITER .2290874 .1359803 59.35738
ZN2138 UG/LITER .3676227 .1561749 42.48239
PB2203 UG/LITER 2.404479 .618733 25.73250
SE1960 UG/LITER -.027120 2.336603 8615.819
SB2068 UG/LITER .8012096 .4922051 61.43275
ttl tt2 tt3
.0717423 .3408661 .0661574
.3372405 3.133564 7.009364
.3662562 .2266783 .0943277
.2587265 Q3.112948 .2975846 2.130150 .5465571 1.970341
-1.02877 -1.69592 2.643321
.4084366 1.353352 .6418406
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .4584406 .3488211 76.08862
22031 UG/LITER 4.747302 1.197668 25-22840
22032 UG/LITER 1.225127 1.434159 117.0621
20681 UG/LITER -.768797 .485017 63.08778
20682 UG/LITER 1.575342 .911874 57.88420
19601 UG/LITER -.420136 4.442463 1057.388
19602 UG/LITER .1593937 1.669346 1047.310
ttl #2 tt3
.5505110 .0728197 .7519910
3.593442 5-984433 4.664031
2.863331 .1961957 .6168642
-.210120 -1.01420 -1.08207
.7076207 2.525662 1.492842
-.398712 -4.87327 4.011577
-1-35305 -.119320 1.950554
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.910108 2.018391 221.7749
BI2230 UG/LITER 1.933399 .849264 43.92593
MO2020 UG/LITER 1.840561 .558482 30.34302
TI3 349 UG/LITER -1.79238 .24141 13.46863
B_2496 UG/LITER 1.894406 .198651 10.48619
Y_3710 PPM 1259-711 4.336 .3442107
ttl tt2 #3
-1-22276 -2.75393 1.246365
1-635624 1.273123 2.891450
2.485232 1.532411 1-504039
-1-54042 -1.81509 -2.02164
2.116636 1.836280 1.731301
1255.733 1259.066 1264.333
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS -OOOOOOO 50.00000
QC PASS .OOOOOOO 50-00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
236
239
Daily Instrument Profile
Maintenance:
[MoMt
Nebulizer pressure: ^ Peak position: - o . t^^^'T-v— Peak intensity: "^yfjTJf^ . I C * Vernier position: } ' * ) ' \
Printed: 8/12/2010 5:32:00 PM Method(s)
(circle one): iJLM05.4^
Operator(s):
T 1
RR RR#X #X L W S B
6010B
6010C
Other
Date/Time Ob.l-Z.U \ »'> < ^ ^
^^t2:?\y\
Ofe -l-^-'U
l 4 - ^
Specified elementfs) fall(s) high Specified elementfs) fallfs) low Re-run sanriple(s) neat '^e-run at a #-fold dilution Sample run at a #-fold dilution (aliquot of sample diluted with acidified water) Matrix = leachate Vlatrix = water Vlatrix = solid Vlatrix = biolopical tissue
SDG
Matrix
Coniments
MC0022
CoMPLEHtgr Ar/ox-\y\.^^
yc^L
MG68M3
TAL_
MY71L3
Iz
MY71S3 vMYSISl.
/AU
''
J '
''_y_
CoHV\jr\E t^^\\z..\o7^^
ICP Run Log (P3) File Name: Seq
P30812A
Sample ID
Client ID
Sample Type
DF
Date
Time
SDG
1
CALI
SO BLANK
CALIB STD
08/12/10
10 54:29
2
CAL2
8 RSTD-1
CALIB STD
08/12/10
01:30
3
CAL4
S RSTD-3
CALIB STD
08/12/10
08:30
4
CAL3
S RSTD-2
CALIB STD
08/12/10
13:57
5
CALS
S RSTD-4
CALIB STD
08/12/10
19:25
6
ICVl
ICVl
ICV
08/12/10
26:26
7
ICBI
ICB
ICB
08/12/10
33:27
8
CRLI
CRI
CRI
08/12/10
40:27
9
IFA1
ICSA
ICS
08/12/10
47:27
10
IFB1
ICSAB
ICS
08/12/10
54:27
11
CCV1
CCV
CCV
08/12/10
12 01:28
12
CCBl
CCB
CCB
08/12/10
12 08:29
13
1007154-12RE2
MY71M4
SAMPLE
08/12/10
12 18:28
MY71L3
14
0080327-PS2
MG68M9A
SAMPLE
08/12/10
12 25:29
MG68M3
10
Action Needed
The presence of the Chemist's/Analyst's employee ID number, cr signature, on this run log attests that strict compliance vinth the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials of the lab supen/isor and a QA department representative, signifying approval of the deviation.
237 Reviewed By:
Date:
^ ' >V n
o
Page 1 of 3
240 ICP Run Log {P3) File Name: P30812A DF
Date
Time
SDG
15
0080337-BS2
LCSS
LCS
2
08/12/10
12:32:29
MC0022
16
1008009-09RE1
MC0037
SAMPLE
3
08/12/10
12:39:29
MC0022
17
1008009-09RE2
MC0037
SAMPLE
25
08/12/10
12:57:03
MC0022
18
1008009-12RE1
MC0040
SAMPLE
3
08/12/10
13:04:02
MC0022
5
08/12/10
13:11:02
MC0022
Seq
Sample ID
Client ID
Sample Type
Action Needed
?b4-Z^;c M ^K-t''Z
19
1008009-12RE2
MC0040
SAMPLE
20
1008009-15RE1
MC0043
SAMPLE
3
08/12/10
13:18:02
MC0022
21
1008009-15RE2
MC0043
SAMPLE
5
08/12/10
13:25:02
MC0022
22
IBLI
IBL
SAMPLE
1
08/12/10
13:35:08
23
CCV2
CCV
CCV
1
08/12/10
13:42:09
24
CCB2
CCB
CCB
1
08/12/10
13:49:10
25
1008009-15RE3
MC0043
SAMPLE
25
08/12/10
13:57:30
26
CRL2
CRI
CRI
1
08/12/10
14:04:30
27
1FA2
ICSA
ICS
1
08/12/10
14:11:30
28
IFB2
ICSAB
ICS
1
08/12/10
14:18:30
29
CCV3
CCV
CCV
1
08/12/10
14:25:31
30
CCB3
CCB
CCB
1
08/12/10
14:32:32
31
0081015-BLKl
PBW
PBW
1
08/12/10
14:40:36
MY71S3
32
0081015-BSl
LCSW
LCS
1
08/12/10
14:47:36
MY71S3
33
1007157-07RE1
MY71T5
SAMPLE
1
08/12/10
14:54:37
MY71S3
34
0081015-DUPl
MY71T5D
SAMPLE
1
08/12/10
15:01:37
MY71S3
35
0081015-MS1
MY71T5S
SAMPLE
1
08/12/10
15:08:37
MY71S3
36
SRD1
MY71T5L
SAMPLE
5
08/12/10
15:15:37
MY71S3
37
0081015-PS1
MY71T5A
SAMPLE
1
08/12/10
15:22:37
MY71S3
38
IBL2
IBL
SAMPLE
1
08/12/10
16:00:29
39
CCV4
CCV
CCV
1
08/12/10
16:07:30
40
CCB4
CCB
CCB
1
08/12/10
16:14:31
41
1007157-07RE1
MY71T5
SAMPLE
2
08/12/10
16:24:57
42
0081015-DUPl
MY71T5D
SAMPLE
2
08/12/10
16:31:57
43
SRD2
MY71T5L
SAMPLE
10
08/12/10
16:38:57
M^ffi1G3 '
44
0072812-BS>sf
LCSS
LCS
2
08/12/10
16:48:20
MY71L3
Tb-f f bt i 5 ' •
^ . 1 y. 1 c y*v
45
CRL3
CRI
CRI
1
08/12/10
16:55:20
46
IFA3
ICSA
ICS
1
08/12/10
17:02:20
^
*
1
MC0022
tiA2x (Mm u UAi ' y MK-t J'
MY71S3
7l^^+ (\9^ l ' i ^^ -IS-r.df^J
The presence of the Chemist's/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together wflth the chemists/analyst's initials and the initials of the lab supervisor and a QA department representative, signifying approval of the deviation.
Reviewed By:
tei.
Date:
^ ^ • ^ • ^ ^ ^ 0
Page 2 of 3
238
241 ICP Run Log (P3) File Name: P30812A Seq
Sample ID
Client ID
Sample Type
DF
Date
Time
47
IFB3
ICSAB
ICS
1
08/12/10
17:09:20
48
CCV5
CCV
CCV
1
08/12/10
17:16:21
49
CCB5
CCB
CCB
1
08/12/10
17:23:22
SDG
Action Needed
The presence of the Chemisfs/Analyst's employee ID number, or signature, on this ain log attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together vjUti the chemist's/analyst's initials and the initials of the lab supervisor and a QA department representative, signifying approval of the deviation.
Reviewed By:
^^^-^-...^^
Date:
c^^-^ir '^^
Page 3 of 3
239
242
o Daily Standards/QC Preparation Log for Trace ICP (P3 & P4) i of 3 compuChem a division of Liberty Analytical corp. worksheet i P(6) n STANDARDS and REAGENTS TRACEABILITY Seq. File Name: ? ^ 0 $ M 2 . / ^ Ref#* HNO3 [Baker Instra-analyzed Trace-Metals grade] HCI [Baker Instra-analyzed Trace-Metals grade] SM-770-027 multi-elenfient standard mix (RSTD-1) SM-770-028 part A multi-element standard mix (RSTD-2A) SM-770-028 part B multi-element standard mix (RSTD-2B) SM-770-029 part A multi-element standard mix (RSTD-3A) SM-770-029 part B multi-element standard mix (RSTD-3B) SM-770-030 multi-element standard mix (RSTD-4) SPEX-R multi-element standard mix ICP-AES-CRQL-R multi-element standard mix ICVl multi-element standard mix ICSA multi-element standard mix ICSB multi-element standard mix SM-770-031 multi-element standard mix (PDS-R) ARSENIC (As) 1,000 PPM single-element standard Internal Mix SM-770-040 multi-element CCV mix (Soln A) SM-770-040 multi-element CCV mix (Soln B) SM-770-042 (LRS 601 OB)
0 0 ( 0 ^ 0 e> I oCfi^ I - 2 0 OFI2002 9J22002 9J22001 OD14008 9G08005 OFI2003 0F12001 9104002 0B04003 0B04002 0B04001 9122001 9F17001 0B04004 OE03001 0E03001 0B23007
10
Manufacturer JT Baker Caledon High Puritv High Purity High Purity High Purity High Puritv High Purity High Purity High Puritv EPA EPA EPA Hiqh Purity High Purity Hiqh Purity High Purity High Purity High Purity
^Lot#
'1loo'?>ft 'rr-z^a^h 1015827 0928011 0928012 0925430 0906204 1015830 1015828 0923808 0307 1206 0203 0926418 0911221 0934101 1010910 1010911 1004021
Expiration Date
oi.(
Multi-Element Stock Standard Concentrations: RSTD-1 multi-element standard mix RSTD-2/V2B multi-element standard mix RSTD-3/V3B multi-element standard mix RSTD-4 multi-element standard mix SPEX-R multi-element standard mix ICP-AES-CRQL-R multi-element standard mix PDS-R multi-element standard mix Intemal Mix LRS 601 OB multi-element standard mix
Entered By:
Cd:1,000 Crr1,000 Cur1,000 Pbrl.OOO Nirl.OOO Ser1,000 AgrlOO Tlrl.OOO Znrl.OOO Part Ar AsrI.OOO Barl.OOO Berl.OOO Corl.OOO Mnrl.OOO Morl.OOO Vrl.OOO Part B: Fe:25,000 Part Ar CarlO.OOO MgrlO.OOO KrlO.OOO NarlO.OOO Part Br AlrlO.OOO Sbrl.OOO Birl.OOO BrI.OOO Sn:1,000 Tlrl.OOO Morl.OOO Snrl.OOO Birl.OOO Tlrl.OOO 6:1,000 AgrlO Ber5 CdrS CorSO Cr:10 Cur25 MnrlS Nir40 Tlr25 VrSO Znr60 PbrlO Se:35 AsrIO Sbr60 Alr400 Bar400 Agr20 BerlO CdrlO CorlOO Crr20 CurSO Fer200 Mnr30 NIrSO Tl:20 VrlOO Znr40 Pb:6 Se;10 Asr20 Sbr120 LIrSO.OOO Y:2S0 Air 20 Sbri Asri Bar20 BerO.5 Bi:2 Br2 CdrO.S CarSOO Crri CorO.S CurO.5 FerlO Pb:0.3 Mgr500 Mnri Mor2 NirO.S CrSOO SerO.S TirO.5 Vr2 Znr2
^ 17/n--^^-.^
Reviewed By; *Ref# = Logbook ID, Page number, and item number from Materials Receipt Log "High Purity is abbreviated "HP" on reporting fornis
^
Date: R'^?h' ^ n 03/25/10: Jcf
243
Daily Standards/QC Preparation Log for Trace ICP
As-
• O ^ M . [ D - 5 A ^
ICSA-
^i>.\\.\t:> ' f ^ ( ^
ICSAB-
0\-\-
\\ocft>
M . \ O ' ^ ^ Y \ C?|4(l
cfb
EPA-CRl-
On w^oq-
0
oft.D^.lo-^^H^ OH-o^OoQ,
P3R1NSE-
P4R1NSE-
^.IO.lo-^(^ Og>JO.tO-5»^H\
PSRINSE-
P3INTSTDP41NTSTD-
^.[o.lO'-'T^^
P51NTSTD-
Asri,000 Al:244,100 Ba:2 Ca:234,900 Co:4 Cr:43 Cu:23 Fer95,600 Mg:247,500 Mn:19 Nl:21 Zn:28 PbrlO
In a 500-mL volumetric flask, combine 350 mL deionized water, 5 mL concentrated HNO3, and 25 mL concentrated HCI. Pipet 50.0 mL ICSA and 50.0 mL ICSB into flask. Add 0.5 mL Compuchem SPEX-R. Bring up to volume with deionized water and transfer to a 500mL Teflon bottle. Final volume 500 mL.
Agr206 Alr241,100 Bar495 Ber475 Car231,100 Cdr940 Cor461 Cr:511 Cu:548 Fe:94,800 Mgr251,l00 Mn:502 Ni:984 Tl:103 V:494 Zn:1028 Pb:61 Ser53 Sb:589 AsrIOl Snrl.OOO BIrl.OOO Mo:1,000 Tlrl.OOO BrI.OOO
In a 500 mL volumetric flask, combine 300 mL deionized water, 5 mL concentrated HN03,and 25 mL concentrated HCI. Pipet 0.50 mL ICP-AESCRQL-R and 25 pL Compuchem SPEX-R into flask. Bring up lo volume with deionized water and transfer to a 500mL Teflon bottle. Final volume 500 mL. Prepare as needed.
AgrlO Mn:15 Se:35 BlrSO
BerS Cdr5 CorSO CnIO Cur2S Nlr40 Tl:25 VrSO Znr60 PbrlO AsriO SbrBO SnrSO BrSO MorSO TlrSO
o ( - t \t> o o T ) ^
In a 10 L container, combine 8 L delonlzed vrater and 400 mL concentrated HNO3 Fill with deionized water. Final volume 10 L.
N/A
0 \ ^ \ o o c *1
In a 10 L container, combine 8 L delonlzed water and 400 mL concentrated HNO3 Fill with deionized water. Final volume 10 L.
N/A
In a 10 L container, combine 8 L deionized water and 400 mL concentrated HNO3 Fill with deionized water. Final volume 10 L,
N/A
N'*" O ^ . ^ l ^ . - ^ t ^
In a 100 mL volumetric flask, combine 50 mL deionized water, 1 mL concentrated HNO3, 5 mL concentrated HCI, and 0.1 mL 1000-ppm As standard. Bring to final 100 mL volume In a 500-mL volumetric flask, combine 350 mL deionized water, 5 mL concentrated HNO3, and 25 mL concentrated HCI. Pipet 50.0 mL ICSA into flask. Bring up to volume with deionized water and transfer to a 500mL Teflon bottle. Final volume 500 mL.
Kv A ^ A - ^ ^ e>o Zl 0\J^ I o o o € >
(MA
MA
In a 10 L container, combine 8 L deionized water, 400 mL concentrated HNO3, and 200 mL Intemal Mix. Fill with deionized water. Final volume 10 L
Ll: 1,000,000
Y:5,000
In a 10 L container, combine 8 L deionized water, 400 mL concentrated HNO3, and 200 mL Intemal Mix. Fill with deionized water. Final volume 10 L.
un,000,000
YrS.OOO
In a 10 L container, combine 8 L deionized water, 400 mL concentrated HNO3, and 200 mL Intemal Mix. Fill with deionized water. Final volume 10 L.
Uri,000,000
YrS,000
Standard Solutions Prepared By: Entered By:
-y
J o m
^aow^^^oU
Reviewed By: •Standard Lot Number consists of standard ID, date prepared, and initials of preparer.
Date •
'^
• ^ e ^ • ^c 03/25/10; jcf
244
Dally Standards/QC Preparation Log for Trace ICP (P3 & P4) 2 of 3 compuchem a division ofLiberty Ajiaiyticaicorp. workstieet 1 F(6^ •SfivtWi^i
^I<2i^.:t-Zi^fMl^UZl \ty. ' <''.y/SS^'&
0\^\\ooz^
Place in a SOO mL volumetric flask 100 mL deionized water 20 mL concentrated HNOs, and 100 mL concentrated HCI. Bring up to volume with deionized vrater. Transfer to a 2L Teflon bottle and add 1.5L deionized vrater. Final volume 2 L. Prepare as needed.
N/A
C?(&.hjt?-f^M OWWQO^
In a 200 mL volumetric flask, combine 150 mL deionized vrater, 2 mL concentrated HNO3, and 10 mL concentrated HCI. Pipet 0.4 mL RSTD-1 into flask. Bring up to 200 mL volume with deionized water. Prepare as needed.
Cd:2,000 Cr;2,000 Cu:2,000 Pbr2,000 Nir2,000 Se:2,000 Ag:200 Tlr2,000 Zn:2,000
SO/ICB/CCB-
RSTD-1-
^^.u.lD-^^^^
RSTD-2- ^ g ) . n . | i ? - ' ^ H t > \ \
\\ 0 0 ^
RSTD-3- O h - \ \ \ ^ - % V \ Q H
\Vi3o<
RSlD-A-0'd • l l . W - ^ 4 ' ^
1CV1-
0\\]\0^^
c^fc-0=^.1*?.^^^ O l^cp^oo)
CCV/CVS1-
ot>.oo.\o-^t^ OHoCeOi^
LRS- p - : } ' . ' M . i o - < ) ^ M (fp^ 2> I o 0 3
in a 200 mL volumetric flask, combine 150 mL deionized water, 2 mL concentrated HNO3, and 10 mL concentrated HCI. Plpet 0.4 mL each RSTD-2A and RSTD-2B into flask. Bring up to 200 mL volume with deionized water. Prepare as needed, In a 200 mL volumetric flask, combine 150 mL deionized vrater, 2 mL concentrated HNO3, and 10 mL concentrated HCI. Pipet 2.0 mL each RSTD-3A and RSTD-3B Into flask. Bring up to 200 mL volume with deionized vrater. Prepare as needed. In a 200 mL volumetric flask, combine 1S0 mL deionized water, 2 mL concentrated HNO3, and 10 mL concentrated HCI. Pipet 0.4 mL RSTD-4 into flask. Bring up to 200 mL volume with deionized water. Prepare as needed.
Place in a 500 mL volumetric flask: 300 mL delonlzed vrater, 5 mL concentrated HN03,and 25 mL concentrated HCI. Plpet 50.0 mL ICVl Into flask and 0.55 mL Compuchem SPEX-R. Bring up to volume with deionized vrater. Transfer to a SOOmL Teflon bottle. Final volume 500 mL. Prepare as needed.
Place in a 500-mL volumetric flask: 300 mL deionized water, 20 mL concentrated HNOs.and 100 mL concentrated HCI. Add SO ml of SM-770-40 Soln A and Soln B. Bring up to volume with deionized vrater. Transfer to a 2000mL Teflon bottle and add 1.5 L of deionized vrater. Prepare as needed.
In a 500 mL volumetric flask, combine 200 mL deionized water, 5 mL concentrated HNOsand 25 mL concentrated HCI. Pipet S.OmL of LRS 6010B. Bring up to volume with deionized vrater and transfer to a SOOmL Teflon bottle. Final volume 500 mL. Prepare as needed,
Asr2,000 Ba:2,000 Ber2,000 Co:2,000 Fer50,000 Mn:2,000 Mor2,000 V:2,000 KrIOO.OOO Na:100,000 Al:100,000 MgrlOO.OOO Ca:100,000 Snr2,000 Blr2,000 Tl:2,000 Sb:2,000 B:2,000
AI:2,S21 Bar497 Kr10,021 Mgr6,074 Na:10,097 Ca:10,026 Agr501 Be:495 Cd:496 Co:499 Crr490 Cur492 Fe:5,082 Mn:499 Ni:S03 Tl: 1,028 V:S01 Zn:1,02S Pb:1002 Se:1,029 As:999 Sb:994 Mori,100 Sn:1,100 Bl:1,100 Tl:1,100 8:1,100 AI:SO,000 Ba:1,000 K:50,000 Mg:50,000 Na:50,000 CarSO.OOO AgrlOO Be:1,000 Cd:1,000 Co;1,000 Cr.l.OOO Cu:1,000 Fe:2S,000 Mn:1,000 Nlrl.OOO Tl:1,000 V:1,000 Znr1,100 Pbrl.OOO Se:1,000 /\s:1,000 Mo:1,000 Snrl.OOO Bin,000 Tl:1,000 Sb:1,000 B:1,000 Al:200 Ba:200 KrS.OOO Mg:5,000 Na:5,000 Ca:5,000 Ag;5 Be:5 CdrS Co:10 CrrlO CurS FerlOO MnrlO Nl;5 Tl:10 V:20 Znr20 Pbr3 SerS AsrIO Mo:20 Sn;20 Blr20 Tlr20 SbrlO Br20
'^^y l ^ ^ y y A f ^ 't'\?lr^•^^..u>M
Standard Solutions Prepared By Entered By: _ Reviewed By:
•Standard Lot Number consists of standard ID, date prepared, and initials of preparer.
Date:
• U -NO 03/25/10: Jcf
245 08/12/10 11:01:26 AM
STANDARDIZATION RPT.
PAGE 1
METHOD: ALT-P3Q3 STANDARD: SO BLANK RUN TIME: 08/12/10 10:54:29 ELEM AVGE SDEV %RSD
AG3280 -.19132 .02995 15.656
AL3082 9.7224 .1089 1.1205
BA4934 .40360 .00631 1.5629
BE3130 1.7385 .0411 2.3661
CA3179 .00000 .00000 .00000
CD2265 -.15031 .03119 20.748
C02286 -.01203 .01006 83.664
#1 #2 #3
-.21599 -.15799 -.19999
9.5970 9.7762 9.7939
.40240 .41042 .39797
1.6938 1.7469 1.7748
.00000 .00000 .00000
-.18041 -.11814 -.15238
-.00178 -.02189 -.01242
ELEM AVGE SDEV %RSD
CR2677 -.00496 .00799 161.15
CU3247 .88296 .00721 .81666
FE2714 .02040 .00193 9.4806
K_7664 .42004 .11434 27.222
MG2790 .00914 .00259 28.338
MN2576 .00855 .00053 6.1927
NA3302 -.35870 .03316 9.2454
#1 #2 #3
-.01083 .00415 -.00820
.89096 .87696 .88096
.01832 .02073 .02215
.53381 .42116 .30514
.01018 .01104 .00619
.00916 .00829 .00820
-.32229 -.38717 -.36666
ELEM AVGE SDEV %RSD
NI2316 -.00437 .00308 70.531
TL1908 -.03229 .01124 34.794
V_2924 -.02705 .00400 14.772
ZN2138 .01792 .00114 6.3567
AS1890 -.09882 .15039 152.18
22031 .04937 .07408 150.06
22032 .12790 .05488 42.907
#1 #2 *3
-.00526 -.00094 -.00692
-.02915 -.04477 -.02297
-.02920 -.02244 -.02951
.01666 .01824 .01887
.06079 -.11938 -.23787
.13491 .00663 .00656
.13325 .17990 .07054
ELEM AVGE SDEV %RSD
20681 .00892 .02001 224.31
20682 -.05497 .06413 116.68
19601 -.22390 .08039 35.904
19602 .25565 .10722 41.941
SN1899 -.04354 .00588 13.504
BI2230 .05390 .12885 239.07
MO2020 .08934 .04754 53.215
Itl #2 «3
.01749 .02321 -.01394
.01749 -.10446 -.07792
-.21069 -.31007 -.15093
.17155 .37639 .21901
-.03748 -.04394 -.04922
-.07079 .18654 .04593
.11333 .12010 .03458
ELEM AVGE SDEV %RSD
TI3349 .81568 .34631 42.457
B_2496 .39940 .02122 5.3128
#1 #2 #3
.43305 1.1076 .90639
.42389 .38634 .38798
243
246 08/12/10 11:08:27 AM
STANDARDIZATION RPT.
PAGE 1
METHOD: ALT-P3Q3 STANDARD: S RSTD-1 RUN TIME: 08/12/10 11:01:30 ELEM AVGE SDEV %RSD
AG3280 27.009 .041 .15058
CD2265 701.96 14.24 2.0291
CR2677 38.639 .787 2.0365
CU3247 • 191.37 .21 .10876
NI2316 34.280 .702 2.0486
TL1908 14.486 .276 1.9052
ZN2138 32.344 .641 1.9824
#1 #2 #3
27.014 27.048 26.967
718.13 696.49 691.27
39.532 38.335 38.049
191.49 191.49 191.13
35.074 34.025 33.740
14.790 14.417 14.251
33.069 32.112 31.852
ELEM AVGE SDEV %RSD
22031 216.99 3.47 1.6001
22032 192.83 3.29 1.7063
19601 48.499 .876 1.8061
19602 87.025 1.253 1.4401
#1 #2 #3
220.93 215.67 214.38
196.60 191.38 190.51
49.496 48.148 47.854
88.470 86.227 86.380
244
247 STANDARDIZATION RPT.
08/12/10 11:13:53 AM
PAGE 1
METHOD: ALT-P3Q3 STANDARD: S RSTD-3 RUN TIME: 08/12/10 11:08:30 ELEM AVGE SDEV %RSD
AL3082 2101.9 80.0 3.8057
CA3179 .12689 .00458 3.6122
K_7664 772.04 23.55 3.0503
MG2790 310.78 11.67 3.7565
NA3302 47.761 1.652 3.4596
ftl #2 #3
2046.5 2193.6 2065.7
.12421 .13218 .12428
756.15 799.10 760.88
302.57 324.15 305.62
46.585 49.650 47.048
245
248 STANDARDIZATION RPT.
08/12/10 11:19:21 AM
PAGE 1
METHOD: ALT-P3Q3 ' STANDARD: S RSTD-2 RUN TIME: 08/12/10 11:13:57 ELEM AVGE SDEV %RSD
BA4934 413.57 4.23 1.0223
BE3130 1858.1 14.7 .78971
C02286 122.91 1.02 .82660
FE2714 67.409 .502 .74445
MN2576 62.422 .531 .85112
V_2924 18.617 .153 .82285
AS1890 185.09 1.68 .90963
#1 #2 #3
418.06 409.67 412.97
1875.0 1848.5 1850.9
124.08 122.25 122.39
67.984 67.060 67.183
63.034 62.083 62.149
18.791 18.505 18.554
187.02 183.89 184.36
ELEM AVGE SDEV %RSD
MO2020 146.94 .70 .47437
ftl ff2 #3
147.73 146.42 146.68
246
249 STANDARDIZATION RPT.
08/12/10 11:26:22 AM
PAGE 1
METHOD: ALT-P3Q3 STANDARD: S RSTD-4 RUN TIME: 08/12/10 11:19:25 ELEM AVGE SDEV %RSD
20681 20.406 .065 .31905
20682 79.360 .045 .05730
SN1899 28.160 .022 .07777
BI2230 178.35 .46 .25998
TI3349 269.94 .50 .18658
B_24 96 161.00 .30 .18379
ftl #2 #3
20.340 20.408 20.471
79.368 79.400 79.311
28.136 28.180 28.163
178.26 177.94 178.85
269.49 269.84 270.49
160.66 161.14 161.20
247
250 ANALYSIS REPORT
QC STANDARD
08/12/10 11:33:23 AM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICVl RUN TIME: 08/12/10 11:26:26 COMMENT: ICVl MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 510.2856 .9038 .1771239
AL3082 UG/LITER 2485.922 11.230 .4517638
BA4934 UG/LITER 508.2357 2.0191 .3972730
BE3130 UG/LITER 495.5665 2.0201 .4075392
CA3179 UG/LITER 9839.246 619.603 6.297259
CD2265 UG/LITER 500.4107 1.5634 .3124141
CO2206 UG/LITER 510.0976 1.7798 .3489065
#1 #2 ff3
509.4417 510.1758 511.2394
2473.398 2489.271 2495.097
505.9522 508.9700 509.7848
493.2916 496.2570 497.1508
10449.93 9856.721 9211.091
498.6057 501.3321 501.2944
508.0676 510.8356 511.3897
ERRORS VALUE RANGE
QC PASS 501.0000 10.40000
QC PASS 2521.000 10.40000
QC PASS 497.0000 10.40000
QC PASS 495.0000 10.40000
QC PASS 10026.00 10.40000
QC PASS 496.0000 10.40000
QC PASS 499.0000 10.40000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 498.9101 2.2125 .4434704
CU3247 UG/LITER 511.4420 .9967 .1948786
FE2714 UG/LITER 5057.037 15.596 .3083982
K_7664 UG/LITER 9781.228 25.225 .2578960
MG2790 UG/LITER 5873.150 24.433 .4160124
MN2576 UG/LITER 496.0943 1.9925 .4016376
NA3302 UG/LITER 9977.557 76.749 .7692152
#1 tf2 ff3
496.6502 499.0081 501.0720
510.3747 511.6030 512.3484
5040.147 5060.069 5070.893
9752.469 9799.609 9791.604
5846.563 5878.268 5894.618
493.8153 496.9609 497.5068
9889.052 10017.87 10025.75
ERRORS VALUE RANGE
QC PASS 490.0000 10.40000
QC PASS 492.0000 10.40000
QC PASS 5082.000 10.40000
QC PASS QC PASS 10021.00 ,6074.000 10.40000 10.40000
QC PASS 499.0000 10.40000
OC PASS 10097.00 10.40000
ELEM UNITS AVGE SDEV %RSD
NI2315 UG/LITER 504.4487 2.0437 .4051318
TLI908 UG/LITER 1028.474 5.912 .5747863
V_2924 UG/LITER 509.3365 2.1758 .4271919
ZN2138 UG/LITER 984.2966 4.0895 .4154708
PB2203 UG/LITER 1008.425 9.658 .9577687
SE1960 UG/LITER 1007.251 9.595 .9525845
SB2068 UG/LITER 1022.229 6.645 .6500671
ffl #2 it3
502.0972 505.4530 505.7959
1022.118 1029.495 1033.808
507.0737 509.5225 511.4135
979.5875 986.3489 986.9535
997.6716 1011.241 1016.362
996.5856 1009.986 1015.182
1014.570 1026.463 1025.655
ERRORS VALUE RANGE
QC PASS 503.0000 10.40000
QC PASS 1028.000 10.40000
QC PASS 501.0000 10.40000
QC PASS 1025.000 10.40000
QC PASS 1002.000 10.40000
QC PASS 1029.000 10.40000
QC PASS 994.0000 10.40000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1011.568 2.456 .2427494
22031 UG/LITER 1007.532 5.451 .5410259
22032 UG/LITER 1008.858 11.771 1.166777
20681 UG/LITER 1023.211 13.390 1.308644
20682 UG/LITER 1021.736 3.953 .3868706
19601 UG/LITER 1001.405 7.329 .7318817
19602 UG/LITER 1010.160 12.894 1.276392
tfl ft2 (f3
1009.573 1010.819 1014.310
1001.628 1008.595 1012.373
995.6841 1012.549 1018.342
1008.092 1027.970 1033.572
1017.801 1025.706 1021.699
995.2543 1009.514 999.4461
997.2403 1010.212 1023.027
ERRORS
OC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
999.0000 10.40000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1114.688 4.493 .4030570
BI2230 UG/LITER 1096.326 5.173 .4718797
MO2020 UG/LITER 1096.386 9.829 .8964823
TI3349 UG/LITER 1113.375 .508 .0456552
B_2496 UG/LITER 1098.141 3.145 .2863749
Y_3710 PPM 1229.511 3.313 .2694428
lfl #2 It3
1110.204 1114.669 1119.189
1090.690 1097.428 1100.059
1085.236 1100.129 1103.794
1112.864 1113.379 1113.881
1094.635 1099.075 1100.713
1233.333 1227.467 1227.733
ERRORS VALUE RANGE
QC PASS QC PASS 1100.000 1100.000 10.4 0000 10.40000
QC PASS 1100.000 10.40000
QC PASS 1100.000 10.40000
QC PASS 1100.000 10.40000
NOCHECK
248
251 ANALYSIS REPORT
QC STANDARD
08/12/10 11:40:24 AM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICB RUN TIME: 08/12/10 11:33:27 COMMENT: ICB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.029168 .309436 1060.867
AL3082 UG/LITER 9.804045 7.535600 76.86216
BA4 934 UG/LITER -.395189 .019144 4.844337
BE3130 UG/LITER .0483972 .0396993 82.02803
CA3179 UG/LITER 4.806745 .071845 1.494668
CD2265 UG/LITER .1231802 .0358732 29.12251
C02286 UG/LITER .0736269 .1662072 225.7424
ffl #2 #3
.3046860 -.306353 -.085838
1.963460 10.45643 16.99224
-.396680 -.375343 -.413544
.0055033 .0558399 .0838485
4.866379 4.826873 4.726983
.1045092 .1645381 .1004935
.1803185 -.117876 .1584386
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .2987913 .4045823 135.4063
CU3247 UG/LITER -.069992 .085509 122.1690
FE2714 UG/LITER -1.95967 2.73629 139.6299
K_7664 UG/LITER 5.548237 2.422342 43.65966
MG2790 UG/LITER 8.481756 1.197583 14.11952
MN2576 UG/LITER -.184075 .038785 21.07021
NA3302 UG/LITER 94.86428 79.31129 83.60501
#1 #2 #3
.7653465 .0447410 .0862863
-.010498 -.031496 -.167983
-1.78946 .6875391 -4.77710
7.639724 6.110908 2.894078
7.544944 8.069258 9.831067
-.141588 -.193054 -.217582
179.5108 82.81490 22.26715
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.003911 .417327 10670.55
TL1908 UG/LITER .0884280 1.194076 1350.337
V_2924 UG/LITER .0952089 .1866630 196.0564
ZN2138 UG/LITER .0031374 .0414586 1321.450
PB2203 UG/LITER .3691087 .1568483 42.49381
SE1960 UG/LITER -.118726 2.140333 1802.754
SB2068 UG/LITER 1.199359 .468991 39.10346
#1 #2 #3
-.466971 .3431339 .1121036
1.189379 -1.18090 .2568058
.3103587 -.001141 -.023591
.0281593 .0259710 -.044718
.4215276 .1927639 .4930344
-2.10326 -.402096 2.149177
.9680944 1.739067 .8909159
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.113430 1.224472 1079.498
22031 UG/LITER 4.325348 .139211 3.218496
22032 UG/LITER -1.61589 .30003 18.56764
20681 UG/LITER -1.47464 2.17281 147.3448
20682 UG/LITER 2.524511 .618549 24.50174
19601 UG/LITER -1.18758 3.89182 327.7108
19602 UG/LITER .4050554 3.735581 922.2395
ftl ft2 #3
.7677686 .4035460 -1.51160
4.344924 4.453735 4.177385
-1.54705 -1.94436 -1.35626
-3.59400 .7479377 -1.57786
3.235896 2.224059 2.113578
1.456646 -5.65649 .6371096
-3.89037 2.211334 2.894199
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1.674047 2.048325 122.3577
BI2230 UG/LITER 1.154827 .657155 56.90505
MO2020 UG/LITER 1.530870 .872659 57.00410
TI3349 UG/LITER .4797632 1.500908 312.8435
B_2496 UG/LITER .9687914 .5986408 61.79254
Y_3710 PPM 1240.111 3.633 .2929883
#1 #2 #3
-.687287 2.971811 2.737517
.5989613 .9854199 1.880099
2.159653 1.898394 .5345643
2.113893 .1626385 -.837242
1.400002 1.221068 .2853037
1242.533 1241.867 1235.933
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
249
252
ANALYSIS REPORT
QC STANDARD
08/12/10 11:47:24 AM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CRI RUN TIME: 08/12/10 11:40:27 COMMENT: CRI MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 8.042521 .022881 .2844945
AL3082 UG/LITER -58.7288 1.7824 3.034971
BA4934 UG/LITER -.461658 .019383 4.198626
BE3130 UG/LITER 4.909658 .027233 .5546802
CA3179 UG/LITER -87.6368 175.5557 200.3220
CD2265 UG/LITER 5.127886 .192745 3.758763
C02286 UG/LITER 50.44278 .15145 .3002340
ftl
ft2 ff3
8.062241 8.017434 8.047890
-57.0173 -58.5947 -60.5745
-.444155 -.482490 -.458327
4.925347 4.925415 4.878212
13.70377 -290.351 13.73698
4.912952 5.285385 5.185320
50.40593 50.31315 50.60925
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS .OOOOOOO 400.0000
QC PASS .OOOOOOO 400.0000
QC PASS 5.000000 1.500000
QC PASS .OOOOOOO 2000.000
QC PASS 5.000000 1.500000
QC PASS 50.00000 15.00000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 9.953398 .340249 3.418424
CU3247 UG/LITER 25.25346 .20529 .8129128
FE2714 UG/LITER -10.0265 4.2476 42.36354
K_7664 UG/LITER 6.073466 1.276528 21.01811
MG2790 UG/LITER 6.300676 .698882 11.09218
MN2576 UG/LITER 14.46793 .03418 .2362369
NA3302 UG/LITER 91.85066 35.37702 38.51580
ttl #2 #3
9.703818 10.34097 9.815410
25.08198 25.48094 25.19747
-5.12183 -12.4754 -12.4823
4.818874 7.370853 6.030671
6.664329 6.742751 5.494947
14.43798 14.46065 14.50516
62.75199 131.2291 81.57089
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS 25.00000 7.500000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 2000.000
QC PASS 2000.000
QC PASS 15.00000 4.500000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 39.54594 .55943 1.414633
TL1908 UG/LITER 21.92710 2.79365 12.74063
V_2924 UG/LITER 49.87632 .20987 .4207729
ZN2138 UG/LITER 52.60809 .08566 .1628184
PB2203 UG/LITER 9.772267 1.101075 11.26734
SE1960 UG/LITER 35.52061 1.22484 3.448241
SB2068 UG/LITER 62.12410 .93018 1.497294
ttl tf2 ft3
38.99131 39.53648 40.11005
19.29993 24.86178 21.61958
49.92062 49.64784 50.06050
52.51725 52.68740 52.61962
9.282766 9.000820 11.03322
36.12206 34.11132 36.32845
61.14039 62.98941 62.24251
ERRORS VALUE RANGE
QC PASS 40.00000 12.00000
QC PASS 25.00000 12.50000
QC PASS 50.00000 15.00000
QC PASS 60.00000 18.00000
QC PASS 10.00000 5.000000
QC PASS 35.00000 10.50000
QC PASS 60.00000 30.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 9.092928 .829386 9.121224
22031 UG/LITER 13.08805 .71915 5.494707
22032 UG/LITER 8.102026 1.920224 23.70054
20681 UG/LITER 59.85881 .34480 .5760266
20682 UG/LITER 63.24516 1.27313 2.013001
19601 UG/LITER 35.79036 2.18752 6.112024
19602 UG/LITER 35.37604 1.11634 3.155653
#1 #2 #3
8.405740 8.858845 10.01420
12.76778 13.91170 12.58468
7.528049 6.534244 10.24379
59.69836 60.25460 59.62347
61.85043 64.34489 63.54016
35.39512 33.82742 38.14856
36.47510 34.24318 35.40984
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
10.00000 3.000000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 54.91233 1.15266 2.099084
BI2230 UG/LITER 51.07381 1.21886 2.386472
MO2020 UG/LITER 50.67345 .27345 .5396326
TI3349 UG/LITER 48.53454 1.08431 2.234091
B_2496 UG/LITER 49.21296 .17868 .3630670
Y_3710 PPM 1234.311 2.011 .1629646
ftl ft2 ft3
54.32433 56.24040 54.17225
49.86904 52.30629 51.04610
50.48342 50.55008 50.98685
49.16098 47.28249 49.16015
49.30230 49.32935 49.00723
1235.267 1235.667 1232.000
ERRORS VALUE RANGE
NOCHECK
QC PASS 50.00000 15.00000
NOCHECK
NOCHECK
QC PASS 50.00000 15.00000
NOCHECK
.OOOOOOO
250
253
ANALYSIS REPORT
QC STANDARD
08/12/10 11:54:24 AM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSA Rira TIME: 08/12/10 11:47:27 COMMENT: ICSA MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.125515 .326083 257.7418
AL3082 UG/LITER 252607.8 4335.3 1.716219
BA4934 UG/LITER 2.583555 .056872 2.201303
BE3130 UG/LITER .7931743 .0555949 7.009161
CA3179 UG/LITER 250878.2 4091.8 1.631004
CD2265 UG/LITER 3.092081 .217660 7.039276
C02286 UG/LITER 5.312391 .342303 6.443482
tfl #2 tf3
-.383972 -.235731 .2401569
257607.7 250322.8 249893.0
2.648873 2.556772 2.545019
.8541067 .7802072 .7452090
255279.4 250165.2 247189.2
3.201349 3.233460 2.841433
5.605882 4.936367 5.394925
ERRORS VALUE RANGE
QC PASS .OOOOOOO 10.00000
QC PASS 244100.0 48820.00
QC PASS 2.000000 400.0000
QC PASS .OOOOOOO 10.00000
QC PASS 234900.0 46980.00
QC PASS .OOOOOOO 10.00000
QC PASS 4.000000 10.00000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 45.97170 .88859 1.932902
CU3247 UG/LITER 23.52463 .09755 .4146742
FE2714 UG/LITER 101050.0 1719.8 1.701954
K_7664 UG/LITER 7.079486 .403458 5.698969
MG2790 UG/LITER 259911.1 4507.8 1.734372
MN2576 UG/LITER 18.53335 .28153 1.519023
NA3302 UG/LITER 1091.339 23.357 2.140241
ffl tf2 ff3
46.98913 45.34802 45.57795
23.59113 23.41265 23.57013
103031.2 100177.9 99940.95
7.545243 6.837601 6.855614
265111.8 257499.7 257122.0
18.85753 18.39213 18.35038
1114.889 1090.950 1068.179
ERRORS VALUE RANGE
QC PASS 43.00000 20.00000
QC PASS 23.00000 10.00000
QC PASS 95600.00 19120.00
QC PASS .OOOOOOO 2000.000
QC PASS 247500.0 49500.00
QC PASS 19.00000 20.00000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 22.56750 .39119 1.733444
TL1908 UG/LITER -1.37486 .76706 55.79163
V_2924 UG/LITER 1.332111 .400297 30.04981
ZN2138 UG/LITER 28.87677 .55848 1.934026
PB2203 UG/LITER 12.25690 1.53256 12.49342
SE1960 UG/LITER -2.05203 1.84821 90.06739
SB2068 UG/LITER 3.489270 1.280775 36.70610
ffl ff2 tf3
22.86013 22.71919 22.12317
-.491385 -1.87119 -1.76200
1.283592 1.754456 .9582848
29.48840 28.74796 28.39394
13.10915 13.19362 10.49793
-.259320 -1.94563 -3.95114
3.170437 4.899343 2.398029
ERRORS VALUE RANGE
QC PASS 21.00000 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS 1.000000 40.00000
QC PASS 28.00000 40.00000
QC PASS 10.00000 6.000000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .9244465 .9251022 100.1791
22031 UG/LITER -6.04577 1.75568 29.03987
22032 UG/LITER 21.39484 1.42166 6.644854
20681 UG/LITER 3.283182 1.518926 46.26384
20682 UG/LITER 3.581536 1.296931 36.21160
19601 UG/LITER -6.36954 4.11046 64.53309
19602 UG/LITER .0928644 2.050180 2207.715
Itl ff2 ff3
1.902712 .8093632 .0612645
-5.02931 -5.03493 -8.07305
22.14987 22.27969 19.75497
2.153923 5.010015 2.685608
3.667129 4.833551 2.243928
-1.77695 -9.70361 -7.62807
.4875565 1.917004 -2.12597
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 20.00000
ELEM UNITS AVGE SDEV %RSD
BI2230 SN1899 UG/LITER UG/LITER 4.03 83 27 5.871619 .294430 2.386029 7.290886 40.63665
MO2020 UG/LITER .5353412 .3871975 72.19239
TI3349 UG/LITER 3.797719 4.240018 111.6464
B_2496 UG/LITER -5.66353 .45193 7.979693
Y_3710 PPM 1155.156 16.310 1.411963
tfl #2 #3
3.713437 4.114035 4.287510
8.618064 4.687914 4.308879
.3121583 .3134275 .9034378
8.659638 .8675949 1.865026
-5.33661 -5.17925 -5.47472
1136.333 1164.000 1165.133
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 100.0000
NOCHECK
251
254 ANALYSIS REPORT
QC STANDARD
08/12/10 12:01:24 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSAB RUN TIME: 08/12/10 11:54:27 COMMENT: ICSAB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 201.9751 .1360 .0673402
AL3082 UG/LITER 248725.0 641.0 .2577162
BA4934 UG/LITER 510.4315 1.6534 .3258897
BE3130 UG/LITER 488.9033 1.1867 .2427243
CA3179 UG/LITER 245065.9 1273.8 .5197647
CD2265 UG/LITER 980.0499 4.0475 .4129869
C02286 UG/LITER 502.7907 1.3055 .2596490
#1 #2 ft3
201.8686 202.1283 201.9284
248141.7 248622.0 249411.2
509.1420 509.8434 512.3091
487.7077 488.9213 490.0809
244061.8 244637.3 246490.7
976.0175 980.0198 984.1123
501.3472 503.1351 503.8887
ERRORS VALUE RANGE
QC PASS 206.0000 41.20000
QC PASS 241100.0 48220.00
QC PASS 495.0000 400.0000
QC PASS 475.0000 95.00000
QC PASS 231100.0 46220.00
QC PASS 940.0000 188.0000
QC PASS 461.0000 92.20000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 534.0649 1.9655 .3680211
CU3247 UG/LITER 533.5948 .9921 .1859332
FE2714 UG/LITER 99334.80 401.36 .4040453
K_7664 UG/LITER 13.96437 1.38202 9.896775
MG2790 UG/LITER 255597.3 780.8 .3054869
MN2576 UG/LITER 515.1384 1.7488 .3394883
NA3302 UG/LITER 1116.175 77.817 6.971720
111 112 If3
531.9269 534.4747 535.7932
533.8293 532.5065 534.4487
98924.12 99354.14 99726.13
12.45092 14.28281 15.15937
254828.0 255574.7 256389.2
513.4376 515.0462 515.9316
1111.307 1196.311 1040.906
ERRORS VALUE RANGE
QC PASS 511.0000 102.2000
QC PASS 548.0000 109.6000
QC PASS 94800.00 18960.00
QC PASS .OOOOOOO 2000.000
QC PASS 251100.0 50220.00
QC PASS 502.0000 100.4000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1022.346 4.622 .4520879
TL1908 UG/LITER 103.9582 2.7191 2.615588
V_2924 UG/LITER 505.5235 1.6853 .3333865
ZN2138 UG/LITER 1020.264 2.683 .2630147
PB2203 UG/LITER 61.56329 2.71075 4.403186
SE1960 UG/LITER 45.32000 1.88609 4.161711
SB2068 UG/LITER 620.3223 5.6232 .9064902
ftl !t2 #3
1017.482 1022.876 1026.680
101.6418 103.2809 106.9519
504.1194 505.0587 507.3925
1017.821 1019.836 1023.136
58.45550 63.44027 62.79409
47.44939 43.85958 44.65102
613.8794 622.8462 624.2413
ERRORS VALUE RANGE
QC PASS 984.0000 196.8000
QC PASS 103.0000 20.60000
QC PASS 494.0000 98.80000
QC PASS 1028.000 205.6000
QC PASS 61.00000 12.20000
QC PASS 53.00000 10.60000
QC PASS 589.0000 117.8000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 101.8702 1.6823 1.651418
22031 UG/LITER 44.27322 2.32311 5.247202
22032 UG/LITER 70.18188 5.13836 7.321487
20681 UG/LITER 619.2186 • 14.1845 2.290716
20682 UG/LITER 620.8670 1.3702 .2206947
19601 UG/LITER 40.45060 6.68956 16.53760
19602 UG/LITER 47.74060 .56954 1.192992
lfl ft2 #3
101.8891 103.5430 100.1786
46.82154 43.72459 42.27354
64.25030 73.26985 73.02550
602,9108 626.0523 628.6928
619.3491 621.2393 622.0126
48.10965 35.75253 37.48962
47.10932 47.89658 48.21590
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
101.0000 20.20000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1001.480 4.160 .4153858
MO2020 BI2230 UG/LITER UG/LITER 1026.988 988.2441 8.6687 4 .945 .4815216 .8771861
TI3349 UG/LITER 1015.412 3.996 .3935778
B_2496 UG/LITER 1011.656 5.113 .5053732
Y_3710 PPM 1175.867 .401 .0408840
ttl tf2 #3
1004.807 1002.817 996.8160
1022.458 1026.243 1032.264
978.7266 990.3178 995.6879
1010.893 1016.865 1018.479
1006.448 1011.853 1016.668
1176.400 1175.467 1175.733
ERRORS VALUE RANGE
QC PASS 1000.000 200.0000
QC PASS 1000.000 200.0000
QC PASS 1000.000 200.0000
QC PASS 1000.000 200.0000
QC PASS 1000.000 200.0000
NOCHECK
252
255 ANALYSIS REPORT
QC STANDARD
08/12710 12:08
PAGE 1
0 OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCV RUN TIME: 08/12/10 12:01:28 COMMENT : CCV CVSl MODE: CONC CORR . FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 100.1573 .3563 .3557646
AL3082 UG/LITER 49448.61 52.76 .1066957
BA4 934 UG/LITER 1004.827 .966 .0960929
BE3130 UG/LITER 1007.807 .994 .0985941
CA3179 UG/LITER 49547.94 644.73 1.301225
CD2265 UG/LITER 992.9445 1.3391 .1348627
C02286 UG/LITER 1002.042 1.171 .1168127
Itl ft2 ff3
99.75493 100.2841 100.4329
49395.28 49449.77 49500.78
1003.912 1004.731 1005.836
1006.778 1007.883 1008.760
49620.97 48869.81 50153.05
992.6401 991.7839 994.4097
1000.766 1003.067 1002.292
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 999.1781 .7821 .0782724
CU3247 UG/LITER 999.8144 3.1618 .3162419
FE2714 UG/LITER 25073.17 1.41 .0056048
K_7664 UG/LITER 48115.87 15.20 .0315934
MG2790 UG/LITER 49286.18 17.98 .0364864
MN2576 UG/LITER 996.5670 .9061 .0909264
NA3302 UG/LITER 49964.34 148.04 .2962933
ftl tf2 ft3
998.8895 998.5814 1000.063
996.7803 999.5729 1003.090
25072.17 25072.56 25074.78
48111.26 48105.27 48134.08
49274.35 49277.31 49306.87
995.9144 996.1849 997.6016
49796.77 50018.85 50077.39
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1000.627 .751 .0751027
TL1908 UG/LITER 1002.894 2.501 .2493876
V_2924 UG/LITER 1016.274 .367 .0361005
ZN2138 UG/LITER 1081.089 .309 .0285447
PB2203 UG/LITER 997.3582 .8265 .0828724
SE1960 UG/LITER 1003.501 2.412 .2403631
SB2068 UG/LITER 1037.983 2.604 .2508432
ttl ft2 tf3
1001.468 1000.391 1000.022
1000.428 1005.429 1002.824
1015.095 1016.030 1016.696
1080.733 1081.282 1081.251
996.4111 997.7294 997.9340
1006.285 1002.186 1002.032
1040.784 1037.529 1035-637
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1015.033 1.423 .1401633
22031 UG/LITER 996.3310 .3103 .0311485
22032 UG/LITER 997.8594 1.0846 .1086899
20681 UG/LITER 1036.965 2.863 .2761090
20682 UG/LITER 1038.488 2.484 .2392092
19601 UG/LITER 997.0240 6.2870 .6305776
19602 UG/LITER 1005.724 1.322 .1313211
ftl ft2 tf3
1014.286 1016.673 1014.139
995.9784 996.4519 996.5627
996.6155 998.3557 998.6071
1040.144 1036.159 1034.590
1041.100 1038.209 1036.155
1003.711 996.1284 991.2328
1007.559 1005.200 1007.413
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1021.676 5.731 .5608946
BI2230 UG/LITER 1018.216 1.425 .1399571
MO2020 UG/LITER 1020.191 4.094 .4013316
TI3349 UG/LITER 1025.926 4.218 .4111191
B_2496 UG/LITER 1020.280 .546 .0534777
Y_3710 PPM 1199.522 1.633 .1361658
tfl ff2 tt3
1015.450 1027.810 1020.756
1016.667 1018.511 1019.471
1016.053 1020.280 1024.241
1021.959 1030.355 1025.464
1019.650 1020.584 1020.606
1198.000 1199.600 1201.267
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
253
256 ANALYSIS REPORT
QC STANDARD
08/12/10 12:15:26 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCB RUN TIME: 08/12/10 12:08:29 COMMENT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.196630 .249344 126.8089
AL3082 UG/LITER -56.9488 1.1716 1.750003
BA4934 UG/LITER -.498390 .024418 4.899464
BE3130 UG/LITER -.048730 .007749 15.90220
CA3179 UG/LITER 4.459580 .120766 2.708018
CD2265 UG/LITER .0534847 .0337149 63.03649
C02286 UG/LITER -.108122 .277211 256.3875
ttl If2 tt3
-.395165 -.277945 .0832208
-56.1700 -68.2962 -66.3802
-.525754 -.478820 -.490596
-.041533 -.047723 -.056933
4.363601 4.419961 4.595180
.0601056 .0833979 .0169505
-.280094 -.255941 .2116699
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.OOOOOO
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.014764 .150713 1020.846
CU324 7 UG/LITER -.167983 .116912 69.59739
FE2714 UG/LITER -10.4403 4.9828 47.72648
K_7664 UG/LITER 2.385253 3.387173 142.0048
MG2790 UG/LITER 5.204436 .458579 8.811317
MN2576 UG/LITER -.276673 .015768 5.699191
NA3302 UG/LITER 38.67661 61.19820 158.2305
#1 #2 #3
.0005944 -.172568 .1276828
-.188981 -.272972 -.041995
-13.3222 -13.3120 -4.68667
-.548459 6.092186 1.612032
5.697668 5.124664 4.790977
-.294879 -.267770 -.267370
-18.7992 31.81088 103.0182
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.329117 .557798 169.4831
TL1908 UG/LITER 1.921023 .641401 33.38851
V_2924 UG/LITER -.223206 .177297 79.43214
ZN2138 UG/LITER -.502591 .058930 11.72521
PB2203 UG/LITER -.816533 .437847 53.62265
SE1960 UG/LITER -.485513 1.138685 234.5322
SB2068 UG/LITER .8029194 .5285876 65.83321
ttl #2 #3
.1206489 -.953277 -.154724
1.412767 2.541683 1.708620
-.231395 -.396267 -.041955
-.439171 -.512945 -.555659
-.409244 -.760751 -1.27959
-1.79611 .0783424 .2612246
1.020194 1.188244 .2003199
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1.54782 .03386 2.187468
22031 UG/LITER 4.794492 2.374954 49.53507
22032 UG/LITER -3.52772 .72492 19.98284
20681 UG/LITER -2.03549 1.14174 56.09168
20682 UG/LITER 2.210064 .310962 14.07027
19601 UG/LITER -.378450 3.810545 1006.882
19602 UG/LITER -.548900 .359179 65.43623
tfl #2 #3
-1.54215 -1.58416 -1.51716
7.531102 3.579916 3.272457
-4.38318 -2.93779 -3.56217
-1.98362 -.920572 -3.20229
2.509960 2.231124 1.889107
-4.76181 2.144657 1.481808
-.325367 -.963213 -.358119
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 3.092603 1.958295 63.32188
BI2230 UG/LITER .6176498 .8897700 144.0574
MO2020 UG/LITER 1.622113 1.134145 69.91774
TI3349 UG/LITER -4.58041 1.94064 42.36823
B_2496 UG/LITER .2547452 .6245622 245.1714
Y_3710 PPM 1228.867 4.789 .3897390
#1 tf2 ft3
.9835863 4.853478 3.440745
.5413123 1.543129 -.231492
2.816363 1.490402 .5595744
-5.87320 -5.51914 -2.34890
.9376330 .1141147 -.287512
1234.200 1227.467 1224.933
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
254
257 ANALYSIS REPORT
08/12/10 12:25:25 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 1007154-12RE2 RUN TIME: 08/12/10 12:18:28 COMMENT: SDG:MY71L3 CLIENTID:MY71M4 1: 10 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.051781 .106374 205.4292
AL3082 UG/LITER 1709.775 130.340 7.623200
BA4934 UG/LITER 11.57834 .60008 5.182743
BE3130 UG/LITER .0059949 .0866949 1446.152
CA3179 UG/LITER 750.1403 28.8401 3.844534
CD2265 UG/LITER 1.269301 .117806 9.281176
C02286 UG/LITER 89.23248 4.30193 4.821035
#1 #2 #3
.0321458 -.016075 -.171415
1563.232 1753.340 1812.752
10.88586 11.90331 11.94583
-.090032 .0295108 .0785058
716.8716 768.0567 765.4928
1.225517 1.179656 1.402730
84.27326 91.95951 91.46467
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS LC PASS 400000.0 50000.00 -200.000' -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1345.687 57.942 5.048846
CU3247 UG/LITER 5.504947 .247535 4.498423
FE2714 UG/LITER 45255.75 2275.67 5.028474
K_7664 UG/LITER 13.68207 3.45594 25.25893
MG2790 UG/LITER 209458.7 10334.1 4.933703
MN2576 UG/LITER 674.9671 32.7692 4.854930
NA3302 UG/LITER 223.7959 16.7350 7.478233
ttl tt2 tt3
1257.299 1387.638 1382.122
5.270470 5.480449 5.763921
42529.03 46632.11 46506.09
16.04210 9.715260 15.28886
197532.0 215751.6 215092.5
637.1561 695.1233 692.6218
233.7911 233.1219 204.4747
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 2319.588 114.401 4.931967
TL1908 UG/LITER -1.42022 .15503 10.91613
V_2924 UG/LITER 15.34442 .65886 4.293826
ZN213 8 UG/LITER 31.44763 1.65373 5.258595
PB2203 UG/LITER 3.400558 .664542 19.54215
SE1960 UG/LITER -.853838 1.218114 142.5634
SB2060 UG/LITER .8253744 .8986135 108.7417
#1 #2 #3
2187.522 2388.186 2383.057
-1.24187 -1.52273 -1.49607
14.61436 15.89481 15.52410
29.53830 32.42873 32.37585
2.752283 4.080253 3.369138
.5509731 -1.61692 -1.49556
1.332887 1.357395 -.211159
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1.00862 .23250 23.05166
22031 UG/LITER 8.352562 .426327 5.104146
22032 UG/LITER .9128521 .7927749 86.84497
20681 UG/LITER -2.22053 .91381 41.15261
20682 UG/LITER 2.337662 1.350243 57.76039
19501 UG/LITER -1.56833 3.62305 231.0133
19602 UG/LITER -.507009 1.318567 260.0677
ffl #2 #3
-.798303 -1.25829 -.969262
8.022352 8.833857 8.201478
.1064467 1.691253 .9408864
-1.22803 -3.02703 -2.40653
2.601959 3.536214 .8748121
1.651731 -.865373 -5.49135
-.008049 -2.00224 .4892626
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 3.858268 3.628873 94.05444
BI2230 UG/LITER .5120058 1.097929 214.4368
MO2020 UG/LITER -.218014 .460100 211.0419
TI3349 UG/LITER -.817537 5.189157 534.7308
B_2496 UG/LITER 8.921568 .947596 10.62129
Y_3710 PPM 1236.622 45.010 3.539764
#1 #2 #3
1.732762 1.793660 8.048382
1.367503 -.726015 .8945290
.2356995 -.205495 -.684245
-6.80943 2.195782 2.161034
7.832423 9.375307 9.556274
1288.533 1208.467 1212.867
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
255
258 08/12/10 12:32:26 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0080327-PS2 RUN TIME: 08/12/10 12:26:29 COMMENT: SDG:MG68M3 CLIENTID:MG68M9A MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM IMITS AVGE SDEV %RSD
AG3280 UG/LITER .9282803 .4292935 46.24611
AL3082 UG/LITER 59273.75 160.90 .2714461
BA4934 UG/LITER 2287.795 8.800 .3845664
BE3130 UG/LITER 3.586715 .049752 1.387127
CA3179 UG/LITER 81268.64 543.43 .6686881
CD2265 UG/LITER 14.13303 .19951 1.411653
C02286 UG/LITER 64.63975 .19181 .2967408
ftl #2 #3
.4538253 1.041160 1.289855
59444.59 59251.56 59125.10
2297.568 2285.316 2280.499
3.642272 3.571603 3.546271
81736.12 81397.41 80672.38
14.34940 13.95635 14.09334
64.82858 64.64559 64.44508
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS LC PASS 4 000.000 400000.0 -5.00000 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 121.7672 .2420 .1987547
CU3247 UG/LITER 277.5641 .2245 .0808902
FE2714 UG/LITER 124355.3 312.6 .2513774
K_7664 UG/LITER 17038.10 53.62 .3147172
MG2790 UG/LITER 38793.53 96.54 .2488443
MN2576 UG/LITER 5021.014 11.090 .2208744
NA3302 UG/LITER 1782.278 67.524 3.794219
ftl ft2 #3
121.5862 122.0421 121.5734
277.4451 277.4241 277.8231
124676.8 124336.6 124052.4
17092.75 17035.96 15985.57
38897.51 38776.32 38706.75
5032.940 5019.091 5011.011
1706.511 1803.413 1836.809
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 160.6153 .0589 .0365465
TL1908 UG/LITER -7.87353 .42936 5.453233
V_2924 UG/LITER 183.4631 .4257 .2320205
ZN2138 UG/LITER 9951.912 27.528 .2766144
PB2203 UG/LITER 2685.053 5.061 .1884703
SE1960 UG/LITER 1.592324 1.118404 70.23722
SB2068 UG/LITER 6.266269 1.532483 24.45507
ffl #2 #3
160.5915 160.5722 160.6824
-7.42420 -7.91673 -8.27966
183.8577 183.5197 183.0120
9979.790 9951.198 9924.747
2680.170 2690.274 2684.714
.4635506 1.613360 2.700063
4.659268 6.428157 7.711381
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000,00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 85.52229 1.25507 1.479234
22031 UG/LITER 2697.888 5.895 .2185340
22032 UG/LITER 2678.633 8.815 .3290760
20681 UG/LITER 8.276811 .892635 10.78477
20682 UG/LITER 5.252920 1.919655 36.54453
19602 19601 UG/LITER UG/LITER -17.9311 11.32984 .7008 , 1.78513 3.908160 15.76483
#1 #2 ft3
86.95431 84.55645 85.05613
2702.967 2699.276 2691.423
2668.779 2685.768 2581.352
7.248804 8.855616 8.726012
3.356813 5.206662 7.195286
-18.1604 -17.1445 -18.4886
9.751925 10.96862 13.26897
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 34.78704 .88841 2.553846
BI2230 UG/LITER 7.717822 2.032901 26.34034
MO2020 UG/LITER 8.589295 .445276 5.184085
TI3349 UG/LITER 1687.677 2.357 .1396880
B_2496 UG/LITER 41.69092 .31681 .7699085
Y_3710 PPM 1275.511 5.834 .4573937
ftl ff2 #3
34.34969 35.80933 34.20208
5.529641 9.547835 8.075989
9.086399 8.227003 8.454483
1690.243 1687.180 1685.607
42.04249 41.42756 41.50271
1269.733 1275.400 1281.400
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
256
259 ANALYSIS REPORT
08/12/10 12:39:25 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 0080337-BS2 RUN TIME: 08/12/10 12:32:29 COMMENT: SDG:MC0022 CLIENTID:LCSS MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:2
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 2 4.5922 6 .28589 1.162509
AL3082 UG/LITER 438.6160 2.8045 .5393923
BA4934 UG/LITER 7.343291 .097566 1.328638
BE3130 UG/LITER 24.68960 .09454 .3829320
CA3179 UG/LITER 228852.5 1435.1 .6270784
CD2265 UG/LITER 56.38753 .16575 .2939392
C02286 UG/LITER 188.8442 1.1064 .5868933
til #2 #3
24.26260 24.77209 24.74210
435.7796 441.3873 438.6812
7.256915 7.449116 7.323841
24.58746 24.77404 24.70729
227205.2 229519.8 229832.4
56.24853 56.57096 56.34310
187.6294 189.7943 189.1089
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 139.3540 .5110 .4384857
CU3247 UG/LITER 8621.754 7.266 .0841558
FE2714 UG/LITER 30619.90 107.90 .3523764
K_7664 UG/LITER 67.80366 7.27767 10.73345
MG2790 UG/LITER 141602.0 448.8 .3169679
MN2576 UG/LITER 297.5652 1.0618 .3568429
NA3302 UG/LITER 656.4239 73.3242 11.17025
#1 tt2 #3
138.5910 139.4766 139.8945
8522.478 8614.163 8528.620
30505.69 30720.11 30633.90
62.79393 76.15160 64.46647
141112.8 141994.7 141698.7
296.4562 298.5726 297.6667
617.2013 741.0170 611.0635
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 78.87386 .4 524 2 .6736055
TL1908 UG/LITER 41.38948 2.34462 5.664784
V_2924 UG/LITER 89.31239 .44285 .4958491
ZN2138 UG/LITER 221.1057 1.1174 .5053867
PB2203 UG/LITER 294.0313 .7787 .2648333
SE1960 UG/LITER 47.41006 3.00763 6.343861
SB2068 UG/LITER 288.8522 .7186 .2487682
#1 #2 tf3
78.67915 78.55138 79.39104
40.18538 44.09150 39.89157
88.81869 89.67463 89.44385
219.8597 222.0190 221.4384
294.1381 294.7511 293.2047
46.26165 45.14583 50.82269
288.1191 289.5535 288.9141
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1192.757 2.859 .2397061
22031 UG/LITER 300.7833 3.2662 1.085884
22032 UG/LITER 290.6501 1.4757 .5077235
20681 UG/LITER 287.7633 2.1673 .7531631
20682 UG/LITER 289.4024 .5704 .1970853
19601 UG/LITER 39.82258 3.65534 9.179055
19602 UG/LITER 51.18784 4.41019 8.615595
ffl #2 tt3
1189.457 1194.487 1194.327
304.2755 300.2681 297.8054
289.0663 291.9864 290.8976
285.2675 288.8520 289.1705
289.5343 289.8952 288.7776
43.31589 36.02433 40.12752
47.72207 49.68946 56.15199
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI 8.9 9 UG/LITER 17.51632 1.47631 8.428174
BI2230 UG/LITER 103.6452 2.6784 2.584182
MO2020 UG/LITER 63.98875 .53409 .8346680
TI3349 UG/LITER 27.20015 4.06960 14.96167
B_2496 UG/LITER 5.605623 .354191 6.318491
Y_3710 PPM 1193.622 1.902 .1593804
#1 #2 #3
16.81173 18.35237 18.38485
104.1036 106.0665 100.7686
63.37273 64.27150 64.32203
22.50325 29.67485 29.42235
5.410845 5.391569 6.014456
1195.467 1191.657 1193.733
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
257
260 08/12/10 12:46:25 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 1008009-09RE1 RUN TIME: 08/12/10 12:39:29 COMMENT: SDG:MC0022 CLIENTID:MC0037 1:3 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 1.104342 .305641 27.67535
AL3082 UG/LITER 40610.31 42.59 .1048862
BA4934 UG/LITER 9341.934 8.117 .0868832
BE3130 UG/LITER 1.109778 .027075 2.439671
CA3179 UG/LITER 61499.70 153.80 .2500787
CD2265 UG/LITER 1.710939 .041640 2.433725
C02286 UG/LITER 8.438650 .206678 2.449186
#1 #2 #3
1.197794 .7528839 1.352347
40582.49 40659.34 40589.09
9332.564 9346.447 9346.790
1.126903 1.078564 1.123867
61630.77 61330.39 61537.93
1.702901 1.673904 1.756011
8.428255 8.237360 8.650325
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 22.86816 .30735 1.343998
CU3247 UG/LITER 99.36201 .44333 .4461718
FE2714 UG/LITER 6889.993 6.468 .0938727
K_7664 UG/LITER 9961.002 9.982 .1002125
MG2790 UG/LITER 1642.021 3.101 .1888532
MN2576 UG/LITER 246.5038 .0925 .0375306
NA3302 UG/LITER 19602.27 74.63 .3807170
ftl ft2 #3
22.82396 22.58530 23.19521
98.87905 99.45650 99.75047
6895.449 6882.849 6891.682
9950.980 9970.944 9961.082
1639.455 1641.141 1645.466
246.4747 246.6073 246.4293
19607.64 19674.07 19525.10
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 11.32368 .26040 2.299574
TLI908 UG/LITER 5.606933 1.545414 27.56255
V_2924 UG/LITER 68.25943 .27378 .4010822
ZN2138 PB2203 UG/LITER UG/LITER 305.7347 H252079.0 .2472 292.0 .0808640 .1158217
SE1960 UG/LITER 5.455429 .809995 14.84750
SB2068 UG/LITER 46.73589 .82437 1.763884
ffl It2 It3
11.29729 11.07749 11.59627
4.491858 4.957910 7.371021
68.38555 67.94521 68.44654
306.0169 H252405.9 305.5310 H251982.7 305.5553 H251847.3
5.147231 4.844771 6.374283
46.12683 47.67396 46.40589
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 50000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC HIGH 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 6.933414 2.024688 29.20188
22031 UG/LITER 250491.8 643.1 .2567309
22032 UG/LITER 252871.4 117.5 .0464686
20681 UG/LITER 67.00326 1.70693 2.547540
20682 UG/LITER 36.60734 .66908 1.827722
19601 UG/LITER -71.6345 1.7323 2.418242
19602 UG/LITER 43.93253 1.11693 2.542368
#1 ft2 «3
8.209615 4.598893 7.991735
251220.1 250253.2 250002.2
252999.5 252846.1 252768.5
65.14239 68.49628 67.37110
36.62320 37.26835 35.93047
-70.2678 -73.5827 -71.0529
42.78812 43.98968 45.01978
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER 4.638462 4.326836 93.28169
BI2230 UG/LITER 29.10824 .57043 1.959681
MO2020 UG/LITER 1.658905 .176205 10.62180
TI3349 UG/LITER 859.9233 1.8474 .2148331
B_2496 UG/LITER 11745.20 11.22 .0955269
Y_3710 PPM 1215.000 4.051 .3334457
#1 ft2 tt3
9.251032 .6694516 3.994902
28.45900 29.33663 29.52908
1.463618 1.707098 1.806000
859.9328 858.0711 861.7659
11732.77 11748.25 11754.58
1210.467 1216.267 1218.267
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
258
261 ANALYSIS REPORT
08/12/10 01:03:59 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 1008009-09RE2 RUN TIME: 08/12/10 12:57:03 COMMENT: SDG:MC0022 CLIENTID:MC0037 1:25 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.173513 .216747 124.9168
AL3082 UG/LITER 5230.498 32.858 .6281957
BA4934 UG/LITER 1195.355 3.381 .2828589
BE3130 UG/LITER .1290811 .0223846 17.34153
CA317 9 UG/LITER 7828.025 361.332 4.615880
CD2265 UG/LITER .3931336 .0807800 20.54772
C02286 UG/LITER 1.166238 .305609 26.20470
ftl ft2 #3
-.166102 .0394335 -.393871
5219.458 5267.455 5204.583
1195.581 1198.519 1191.868
.1363185 .1469516 .1039732
8049.560 7411.067 8023.448
.4863512 .3436496 .3494000
.9767022 1.518792 1.003218
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 2.814171 .245441 8.721623
CU3247 UG/LITER 12.87171 .43656 3.391612
FE2714 UG/LITER 887.8501 4.5175 .5088180
K_7664 UG/LITER 1036.706 5.935 .5724832
MG2790 UG/LITER 220.7886 4.0311 1.825788
MN2576 UG/LITER 31.64349 .11379 .3595956
NA3302 UG/LITER 2570.069 85.028 3.308411
#1 #2 ff3
2.616598 3.088927 2.736988
12.71422 13.36515 12.53574
884.5838 893.0055 885.9609
1034.800 1043.359 1031.957
219.3863 225.3335 217.6458
31.54285 31.76696 31.62066
2483.625 2653.608 2572.974
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1.777026 .560443 31.53824
TLI908 UG/LITER .8046823 1.937970 240.8365
V_2924 UG/LITER 8.895762 .098163 1.103483
ZN2138 UG/LITER 37.14350 .39610 1.066394
PB2203 UG/LITER 32202.77 88.27 .2740974
SE1960 UG/LITER 1.288341 2.238428 173.7450
SB2060 UG/LITER 6.625843 .298691 4.507973
ffl ff2 #3
1.249336 2.355299 1.716443
-1.17688 2.695902 .8950233
8.918801 8.788129 8.980357
37.21205 37.50085 36.71761
32151.87 32304.69 32151.76
1.252997 -.932206 3.544230
6.281033 6.791467 6.805029
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .8907894 .4950882 55.57860
22031 UG/LITER 32215.22 54.00 .1676240
22032 UG/LITER 32196.56 106.40 .3304566
20681 UG/LITER 8.421769 2.274571 27.00824
20682 UG/LITER 5.719308 .702648 12.28555
19601 UG/LITER -12.2186 2.3282 19.05452
19602 UG/LITER 8.021701 2.267807 28.27090
tfl tf2 tt3
1.393321 .8755507 .4034964
32171.02 32275.69 32198.14
32141.90 32319.16 32128.59
5.861436 9.194794 10.20908
6.480590 5.581673 5.095662
-13.0202 -14.0336 -9.59354
0.372975 5.698753 10.09337
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI 899 UG/LITER 2.674583 .618622 23.12968
BI2230 UG/LITER 4.071118 1.968243 48.34649
MO2020 UG/LITER -.233603 .455805 195.1193
TI3349 UG/LITER 107.4723 2.0383 1.896608
B_24 96 UG/LITER 1541.815 4.623 .2998667
Y_3710 PPM 1231.178 2.516 .2043580
tfl tf2 ff3
2.086830 2.616885 3.320032
5.175178 1.798691 5.239486
-.628068 -.464162 .2914203
106.6735 109.7890 105.9544
1540.723 1546.887 1537.835
1230.000 1229.467 1234.066
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
259
262 ANALYSIS REPCRT
08/12/10 01:10:59 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 1008009-12RE1 RUN TIME: 08/12/10 13:04:02 COMMENT: SDG:MC0022 CLIENTID:MC004 0 1:3 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .6950931 .1688814 22.85757
AL3082 UG/LITER 3820.177 5.724 .1498479
BA4934 UG/LITER 424.8774 .8655 .2035941
BE3130 UG/LITER .2582891 .0184080 7.126890
CA3179 UG/LITER 30930.27 435.60 1.408330
CD2265 UG/LITER 21.90366 .23403 1.058446
C02286 UG/LITER 2217.576 5.014 .2250951
#1 #2 #3
.7631559 .5135189 .8006045
3819.727 3814.690 3826.113
425.5276 423.8951 425.2095
.2592119 .2394371 .2762184
31426.42 30610.52 30753.77
21.71637 21.82860 22.16601
2216.299 2213.325 2223.105
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1352.138 2.395 .1771128
CU3247 UG/LITER 638.0139 .6825 .1069750
FE2714 UG/LITER 8588.421 20.331 .2367204
K_7664 UG/LITER 225.2281 9.0336 4.010847
MG2790 UG/LITER 1764.262 6.598 .3173243
MN2576 UG/LITER 658.2695 1.4285 .2170098
NA3302 UG/LITER 590.2190 54.3911 9.215417
#1 #2 #3
1351.889 1349.878 1364.548
637.7584 638,7872 637.4959
8585.507 8569.704 8610.051
232.6749 215.1790 227.8304
1765.021 1758.323 1769.443
657.8378 657.1066 659.8640
652.9092 555.5805 562.1572
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 30.20313 .33165 1.098051
TL1908 UG/LITER -3.93760 4.52664 114.9595
V_2924 ZN2138 UG/LITER UG/LITER 30.56851 H15139.32 .27322 53.05 .8937831 .3503967
PB2203 SE1960 UG/LITER UG/LITER 27817.52 L-7.71477 70.09 1.44717 .2619810 18.75842
SB2068 UG/LITER -3.80020 .62803 16.52612
#1 ff2 #3
30.57461 30.09794 29.93683
-1.91389 -9.12305 -.775846
30.34787 H15125.20 30.48379 H15094 .75 30.87418 H15197.99
27778.64 L-8.22100 27775.48 L-8.84082 27898.44 L-6.08249
-3.28628 -3.61406 -4.50025
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC HIGH 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC LOW 30000.00 -5.00000
LC PASS 40000.00 -50.0000
ELEM UNITS AVGE SDEV %RED
AS1890 UG/LITER 17.29035 .43609 2.522132
22031 UG/LITER 27810.82 66.42 .2388322
22032 UG/LITER 27820.85 78.07 .2806154
20681 UG/LITER 12.31923 .36841 2.990521
20682 UG/LITER -11.8578 .9451 7.970046
19601 UG/LITER -44.4163 3.0687 6.908918
19602 UG/LITER 10.59847 1.15588 10.90606
Itl #2 #3
16.90277 17.76254 17.20572
27812.28 27743.69 27876.50
27761.83 27791.34 27909.37
12.04370 12.73769 12.17630
-10.9498 -11.7876 -12.8360
-47.0618 -45.1350 -41.0520
11.16028 9.269077 11.36605
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 29462.66 76.63 .2600989
BI2230 UG/LITER 6.156139 1.562385 25.37929
NO2020 UG/LITER .2521414 .7263557 288.0747
TI3349 UG/LITER 61.22361 2.36555 3.863787
B_2496 UG/LITER 50.72751 .60673 1.130838
Y_3710 PPM 1221.089 3.472 .2843338
#1 #2 #3
29468.33 29383.35 29535.30
5.447237 7.947301 5.073878
.0879476 -.378063 1.046539
61..06031 58.94394 63.66657
61.51598 60.26024 60.40631
1218.667 1225.066 1219.533
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
260
263 ANALYSIS REPORT
08/12/10 01:17:59 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 1008009-12RE2 RUN TIME: 08/12/10 13:11:02 COMMENT: SDG:MC0022 CLIENTID:MC004 0 1:5 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .3631720 .1700843 46.83299
AL3082 UG/LITER 2277.338 18.920 .8308041
BA4934 UG/LITER 253.5065 1.6524 .5518215
BE3130 UG/LITER .2177066 .0428592 19.58667
CA3179 UG/LITER 18557.91 464.25 2.488234
CD2265 UG/LITER 13.21446 .09409 .7120154
C02286 UG/LITER 1334.343 6.885 .5160102
ttl #2 ft3
.4684009 .4541676 .1669476
2297.354 2274.914 2259.747
255.1855 253.4519 251.8820
.2639145 .2099496 .1792556
19190.06 18447.92 18335.76
13.11228 13.23360 13.29751
1340.847 1335.053 1327.131
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 812.5743 5.8072 .7146672
CU3247 UG/LITER 383.6804 .0802 .0208976
FE2714 UG/LITER 5182.474 28.976 .5591075
K_7664 UG/LITER 131.6891 1.3025 .9890860
MG2790 UG/LITER 1063.434 5.189 .5819684
MN2576 UG/LITER 395.1523 2.2907 .5797041
NA3302 UG/LITER 465.2951 91.3610 19.63506
ifl tf2 ft3
817.0301 814.6862 806.0067
383.6104 383.7679 383.6629
5207.711 5188.879 5150.832
131.0641 130.8168 133.1863
1059.390 1063.876 1057.036
397.4377 395.1631 392.8563
380.4593 453.4083 562.0175
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 18.14404 .62216 3.428988
TL1908 UG/LITER -1.05991 1.53270 144.6070
V_2924 UG/LITER 18.54783 .10795 .5819861
ZN2130 UG/LITER 8838.600 57.255 .6477820
PB2203 UG/LITER 16780.55 97.92 .5835356
SE1960 UG/LITER -4.89462 2.26188 46.21154
SB2060 UG/LITER -2.01240 .49688 24.69105
#1 #2 tf3
18.44948 18.55446 17.42820
.7016303 -1.79266 -2.08870
18.48646 18.67247 18.48455
8893.644 8842.792 8779.364
16855.44 L-6.33890 16816.46 L-6.05707 16669.74 -2.28790
-1.50041 -2.49266 -2.04415
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 10.95678 1.12986 10.31198
22031 UG/LITER 15764.19 93.52 .5578511
22032 UG/LITER 16788.71 100.48 .5984905
20681 UG/LITER 6.527532 .968118 14.83130
20682 UG/LITER -6.28587 .30593 4.866874
19601 UG/LITER -25.1219 5.9697 27.74357
19602 UG/LITER 5.193970 .882083 16.98282
#1 #2 #3
9.806074 12.06457 10.99968
15843.65 16787.78 16661.13
16861.32 16830.77 16674.03
7.622421 5.784729 6.175446
-6.06494 -6.63504 -6.15762
-27.7280 -30.4131 -17.2247
4.329644 6.092797 5.159468
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 17883.01 100.87 .5640436
BI2230 UG/LITER 5.829096 1.841796 31.59660
MO2020 UG/LITER -.245535 .215365 87.71233
TI3349 UG/LITER 38.04600 2.93900 7.724859
B_2496 UG/LITER 35.52909 .59510 1.674956
Y_3710 PPM 1233.911 6.775 .5490322
#1 #2 #3
17976.05 17897.17 17775.81
4.345572 7.890547 5.251168
-.156982 -.088564 -.491060
36.55961 41.43130 36.14709
36.05422 35.65036 34.88271
1227.333 1233.533 1240.867
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
261
264 08/12/10 01:24:69 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 1008009-15RE1 RUN TIME: 08/12/10 13:18:02 COMMENT: SDG:MC0022 CLIENTID:MC0043 1:3 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 4.311152 .164476 3.815135
AL3082 UG/LITER 53501.09 731.55 1.367351
BA4934 UG/LITER 13597.67 182.36 1.341139
BE3130 UG/LITER 1.679675 .030437 1.812058
CA3179 UG/LITER 88784.84 1369.79 1.542821
CD2265 UG/LITER 2.109331 .072422 3.433390
C02286 UG/LITER 2.247511 .345459 15.37073
#1 ft2 If3
4.323204 4.469271 4.140981
53138.90 53021.29 54343.08
13503.32 13481.81 13807.88
1.679342 1.649407 1.710277
87969.84 88018.41 90365.30
2.109347 2.036901 2.181744
2.645576 2.027440 2.069418
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 23.10522 .72846 3.152799
CU3247 UG/LITER 31.30785 .23780 .7595403
FE2714 UG/LITER 3756.117 44.248 1.178014
K_7654 UG/LITER 14512.93 173.71 1.196907
MG2790 UG/LITER 1152.863 14.209 1.232459
MN2576 UG/LITER 99.98196 1.13822 1.138429
NA3302 UG/LITER 26716.00 319.01 1.194097
#1 ft2 tt3
22.76499 22.60913 23.94165
31.27635 31.08737 31.55983
3732.720 3728.480 3807.151
14431.80 14394.63 14712.35
1146.223 1143.190 1169.175
99.45257 99.20486 101.2885
26591.87 26477.70 27078.42
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 7.801017 .195529 2.506457
TL1908 UG/LITER 6.898386 1.403051 20.33882
V_2924 UG/LITER 28.11345 ..51135 1.818876
PB2203 ZN2138 UG/LITER UG/LITER 279.0978 H341211.3 3.8143 2734.9 1.366636 .8015211
SE1960 UG/LITER 7.351719 2.891473 39.33057
SD2068 UG/LITER 28.69273 .01918 .0668467
tfl ft2 fi3
7.586709 7.969699 7.846641
5.469463 5.767270 8.468426
28.03371 27.64666 28.65999
277.2399 H340253.4 276.5685 H339084.2 283.4851 H344296.3
4.118680 9.690188 8.246289
28.68883 28.67580 28.71356
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS lOOOO.OO -20.0000
LC HIGH 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 12.07994 1.41190 11.68797
22031 UG/LITER 339395.1 2445.3 .7204921
22032 UG/LITER 342118.1 2887.6 .8440337
20681 UG/LITER 58.78739 3.35843 5.712836
20682 UG/LITER 13.65791 1.64856 12.07039
19601 UG/LITER -95.2072 3.8492 4.043016
19502 UG/LITER 58.54427 2.44249 4.172043
#1 ft2 ff3
13.02329 10.45673 12.75979
338282.3 337704.1 342198.9
341237.6 339773.3 345343.5
57.39166 56.35189 62.61862
14.34890 14.84853 11.77630
-99.3301 -91.7077 -94.5838
55.75551 60.30319 59.57411
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER L-21.4805 3.3047 15.38464
BI2230 UG/LITER 63.92387 1.02639 1.605647
MO2020 UG/LITER .4132838 .6499184 157.2572
TI3349 UG/LITER 1116.227 15.593 1.396944
B_2496 UG/LITER 18148.60 233.03 1.284016
Y_3710 PPM 1217.911 10.965 .9002819
ffl ft2 #3
-19.3056 -19.8525 L-25.2833
64.49069 64.54186 62.73907
-.126176 .2312045 1.134823
1110.501 1104.307 1133.874
18022.28 18006.00 18417.52
1219.600 1227.933 1206.200
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
ERRORS HIGH LOW
LC LOW 40000.00 -20.0000
262
265
ANALYSIS REPORT
08/12/10 01:31:59 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 1008009-15RE2 RUN TIME: 08/12/10 13:25:02 COMMENT: SDG:MC0022 CLIENTID:MC0043 1:5 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG32 80 UG/LITER 2.507725 .126286 5.035879
AL3082 UG/LITER 31689.57 195.03 .6154350
BA4 934 UG/LITER 8005.055 47.598 .5945287
BE3130 UG/LITER .9594444 .0161172 1.575617
CA3179 UG/LITER 52967.48 519.85 .9814539
CD2265 UG/LITER 1.139587 .110949 9.735860
C02286 UG/LITER 1.199117 .212238 17.69957
#1 ft2 #3
2.640700 2.493068 2.389407
31694.78 31491.99 31881.94
8007.665 7957.673 8052.829
.9619106 .9432458 .9731768
53515.34 52481.10 52906.99
1.266138 1.093582 1.059042
.9772661 1.219865 1.400219
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 13.59530 .32674 2.403317
CU3247 UG/LITER 14.12108 .13155 .9315906
FE2714 UG/LITER 2231.318 7.094 .3179441
K_7664 UG/LITER 8144.308 39.601 .4862443
MG2790 UG/LITER 688.5894 3.3172 .4815658
MN2576 UG/LITER 59.30950 .27953 .4713132
NA3302 UG/LITER 15802.60 6.30 .0398855
#1 tt2 #3
13.47841 13.34308 13.96440
14.13158 14.24707 13.98459
2230.928 2224.427 2238.599
8158.266 8099.618 8175.041
691.1724 684.9221 689.9737
59.35183 59.01121 59.56545
15809.01 15796.41 15802.37
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 4.305190 .257298 5.976473
TL1908 UG/LITER 4.082047 4.703829 115.2321
V_2924 UG/LITER 16.65487 .25915 1.656027
PB2203 ZN2138 UG/LITER UG/LITER 164.0778 H202523.2 922.6 .8640 .5265838 .4555420
SE1960 UG/LITER 4.958709 3.022587 60.95612
SB2068 UG/LITER 17.21324 1.33144 7.734953
#1 #2 •tf3
4.143949 4.601921 4.169700
-.119972 3.202572 9.163540
16.90404 16.67379 16.38677
163.8929 H202396.0 163.3212 H201670.8 165.0193 H203502.8
1.574358 7.389572 5.912198
18.50100 15.84205 17.29666
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC HIGH 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 7.506610 1.735017 23.11318
22031 UG/LITER 202258.1 913.4 .4516137
22032 UG/LITER 202655.6 941.0 .4643542
20681 UG/LITER 34.52332 1.85447 5.371642
20682 UG/LITER 8.561219 1.204806 14.07283
19601 UG/LITER -56.1880 1.1492 2.045233
19602 UG/LITER 35.47627 4.23192 11.92887
tfl tf2 tf3
8.788435 8.199106 5.532290
202346.0 201303.8 203124.3
202420.9 201854.0 203591.7
36.63451 33.15754 33.77792
9.437865 7.187388 9.058404
-56.6526 -54.8793 -57.0321
30.63422 38.46741 37.32719
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -12.9317 .9956 7.699270
BI2230 UG/LITER 37.03475 .42936 1.159333
MO2020 UG/LITER -.009150 .577421 5310.720
TI3349 UG/LITER 562.0119 1.8063 .2728439
B_2496 UG/LITER 10879.35 59.63 .5481340
Y_3710 PPM 1227.755 5.269 .4291493
ftl tt2 ti3
-12.2007 -12.5287 -14.0657
36.98788 37.48562 36.63075
.6572281 -.323104 -.351574
562.3291 560.0680 563.6306
10874.44 10822.32 10941.29
1225.333 1233.800 1224.133
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
263
266 08/12/10 01:42:05 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: IBL RUN TIME: 08/12/10 13:35:08 COMMENT: SDG: CLIENTID: MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.184498 .209239 113.4098
AL3082 UG/LITER -44.0974 22.1692 50.27325
BA4934 UG/LITER .8052523 1.405068 174.4879
BE3130 UG/LITER -.001512 .009709 642.2541
CA3179 UG/LITER 116.8737 194.7497 166.6325
CD2265 UG/LITER .0830663 .1133278 136.4305
C02286 UG/LITER -.027217 .190243 698.9965
#1
#2 #3
-.394574 .0238942 -.182815
-59.3425 -18.5658 -54.2839
-.411298 2.343161 .4838932
.0080682 -.001259 -.011344
4.635915 341.7511 4.233089
-.002958 .2114779 .0406792
.1675688 -.212449 -.036869
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .0406845 .0737050 181.1616
CU3247 UG/LITER .0384958 .1529872 397.4028
FE2714 UG/LITER -2.93904 2.56671 87.33161
K_7664 UG/LITER 4.769963 5.521138 115.7480
MG2790 UG/LITER 8.376113 3.403034 40.62785
MN2576 UG/LITER -.204954 .031641 15.43805
NA3302 UG/LITER 78.28971 107.8636 137.7749
#1 #2 #3
.0824564 .0840054 -.044418
-.083991 .2099796 -.010498
-1.41170 -1.50307 -5.90235
9.774261 5.688446 -1.16282
6.946510 12.26074 5.921085
-.185281 -.188127 -.241452
159.5073 119.4569 -44.0951
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.539121 .415915 77.14683
TL1908 UG/LITER -1.18161 1.35523 114.6930
V_2924 UG/LITER -.273285 .286653 104.8913
ZN2138 UG/LITER .0317596 .2468202 777.1513
PB2203 UG/LITER 28.81004 32.78812 113.8080
SE1960 UG/LITER .5160652 1.294775 250.8937
SB2068 UG/LITER 1.680054 .180257 10.72922
#1 #2 #3
-.136622 -.513477 -.967264
.1548499 -2.55486 -1.14483
-.003476 -.242142 -.574238
-.107426 .3167375 -.114033
1.244913 65.06889 20.11631
1.457305 -.960534 1.051424
1.871774 1.654374 1.514015
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.739602 .529522 71.59556
22031 UG/LITER 29.11611 23.65454 81.24210
22032 UG/LITER 28.64717 38.10235 133.0056
20681 UG/LITER .6035604 1.534378 254.2211
20682 UG/LITER 2.207473 .499423 22.62419
19601 UG/LITER 3.188819 1.882068 59.02084
19602 UG/LITER -.828330 1.617314 195.2500
#1 #2 #3
-1.35088 -.446011 -.421911
4.414341 51.56176 31.37223
-.347521 71.80232 14.48672
2.131368 .5166171 -.937304
1.732075 2.162470 2.727874
2.550855 1.708654 5.306948
.9012534 -2.30313 -1.08311
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 3.679004 3.479508 94.57745
BI2230 UG/LITER -.157269 .216847 137.8833
MO2020 UG/LITER -.206246 .594939 288.4604
TI3349 UG/LITER -4.43003 2.35294 53.11340
B_2496 UG/LITER 12.66950 3.24504 25.51305
Y_3710 PPM 1218.600 8.141 .6580374
tfl #2 #3
7.687729 1.908247 1.441037
.0848769 -.333539 -.223143
-.887088 .0548376 .2135107
-2.88142 -3.27102 -7.13764
13.85308 15.15661 8.998799
1209.667 1220.533 1225.600
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
264
267 ANALYSIS REPORT
QC STANDARD
08/12/10 01:49:06 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCV RUN TIME: 08/12/10 13:42:09 COMMENT: CCV CVSl MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 100.3760 .8461 .8428954
AL3082 UG/LITER 49479.18 244.56 .4942643
BA4 934 UG/LITER 1013.204 5.173 .5105883
BE3130 UG/LITER 1001.810 8.108 .8093525
CA3179 UG/LITER 48664.01 272.46 .5598702
CD2265 UG/LITER 990.4900 6.2784 .6338662
C02286 UG/LITER 997.5090 6.2816 .5297323
#1 #2 #3
99.44177 100.5958 101.0905
49198.04 49642.75 49596.75
1007.451 1017.473 1014.687
992.4647 1006.974 1005.991
48382.33 48683.51 48926.19
983.2792 994.7444 993.4464
990.2768 1001.505 1000.646
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 994.5882 5.6735 .5703816
CU3247 UG/LITER 1014.173 3.104 .3060575
FE2714 UG/LITER 24937.37 147.47 .5913518
K_7664 UG/LITER 48314.71 134.36 .2780973
MG2790 UG/LITER 49051.46 291.59 .5944591
MN2576 UG/LITER 991.0584 6.0225 .6076879
NA3302 UG/LITER 49597.57 248.95 .5019390
#1 #2 #3
988.2211 998.8283 997.0151
1010.628 1016.403 1015.489
24768.19 25038.72 25005.19
48174.51 48442.35 48327.29
48719.20 49264.76 49170.44
984.1367 995.1012 993.9373
49318.89 49675.85 49797.98
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 997.3358 6.2567 .6273444
TL1908 UG/LITER 1000.367 11.430 1.142554
V_2924 UG/LITER 1012.640 6.118 .6041632
ZN2138 UG/LITER 1073.830 5.481 .5104289
PB2203 UG/LITER 989.1821 5.3634 .5422056
SE1960 UG/LITER 999.3820 3.6692 .3671442
SB2068 UG/LITER 1035.498 4.169 .4026534
#1 #2 #3
990.1255 1001.336 1000.546
987.1832 1006.427 1007.490
1005.676 1017.149 1015.095
1067.675 1078.185 1075.628
983.1949 993.5474 990.8040
995.2031 1002.076 1000.867
1031.396 1039.732 1035.367
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1013.770 5.360 .5287442
22031 UG/LITER 987.8854 6.8315 .6915427
22032 UG/LITER 989.8169 4.9828 .5034041
20681 UG/LITER 1029.990 5.894 .5722256
20682 UG/LITER 1038.244 4.026 .3877549
19601 UG/LITER 996.3460 5.2462 .5265394
19602 UG/LITER 1000.888 4.770 .4765531
#1 #2 ft3
1008.005 1018.604 1014.700
981.4282 995.0383 987.1895
984.0644 992.7904 992.5960
1023.185 1033.449 1033.336
1035.492 1042.865 1036.376
992.5013 994.2141 1002.322
996.5419 1005.991 1000.130
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER 1011.762 9.033 .8928457
BI2230 UG/LITER 1016.803 6.586 .6477612
MO2020 UG/LITER 1016.664 8.715 .8572629
TI3349 UG/LITER 1019.045 8.739 .8575911
B_2496 UG/LITER 1025.717 4.811 .4690529
y_3710 PPM 1215.644 3.822 .3143795
#1 ft2 #3
1002.256 1020.233 1012.798
1009.564 1022.443 1018.404
1006.685 1020.520 1022.786
1009.101 1025.501 1022.536
1020.380 1029.721 1027.050
1219.933 1212.600 1214.400
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
265
268 ANALYSIS REPORT
QC STANDARD
08/12/10 01:56:08 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCB RUN TIME: 08/12/10 13:49:10 COMMENT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.306539 .306397 99.95375
AL3 082 UG/LITER -63.1555 3.5621 5.640194
BA4934 UG/LITER -.430922 .018716 4.343336
BE313 0 UG/LITER -.004608 .022384 485.7841
CA3179 UG/LITER -96.0104 174.2352 181.4753
CD2265 UG/LITER .1550489 .0801407 51.58733
C02286 UG/LITER -.174318 .196211 112.5597
#1 tf2 #3
.0472580 -.483236 -.483640
-59.1683 -66.0237 -64.2745
-.410773 -.434225 -.447766
.0170663 -.027639 -.003250
4.820762 -297.200 4.347700
.2389242 .0792553 .1469674
-.190854 -.361737 .0296389
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.609955 .435433 71.38761
CU3247 UG/LITER -.178482 .144337 00.86919
FE2714 UG/LITER -5.34274 5.10172 95.48896
K_7664 UG/LITER 3.702044 4.803028 129.7399
MG2790 UG/LITER 5.805048 1.806903 31.12642
MN2576 UG/LITER -.277958 .039041 14.04571
NA3302 UG/LITER 62.99644 61.36230 97.40599
ftl ft2 tt3
-.430451 -.292970 -1.10644
-.335966 -.146985 -.052494
.2821830 -6.63935 -9.67104
9.247923 .9678526 .8903579
7.763372 4.202487 5.449287
-.267606 -.245137 -.321132
113.1511 -5.42503 81.26324
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 6000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.642971 .707768 110.0777
TL1908 UG/LITER 2.270395 1.707727 75.21717
V_2924 UG/LITER -.074630 .311661 417.6070
ZN2138 UG/LITER -.332295 .084087 25.30498
PB2203 UG/LITER .1566573 .1398221 89.25350
SE1960 UG/LITER .2733265 1.060393 387.9586
SB2068 UG/LITER .8991247 .5095113 56.66747
#1 It2 #3
-.043213 -.462066 -1.42363
1.255534 1.313628 4.242024
.2732799 -.168890 -.328280
-.396869 -.362803 -.237212
.0369294 .3103250 .1227174
-.339269 -.338515 1.497763
1.343212 .3428780 1.011285
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1.31254 .63266 48.20084
22031 UG/LITER 3.156987 1.256748 39.80845
22032 UG/LITER -1.35114 .50759 37.56750
20681 UG/LITER -.439263 1.868963 425.4767
20682 UG/LITER 1.557440 .519576 33.36088
19501 UG/LITER -.926095 3.578821 386.4421
19602 UG/LITER .8622601 1.839058 213.2834
#1 #2 #3
-1.20221 -.742309 -1.99311
1.710724 3.776887 3.983351
-.808672 -1.43016 -1.81458
.1258502 -2.52557 1.081928
1.941029 1.765150 .9661415
1.484088 -5.03829 .7759128
-1.25954 1.998047 1.848273
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.546094 .522993 20.64100
BI2230 UG/LITER -.025350 1.935111 7630.466
MO2020 UG/LITER 1.252845 .232676 18.57178
TI3349 UG/LITER -3.14856 3.73565 118.6464
B_2496 UG/LITER 2.681087 .540777 20.17007
Y_3710 PPM 1235.867 9.673 .7825810
#1 #2 #3
3.148897 2.276205 2.213180
2.179955 -1.43962 -.816418
1.457720 .9998829 1.300931
1.159563 -5.11511 -5.49012
3.288270 2.503736 2.251255
1226.000 1245.333 1236.267
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
266
269 08/12/10 02:04:26 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 1008009-15RE3 RUN TIME: 08/12/10 13:57:30 COMMENT: SDG:MC0022 CLIENTID:MC0043 1:25 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
• AL3082 AG3280 UG/LITER UG/LITER .3322672 6737.638 84.146 .0890722 26.80738 1.248889
BA4934 UG/LITER 1689.389 20.435 1.209517
BE3130 UG/LITER .1958568 .0197595 10.08876
CA3179 UG/LITER 11131.32 439.94 3.952289
CD2266 UG/LITER .2657585 .1598018 60.13045
C02286 UG/LITER .0865585 .0735794 85.00539
ffl #2 #3
.2314558 .4003263 .3650195
6797.994 6641.518 6773.403
1706.659 1666.454 1696.056
.2074771 .1730418 .2070516
10991.29 10778.44 11624.24
.1116691 .2548888 .4307177
.1268514 .1311909 .0016333
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 3.024028 .070559 2.333624
CU3247 UG/LITER 3.041196 .125256 4.118540
FE2714 UG/LITER 468.1750 6.7655 1.445069
K_7664 UG/LITER 1456.937 19.182 1.316595
MG2790 UG/LITER 152.7185 2.5752 1.686225
MN2576 UG/LITER 12.49150 .14129 1.131051
NA3302 UG/LITER 3356.609 122.737 3.656696
ffl tt2 #3
3.100181 2.960840 3.011064
2.897710 3.097189 3.128686
466.3446 452.5131 475.6674
1468.759 1434.804 1467.247
152.1323 150.4870 155.5363
12.58095 12.32862 12.56492
3385.354 3221.918 3462.255
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER .8144790 .1159938 14.24147
TL1908 UG/LITER -.653211 .351901 53.87244
V_2924 UG/LITER 3.456233 .308199 8.917205
ZN2138 UG/LITER 33.50412 .35381 1.056028
PB2203 UG/LITER 42844.81 474.50 1.107480
SE1960 UG/LITER .8648621 1.311302 151.6198
SB2068 UG/LITER 4.738793 .588544 12.41971
#1 tf2 #3
.9381259 .7972445 .7080668
-.345989 -1.03714 -.576507
3.326612 3.234014 3.808072
33.42899 33.19391 33.88947
43161.41 42299.25 43073.77
.9289382 2.142952 -.477303
4.965340 4.070640 5.180400
ERRORS HIGH . LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 2.119735 .676299 31.90486
22031 UG/LITER 42898.59 485.14 1.130907
22032 UG/LITER 42817.94 470.76 1.099439
20681 UG/LITER 7.772938 1.465630 18.85555
20682 UG/LITER 3.214082 1.421843 44.23792
19601 UG/LITER -15.2985 2.5276 16.52179
19602 UG/LITER 8.924511 2.141163 23.99194
#1 #2 #3
1.908185 1.574500 2.876521
43263.25 42347:98 43084.56
43110.56 42274.91 43068.37
8.798122 8.426458 6.094233
3.041840 1.886206 4.714199
-12.4063 -16.4054 -17.0838
7.576574 11.39344 7.803519
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER -.799623 1.986840 248.4720
BI2230 UG/LITER 7.041733 1.474498 20.93943
MO2020 UG/LITER -.218952 .508811 232.3846
TI3349 UG/LITER 139.3413 2.1740 1.560162
B_2496 UG/LITER 2327.010 27.183 1.168150
Y_3710 PPM 1231.933 13.240 1.074721
tfl tf2 tf3
1.089537 -2.87152 -.616889
5.339196 7.879904 7.906098
-.206158 .2833412 -.734039
139.4159 137.1310 141.4770
2348.838 2296.562 2335.630
1223.600 1247.200 1225.000
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
267
270 ANALYSIS REPORT
QC STANDARD
08/12/10 02:11:26 PM
PAGE 1
OPERATOR:
METHOD: ALT-P303 SAMPLE NAME: CRI RUN TIME: 08/12/10 14:04:30 COMMENT: CRI MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 7.985641 .141932 1.777346
AL3082 UG/LITER -59.7182 1.5675 2.624769
BA4934 UG/LITER -.419587 .033213 7.913736
BE3130 UG/LITER 4.870305 .043334 .8897677
CA3179 UG/LITER -88.8566 177.4809 199.7162
CD2265 UG/LITER 5.072174 .105393 2.077872
C02286 UG/LITER 50.45720 .58646 1.160317
ftl #2 #3
7.950846 8.141735 7.864341
-50.1685 -51.0112 -57.9749
-.381348 -.438032 -.439682
4.861419 4.832102 4.917393
13.56355 13.64059 -293.804
5.122777 4.951023 5.142723
50.12307 50.11531 51.13322
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS .OOOOOOO 400.0000
QC PASS .OOOOOOO 400.0000
QC PASS 5.000000 1.500000
QC PASS .OOOOOOO 2000.000
QC PASS 5.000000 1.500000
QC PASS 50.00000 15.00000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 9.474720 .391922 4.136507
CU3247 UG/LITER 25.07848 .21267 .8480271
FE2714 UG/LITER -5.45927 4.46626 81.81063
K_7664 UG/LITER 3.125611 4.694130 150.1828
MG2790 UG/LITER 5.190321 1.255056 24.18070
MN2 57 6 UG/LITER 14.43214 .10063 .6972700
NA3302 UG/LITER 96.43726 89.59667 92.90670
ffl #2 #3
9.022737 9.681061 9.720364
24.84050 25.24996 25.14497
-3.17023 -2.60157 -10.5060
7.829620 -1.55858 3.105791
6.634438 4.363102 4.573421
14.38248 14.36599 14.54795
188.6839 9.749346 90.87856
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS 25.00000 7.500000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 2000.000
QC PASS .OOOOOOO 2000.000
QC PASS 15.00000 4.500000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 39.73208 .50143 1.262020
TL1908 UG/LITER 24.48847 1.38547 5.657657
V_2924 UG/LITER 49.67430 .42717 .8599454
ZN2138 UG/LITER 52.52344 .35428 .6745180
PB2203 UG/LITER 10.61889 .32819 3.090517
SE1960 UG/LITER 34.67245 1.86461 5.377789
SB2068 UG/LITER 62.69801 1.60159 2.554453
#1 #2 #3
40.12560 39.15751 39.90313
25.76584 24.68392 23.01565
49.48357 49.37573 50.16361
52.28191 52.35827 52.93015
10.49497 10.37070 10.99100
33.01585 36.69177 34.30973
64.02961 60.92080 63.14362
ERRORS VALUE RANGE
QC PASS 40.00000 12.00000
QC PASS 25.00000 12.50000
QC PASS 50.00000 15.00000
QC PASS 60.00000 18.00000
QC PASS 10.00000 5.000000
QC PASS 35.00000 10.50000
QC PASS 60.00000 30.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 9.460836 1.080977 11.42580
22031 UG/LITER 14 .77578 1.07563 7.286435
22032 UG/LITER 8.528652 .828882 9.718787
20681 UG/LITER 60.98519 1.85782 3.046353
20682 UG/LITER 63.54319 1.59942 2.517053
19601 UG/LITER 32.32181 2.44006 7.549276
19602 UG/LITER 35.83607 1.57797 4.403289
#1 #2 #3
10.15831 10.00857 8.215630
13.77327 15.91371 14.64035
8.843380 7.588501 9.154074
61.78928 58.86077 62.30553
65.13817 61.93937 53.55204
30.11118 34.93998 31.91426
34.45608 37.55645 35.49558
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
10.00000 3.000000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 54.63136 .52618 .9631435
BI2230 UG/LITER 50.90025 1.53256 3.010915
MO2020 UG/LITER 50.19992 .37929 .7665502
TI3349 UG/LITER 47.28729 .83903 1.776022
B_2495 UG/LITER 51.81078 1.04323 2.013538
Y_3710 PPM 1228.089 5.376 .4377367
ffl ft2 #3
55.22762 54.43434 54.23212
51.36533 49.18901 52.14539
49.97659 50.63785 49.90531
45.86458 48.25449 45.74279
52.81358 51.88740 50.73135
1229.333 1232.733 1222.200
ERRORS VALUE RANGE
NOCHECK
QC PASS 50.00000 15.00000
NOCHECK
NOCHECK
QC PASS 50.00000 15.00000
NOCHECK
268
271 ANALYSIS REPORT
QC STANDARD
08/12/10 02:18:26 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSA RUN TIME: 08/12/10 14:11:30 COMMENT: ICSA MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER .0151851 .2592933 1707.555
AL3082 UG/LITER 255608.6 8876.9 3.472858
BA4934 UG/LITER 2.683943 .128618 4.792137
BE3130 UG/LITER .8589730 .0910830 10.50371
CA3179 UG/LITER 254149.1 9681.7 3.809449
CD2265 UG/LITER 2.975630 .240021 8.066230
C02286 UG/LITER 5.478673 .094051 1.715674
#1 #2 ff3
.0717467 .2415287 -.267720
251781.4 255757.1 249287.2
2.612014 2.832435 2.607381
.8107958 .9640267 .8020967
248294.6 265324.3 248828.4
2.964572 3.220988 2.741328
5.382423 5.570359 5.483235
ERRORS VALUE RANGE
QC PASS .OOOOOOO 20.00000
QC PASS 243900.0 49997.06
QC PASS 2.000000 400.0000
QC PASS .OOOOOOO 10.00000
QC PASS 234100.0 47990.00
QC PASS .OOOOOOO 10.00000
QC PASS 3.000000 100.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 46.18484 2.11183 4.572552
CU3247 UG/LITER 23.64012 .31799 1.345122
FE2714 UG/LITER 102140.1 3774.2 3.595133
K_7664 UG/LITER 8.349497 .703802 8.429271
MG2790 UG/LITER 262944.8 9424.4 3.584171
MN2576 UG/LITER 18.62593 .77323 4.151345
NA3302 UG/LITER 1099.179 11.074 1.007441
#1 #2 #3
45.39535 48.57767 44.58150
23.78011 23.86410 23.27615
100453.6 106463.5 99503.23
7.944673 9.162175 7.941642
258715.6 273742.9 256375.7
18.32649 19.50409 18.04721
1089.763 1096.395 1111.379
ERRORS VALUE RANGE
QC PASS 36.00000 20.00000
QC PASS 15.00000 50.00000
QC PASS 94900.00 19454.00
QC PASS .OOOOOOO 2000.000
QC PASS 248800.0 51003.00
QC PASS 19.00000 30.00000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 21.74983 1.00731 4.631350
TL1908 UG/LITER -.001382 1.692704 122521.5
V_2924 UG/LITER 1.155233 .387003 33.47102
ZN2138 UG/LITER 29.10224 1.09851 3.774674
PB2203 UG/LITER 12.09639 1.28442 10.61818
SE1960 UG/LITER .0197644 3.314868 16771.89
SB2068 UG/LITER 2.801398 .790629 28.22265
ffl #2 ff3
21.18218 22.91286 21.15444
-1.95498 .9221916 1.028645
1.232492 1.499429 .7367770
28.67844 30.34953 28.27876
11.42805 13.57718 11.28395
-2.59007 3.749535 -1.10017
2.632487 2.108874 3.662831
ERRORS VALUE RANGE
QC PASS 10.00000 80.00000
QC PASS .OOOOOOO 50.00000
QC PASS 1.000000 100.0000
QC PASS 39.00000 120.0000
QC PASS 5.000000 20.00000
QC PASS .OOOOOOO 70.00000
QC PASS .OOOOOOO 120.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .5627206 2.656747 472.1255
22031 UG/LITER -6.73973 .53747 7.974713
22032 UG/LITER 21.48603 2.17954 10.14397
20581 UG/LITER 3.268242 1.474845 45.12655
20682 UG/LITER 2.557606 1.156575 45.22100
19601 UG/LITER -3.32586 3.56800 107.2806
19602 UG/LITER 1.679344 5.877724 350.0012
#1 #2 #3
-2.48599 2.382585 1 .791568
-6.67112 -7.30821 -6.23985
20.44944 23.99039 20.01825
1.590092 3.856265 4.358370
3.142301 1.225420 3.305097
-5.05731 -5.69775 .7774870
-1.36891 8.455018 -2.04807
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RAJJGE
.OOOOOOO 20.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 3.290781 2.940468 89.35472
BI2230 UG/LITER 5.387895 3.081109 48.23356
MO2020 UG/LITER .3945822 .3426370 86.83540
TI3349 UG/LITER 5.971766 6.724928 112.6120
B_2496 UG/LITER -3.56350 1.01605 28.51261
Y_3710 PPM 1145.267 31.940 2.788882
#1 tf2 #3
3.477683 6.133340 .2613201
8.370147 7.955332 2.830207
.5195162 .0070094 .6572208
.2589798 13.38312 4.273193
-4.41311 -2.43800 -3.83939
1156.933 1109.133 1169.733
ERRORS VALUE RANGE
NOCHECK
NOCHECK
NOCHECK
NOCHECK
QC PASS .OOOOOOO 200.0000
NOCHECK
269
272 ANALYSIS REPORT
QC STANDARD
08/12/10 02:25:27 PM
METHOD: ALT-P3Q3 SAMPLE NAME: ICSAB RUNTIME: 08/12/10 14:18:30 COMMENT: ICSAB MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 201.5704 .8448 .4191138
AL3082 UG/LITER 248969.0 297.7 .1195688
BA4934 UG/LITER 514.6888 .5832 .1133064
BE3130 UG/LITER 488.1935 1.0793 .2210867
CA3179 UG/LITER 245306.7 973.6 .3969071
CD2265 UG/LITER 981.3621 1.7391 .1772121
C02286 OG/LITER 501.8581 .3691 .0735371
#1 #2 #3
201.3510 202.5033 200.8570
248654.7 249005.7 249246.7
514.4177 514.2905 515.3582
489.4364 487.4919 487.6523
246326.7 244387.2 245206.2
983.1326 979.6562 981.2974
502.2380 501.5009 501.8354
ERRORS VALUE RANGE
QC PASS 210.0000 43.00000
QC PASS 248400.0 50922.00
QC PASS 475.0000 400.0000
QC PASS 482.0000 98.00001
QC PASS 234300.0 48031.00
QC PASS 916.0000 187.0000
QC PASS 455.0000 100.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 533.8860 1.0709 .2005882
CU3247 UG/LITER 534.1617 2.4328 .4554439
FE2714 UG/LITER 99329.39 83.24 .0837975
K_7664 UG/LITER 14.18943 3.36919 23.74439
HG2790 UG/LITER 255874.5 145.4 .0568296
MN2676 UG/LITER 514.6636 .8150 .1583504
NA3302 OG/LITER 1019.544 9.586 .9401997
#1 #2 #3
535.0843 533.5514 633.0225
531.3621 535.7611 535.3621
99364.19 99234.41 99389.59
18.06592 12.53597 11.96640
256007.1 255719.0 255897.5
515.4786 513.8487 614.5636
1030.324 1011.979 1016.330
ERRORS VALUE RANGE
QC PASS 506.0000 103.0000
QC PASS 537.0000 110.0000
QC PASS 95100.00 19495.00
QC PASS .OOOOOOO 2000.000
QC PASS 254100.0 52090.00
QC PASS
483.0000 99.00000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1025.389 .731 .0712918
TL1908 UG/LITER 100.1913 1.7595 1.756151
V_2924 UG/LITER 505.4129 .3961 .0783685
ZN213 8 UG/LITER 1019.648 1.293 .1268204
PB2203 UG/LITER 62.54863 .54103 .8649735
SE1960 UG/LITER 50.49160 1.94288 3.847919
SB2068 UG/LITER 619.5793 1.8203 .2938023
#1 #2 #3
1025.106 1024.842 1026.219
101.3335 98.16505 101.0753
505.8473 505.0717 505.3197
1021.126 1018.724 1019.094
63.10822 62.50935 62.02831
51.45286 51.76645 48.25547
621.3561 619.6635 617.7184
ERRORS VALUE RANGE
QC PASS 930.0000 190.0000
QC PASS 96.00000 50.00000
QC PASS 481.0000 99.99999
QC PASS 975.0000 199.0000
QC PASS 51.00000 20.00000
QC PASS 61.00000 70.00000
QC PASS 585.0000 120.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 100.8308 2.0860 2.068796
22031 UG/LITER 40.71307 1.48925 3.657922
22032 UG/LITER 73.43655 .58040 .7903404
20681 UG/LITER 617.8444 3.4135 .5524827
20682 UG/LITER 620.4392 1.0824 .1744616
19501 UG/LITER 43.47355 2.58873 5.954726
19602 UG/LITER 53.98491 1.54746 3.051705
#1 #2 ff3
102.0556 102.0146 98.42221
42.35603 39.45182 40.33138
73.45522 74.00739 72.84705
620.7940 618.6337 614.1054
621.6304 620.1713 619.5158
44.32674 45.52799 40.56591
55.00008 54.87059 52.08406
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
97.00000 20.00000
ELEM UNITS AVGE SDEV %R.SD
SN1899 UG/LITER 993.1072 2.4664 .2483474
BI2230 UG/LITER 1035.095 .955 .0922419
MO2020 UG/LITER 987.8198 3.1518 .3190700
TI3349 UG/LITER 1017.595 4.151 .4079061
B_24 96 UG/LITER 1015.336 2.259 .2224911
y_3710 PPM 1174.644 4.411 .3754983
itl f;2 ft3
993.0371 995.5080 990.6768
1034.599 1034.491 1036.196
984.1805 989.5180 989.6609
1016.811 1022.081 1013.891
1013.629 1014.482 1017.898
1169.667 1178.067 1176.200
ERRORS VALUE RANGE
QC PASS 1000.000 205.0000
QC PASS 1000.000 205.0000
QC PASS 1000.000 205.0000
QC PASS 1000.000 205.0000
QC PASS 1000.000 200.0000
NOCHECK
270
273 ANALYSIS REPORT
QC STANDARD
08/12/10 02:32:28 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCV RUN TIME: 08/12/10 14:26:31 COMMENT: CCV CVSl MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 100.0210 .3220 .3219580
AL3082 UG/LITER 49077.81 118.59 .2416318
BA4934 UG/LITER 1005.283 2.274 .2262277
BE3130 UG/LITER 994.1913 2.3155 .2329066
CA3179 UG/LITER 48472.79 383.34 .7908410
CD2265 UG/LITER 983.2340 2.1581 .2194866
CO2206 UG/LITER 990.6490 1.4983 .1612399
#1 #2 #3
99.65050 100.1787 100.2338
49013.23 49005.52 49214.67
1004.717 1003.345 1007.787
992.9472 992.7637 996.8629
48123.34 48412.21 48882.81
982.2214 981.7683 985.7121
989.9675 989.6126 992.3668
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 6200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 987.5866 1.8033 .1025967
CU3247 UG/LITER 1008.808 .927 .0919215
FE2714 UG/LITER 24789.28 45.82 .1848259
K_7664 UG/LITER 47994.49 73.05 .1522002
MG2790 UG/LITER 48738.72 96.57 .1981342
MN2576 UG/LITER 984.1916 2.1810 .2216063
NA3302 UG/LITER 49328.37 58.50 .1388713
tfl #2 #3
986.9524 986.1861 989.6213
1008.382 1008.172 1009.872
24806.08 24737.44 24824.33
47996.48 47920.46 48066.52
48687.92 48678.15 48850.08
983.3331 982.5706 986.6713
49277.55 49301.29 49406.27
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 991.0790 2.4987 .2521208
TL1908 UG/LITER 990.3719 7.4127 .7484781
V_2924 UG/LITER 1005.028 2.382 .2370055
ZN2138 UG/LITER 1065.866 2.964 .2780917
PB2203 UG/LITER 982.6628 2.1797 .2218174
SE1960 UG/LITER 993.3126 2.9292 .2948894
SB2068 UG/LITER 1027.075 2.208 .2150189
fil tf2 #3
989.4672 989.8124 993.9574
983.6182 989.1948 998.3028
1003^903 1003.418 1007.764
1064.045 1064.266 1069.286
980.4765 982.6759 984.8359
990.3752 996.2335 993.3292
1024.590 1027.824 1028.812
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1006.180 .977 .0971161
22031 UG/LITER 981.0820 2.2666 .2310352
22032 UG/LITER 983.4407 3.0715 .3123218
20681 UG/LITER 1021.977 4.175 .4085441
20682 UG/LITER 1029.617 1.390 .1349538
19601 UG/LITER 987.2449 7.1928 .7285735
19602 UG/LITER 996.3319 4.9641 .4982377
tfl #2 #3
1007.184 1005.232 1006.122
981.5246 978.6258 983.0948
979.9420 984.6862 985.6937
1017.158 1024.486 1024.288
1028.296 1029.487 1031.066
981.5227 984.8927 995.3193
994.7847 1001.885 992.3256
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1009.819 3.604 .3669300
BI2230 UG/LITER 1008.407 1.007 .0998858
MO2020 UG/LITER 1011.794 4.184 .4135160
TI3349 UG/LITER 1012.858 3.219 .3177940
B_24 96 UG/LITER 1014.988 1.638 .1613381
Y_3710 PPM 1217.689 1.891 .1552711
tfl #2 #3
1011.057 1005.759 1012.642
1007.265 1008.787 1009.169
1008.008 1011.089 1016.286
1009.926 1012.345 1016.302
1013.886 1014.208 1016.869
1218.467 1219.066 1215.533
ERRORS V/VLUS RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
271
274
ANALYSIS REPORT
QC STANDARD
08/12/10 02:39:30 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCB RUN TIME: 08/12/10 14:32:32 COMMENT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.335834 .175826 52.35500
AL3082 UG/LITER -50.4746 4.9643 9.835233
BA4 934 UG/LITER -.392797 .037271 9.488733
BE3130 UG/LITER .0910076 .0244888 26.90857
CA3179 UG/LITER 644.6694 1.2696 .1969288
CD2265 UG/LITER .0989150 .0546956 55.29561
C02286 UG/LITER .0273162 .2943382 1077.523
#1 #2 #3
-.490229 -.372812 -.144460
-54.6214 -44.9738 -51.8288
-.395915 -.428412 -.354065
.0736666 .1190216 .0803343
645.7468 643.2698 644.9916
.0958679 .1546102 .0452769
-.278523 .0518554 .3086165
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .1561655 .4694981 300.6413
CU3247 UG/LITER -.285971 .203130 70.78433
FE2714 UG/LITER -3.28449 6.16724 187.7587
K_7664 UG/LITER 8.242606 4.286750 52.00721
MG2790 UG/LITER 14.81808 5.56838 37.57830
MN2576 UG/LITER -.181772 .029421 16.18584
NA3302 UG/LITER 133.3567 58.9610 44.21302
ftl ft2 ft3
-.215188 .6838962 -.000211
-.409458 -.398959 -.052494
-8.99163 3.257813 -4.11975
7.562616 4.336493 12.82871
9.597012 20.67857 14.17866
-.215740 -.155295 -.164282
95.05067 103.7667 201.2528
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.678878 .563139 82.95143
TLI908 UG/LITER -.136038 2.561772 1883.127
V_2 924 UG/LITER -.029188 .084506 289.5235
ZN2138 UG/LITER -.303363 .096855 31.92696
PB2203 UG/LITER .1276961 1.001369 784.1811
SE1960 UG/LITER -.578795 .809033 139.7789
SB2068 UG/LITER 1.220605 .838272 68.67679
ffl tf2 ff3
-1.32347 -.282432 -.430728
-2.94294 2.075895 .4589322
-.027167 -.114686 .0542897
-.392498 -.200297 -.317294
1.223465 -.739888 -.100488
-.502841 .1895823 -1.42313
.9730725 2.154770 .5339726
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
OC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .2092062 .3123159 149.2862
22031 UG/LITER 3.292338 .849779 25.81082
22032 UG/LITER -1.46218 1.26793 86.71536
20681 UG/LITER -1.50548 .97832 64.98377
20682 UG/LITER 2.571685 .813381 31.62835
19601 UG/LITER -2.10130 1.85463 88.26077
19602 UG/LITER .1713094 1.166634 681.0097
ftl ft2 ft3
-.150921 .3727580 .4057814
4.133889 3.308563 2.434562
-.239510 -2.77098 -1.37604
-2.14409 -.379182 -1.99316
2.519381 3.409956 1.785718
-.100119 -2.44153 -3.76225
-.714093 1.493261 -.265240
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1.818580 .357473 19.65671
BI2230 UG/LITER .2959990 2.142877 721.5096
MO2020 UG/LITER 1.716023 1.349772 78.65701
TI3349 UG/LITER -2.43354 3.51289 144.3529
B_2496 UG/LITER .8581078 .0815012 9.497786
Y_3710 PPM 1230.044 2.443 .1985735
#1 #2 #3
2.207012 1.745305 1.503421
.4359208 -1.91196 2.367035
3.229548 1.281461 .6370580
-5.53001 -3.15451 1.383895
.9505993 .8269104 .7968138
1227.733 1232.600 1229.800
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
272
275 08/12/10 02:47:33 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0081015-BLKl RUN TIME: 08/12/10 14:40:36 COMMENT: SDG:MY71S3 CLIENTID:PBW 1:1 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
AG3280 UG/LITER -.350680 .097804 27.88973
AL3082 UG/LITER -33.4650 7.1065 21.23556
BA4934 UG/LITER -.328778 .068478 20.82794
BE3130 UG/LITER .1123409 .0269747 24.01147
CA3179 UG/LITER 213.1582 361.5011 169.5929
CD2255 UG/LITER .1688754 .2114570 125.2148
C02286 UG/LITER -.017257 .018293 106.0011
#2 #3
-.461581 -.276756 -.313703
-41.0276 -25.9256 -32.4417
-.405855 -.274960 -.305518
.0947147 .1433941 .0989139
4.369874 630.5837 4.521031
-.042154 .3807577 .1680223
-.008253 -.005203 -.038305
ERRORS HIGH LOW
LC PASS 5.000000 -5.00000
LC PASS 200.0000 -200.000
LC PASS 200.0000 -200.000
LC PASS 5.000000 -5.00000
LC PASS 5000.000 -5000.00
LC PASS 5.000000 -5.00000
LC PASS 50.00000 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.168142 .149881 89.14005
CU3247 UG/LITER 7.293267 1.047021 14.35599
FE2714 UG/LITER 4.583788 3.849125 83.97259
K_7664 UG/LITER 6.700023 1.630577 24.33689
MG2790 UG/LITER 25.06588 10.04487 40.07389
MN2576 UG/LITER -.132516 .049558 37.39766
NA3302 UG/LITER 216.5956 46.9054 21.65576
#1 #2 ft3
-.217239 -.287317 .0001309
6.152381 7.517245 8.210175
1.552982 8.914582 3.283801
8.075617 4.898858 7.125595
15.39523 35.44722 24.35518
-.188855 -.095662 -.113031
193.7709 185.4710 270.5449
ERRORS HIGH LOW
LC PASS 10.00000 -10.0000
LC PASS 25.00000 -25.0000
LC PASS 100.0000 -100.000
LC PASS 5000.000 -5000.00
LC PASS 5000.000 -5000.00
LC PASS 15.00000 -15.0000
LC PASS 5000.000 -5000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER .5751747 .3253943 56.47494
TL1908 UG/LITER .8447825 1.513146 179.1166
V_2924 UG/LITER -.083858 .213953 255.1386
ZN2138 UG/LITER 1.272707 .233214 18.32427
PB2203 UG/LITER 1.137229 .250863 22.05911
SE1960 UG/LITER .5849503 1.408834 240.8468
SB2068 UG/LITER 1.737839 1.223240 70.38856
#1 #2 #3
.3334836 .9459296 .4491108
2.515367 .4527408 -.433760
-.327627 .0727880 .0032661
1.040082 1.506506 1.271534
1.290900 1.273046 .8477411
2.205651 -.347099 -.103701
2.908867 1.836311 .4683393
ERRORS HIGH LOW
LC PASS 40.00000 -40.0000
LC PASS 10.00000 -10.0000
LC PASS 50.00000 -50.0000
LC PASS 60.00000 -60.0000
LC PASS 10.00000 -10.0000
LC PASS 35.00000 -35.0000
LC PASS 60.00000 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.862479 .684619 79.37810
22031 UG/LITER 4.426258 1.442500 32.58962
22032 UG/LITER -.514687 .368815 71.55807
20681 UG/LITER -.847416 1.060756 125.1753
20682 UG/LITER 3.018667 1.346198 44.59578
19601 UG/LITER -.257842 .286851 111.2509
19602 UG/LITER .9958470 2.151456 216.0428
ffl ff2 #3
-.973795 -1.48462 -.129023
5.638302 4.809689 2.830782
-.889527 -.502328 -.152207
-.118151 -.359797 -2.06430
4.410140 2.923016 1.722846
-.310484 .0516848 -.514726
3.451848 -.555896 .0915889
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
10.00000 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER 3.190677 1.790454 56.11519
BI2230 UG/LITER .4929293 .4017917 81.51102
MO2020 UG/LITER .6866925 .5366010 78.14283
TI3349 UG/LITER -5.40441 2.23821 41.41456
B_2496 UG/LITER .9282251 .0511905 5.514883
Y_3710 PPM 1236.978 18.073 1.451099
#1 #2 ff3
2.562605 5.210547 1.798878
.0327733 .6717344 .7742803
.2312915 1.278259 .5505275
-7.48875 -3.03890 -5.68557
.9871597 .9026954 .8948202
1222.600 1257.267 1231.066
ERRORS HIGH LOW
LC PASS 100.0000 -100.000
LC PASS 50.00000 -50.0000
LC PASS 10.00000 -10.0000
LC PASS 40.00000 -40.0000
LC PASS 10.00000 -10.0000
NOCHECK
ELEM UNITS AVGE SDEV %RSD ftl
273
276 08/12/10 02:54:33 PM
ANALYSIS REPORT
METHOD: ALT-P303 SAMPLE NAME: 0081015-BSl RUN TIME: 08/12/10 14:47:36 COMMENT: SDG:MY71S3 CLIENTID:LCSW MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 505.7887 1.3125 .2594901
AL3082 UG/LITER 2481.045 9.299 .3748107
BA4934 UG/LITER 511.1945 2.0301 .3971298
BE3130 UG/LITER 490.9546 1.7110 .3485061
CA3179 UG/LITER 9529.755 335.004 3.515352
CD2265 UG/LITER 496.3599 1.7170 .3459279
C02286 UG/LITER 505.8427 1.8091 .3576330
#1 ff2 ff3
504.5361 506.5752 507.1538
2491.068 2472.697 2479.371
513.5029 510.3939 509.5868
492.8977 490.2927 489.5734
9143.574 9742.244 9703.446
498.2567 495.9114 494.9116
507.8791 505.2276 504.4214
ERRORS HIGH LOW
LC PASS 594.0000 396.0000
LC PASS 2978.000 1985.000
LC PASS 602.0000 402.0000
LC PASS 591.0000 395.0000
LC PASS 12215.00 8144.000
LC PASS 592.0000 395.0000
LC PASS 595.0000 397.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 494.8761 1.9348 .3909663
CU3247 UG/LITER 511.3161 1.2205 .2387028
FE2714 UG/LITER 5018.076 15.967 .3181878
K_7664 UG/LITER 9005.614 37.934 .4212362
MG2790 UG/LITER 5855.855 19.778 .3377413
MN2576 UG/LITER 492.5353 1.8719 .3800641
NA3302 UG/LITER 10035.97 53.97 .5378041
ffl tf2 tt3
497.1086 493.8326 493.6871
510.4167 510.8261 512.7054
5036.481 5009.807 5007.940
9048.888 8989.125 8978.529
5877.697 5850.708 5839.159
494.6552 491.8413 491.1095
10087.28 10040.94 9979.677
ERRORS HIGH LOW
LC PASS 588.0000 392.0000
LC PASS 588.0000 392.0000
LC PASS 6128.000 4086.000
LC PASS 12009.00 8007.000
LC PASS 7203.000 4003.000
LC PASS 594.0000 396.0000
LC PASS 12045.00 8031.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 500.7257 3.0389 .5059003
TL1908 UG/LITER 1024.384 4.414 .4309085
V_2924 UG/LITER 504.6175 1.5863 .3143646
ZIW138 UG/LITER 977.3535 2.9176 .2985185
PB2203 UG/LITER 996.7139 3.7219 .3734125
SE1960 UG/LITER 986.2211 3.5884 .3638512
SB2058 UG/LITER 1009.771 6.599 .6535088
tfl tf2 tf3
504.0466 500.0469 498.0836
1027.437 1019.323 1026.393
506.4471 503.7795 503.6259
980.5964 976.5225 974.9415
999.3048 998.3878 992.4490
989.0836 987.3844 982.1954
1014.252 1012.868 1002.193
ERRORS HIGH LOW
LC PASS 590.0000 394.0000
LC PASS 1232.000 822.0000
LC PASS 601.0000 401.0000
LC PASS 1200.000 800.0000
LC PASS 1195.000 797.0000
LC PASS 1206.000 804.0000
LC PASS 1190.000 794.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1001.195 3.631 .3526771
22031 UG/LITER 1001.159 4.496 .4491213
22032 UG/LITER 994.4828 3.8653 .3886733
20681 UG/LITER 1008.143 4.525 .4488665
20682 UG/LITER 1010.581 7.753 .7671887
19601 UG/LITER 978.2769 5.1185 .5232235
19602 UG/LITER 989.9039 3.3143 .3348142
ffl tt2 tt3
1005.285 998.3507 999.9484
1006.010 1000.336 997.1303
995.9462 997.4027 990.0995
1012.286 1008.828 1003.314
1015.230 1014.881 1001.630
979.9651 982.3381 972.5275
993.3513 989.6195 986.7409
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
1195.000 797.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1.877258 2.352613 125.3218
BI2230 UG/LITER -.024152 1.698117 7030.888
MO2020 UG/LITER .0225591 .3517200 1559.103
B_2496 TI3349 UG/LITER UG/LITER -4.98514 L.0444983 2.39824 .3497496 48.10781 785.9834
Y_3710 PPM 1225.733 5.581 .4553442
ffl ff2 ff3
-.706251 2.441787 3.896246
1.208668 -1.96106 .6799358
-.319638 .3830849 .0042310
-2.96203 L.4435199 -7.63432 L-.101058 -4.35905 L-.208967
1219.933 1226.200 1231.065
ERRORS HIGH LOW
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
LC LOW 1200.000 800.0000
274
277 08/12/10 03:01:34 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-07RE1 RUN TIME: 08/12/10 14:54:37 COMMENT: SDG:MY71S3 CLIENTID:MY71T5 1:1 MODE: CONC CORR. FACTOR: 1
PAGS 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.454722 .256544 56.41773
AL3082 UG/LITER 23480.07 181.94 .7748573
BA4934 UG/LITER 40.54719 .30204 .7449071
BE3130 UG/LITER 1.475173 .040413 2.739553
CA3179 UG/LITER 115468.8 886.5 .7677255
CD2265 OG/LITER 1.743421 .074541 4.275553
C02286 UG/LITER 118.9213 .7702 .6476616
#1 #2 #3
-.741993 -.248457 -.373706
23390.78 23360.03 23689.40
40.40879 40.33915 40.89363
1.443359 1.461513 1.520646
115173.9 114767.3 116465.1
1.669277 1.742633 1.818353
118.4318 118.5230 119.8091
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 12.93345 .24585 1.900911
CU3247 UG/LITER 16.25587 .31590 1.943302
FE2714 UG/LITER 43469.04 344.84 .7932894
K_7664 MG2790 UG/LITER UG/LITER 11296.34 H304116.0 76.94 2373.8 .5810806 .7805607
MN2576 UG/LITER 2405.260 18.439 .7666099
NA3302 UG/LITER 121576.2 820.2 .6745978
#1
#2 #3
12.65137 13.10215 13.04684
15.92690 16.28386 15.55583
43235.03 43307.04 43865.04
11274.40 H302622.9 11232.76 H302871.8 11381.86 H306853.2
2393.274 2396.013 2426.492
121257.2 120963.4 122507.9
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC HIGH 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 339.4680 2.5170 .7414499
TL1908 UG/LITER -.996105 3.240886 325.3554
V_292 4 UG/LITER 2.378052 .186764 7.853645
ZN2138 UG/LITER 1150.525 8.533 .7416676
PB2203 UG/LITER 3.331777 .924754 27.76557
SE1960 UG/LITER 3.617969 1.998738 56.24475
SB2068 UG/LITER 2.869292 .217782 7.590103
#1 tt2 #3
336.9265 339.5178 341.9598
-3.57161 2.642908 -2.05962
2.169965 2.531142 2.433049
1144.455 1146.839 1160.282
2.321747 3.536711 4.136874
2.071247 2.907858 5.874803
3.055907 2.630004 2.921964
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 50000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.547925 .655448 119.6238
22031 UG/LITER 5.784345 1.481242 25.60777
22032 UG/LITER 2.092497 1.065482 50.91916
20681 UG/LITER 1.813479 1 .330020 73.34077
20682 UG/LITER 3.386742 .931600 27.50728
19601 UG/LITER -2.45794 2.28023 92.77018
19602 UG/LITER 6.641698 1.927870 29.02576
#1 #2 #3
.1503989 -1.14981 -.644360
5.153403 4.723041 7.476592
.8930778 2.929477 2.454936
1.664915 3.211544 .5639795
3.740719 2.330035 4.089471
-4.69255 -2.54661 -.134664
5.438432 5.621359 8.865304
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 6.681134 2.258335 33.80167
BI2230 UG/LITER 2.160090 1.253071 58.01014
MO2020 UG/LITER -.397419 .514488 129.4575
TI3349 UG/LITER 3.596224 3.216632 89.44469
B_2496 UG/LITER 3574.393 27.291 .7635251
Y_3710 PPM 1265.289 6.031 .4766601
ttl #2 #3
9.216328 4.884696 5.942380
3.483614 2.004590 .9919668
-.816372 .1768275 -.552712
.5144348 3.341667 6.932571
3558.506 3558.767 3605.906
1268.467 1269.066 1258.333
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
275
278 08/12/10 03:08:34 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0081015-DUPl RUN TIME: 08/12/10 15:01:37 COMMENT: SDG:MY71S3 CLIENTID:MY71T5D 1:1 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.194686 .310792 159.6378
AL3082 UG/LITER 23284.01 78.03 .3351283
BA4934 UG/LITER 40.14502 .15834 .3944210
BE3130 UG/LITER 1.474345 .018364 1.245537
CA3179 UG/LITER 114639.7 888.8 .7753034
CD2265 UG/LITER 1.889819 .052992 3.333245
C02286 UG/LITER 118.1342 .3300 .2793213
#1 «2 #3
-.160722 .0977296 -.521065
23370.14 23218.03 23263.07
40.32178 40.01615 40.09713
1.494622 1.469577 1.458836
1154 51.4 114777.9 113609.9
1.889062 1.953186 1.827209
118.5082 118.0101 117.0043
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 13.50936 .36288 2.686109
CU3247 UG/LITER 20.03898 .14934 .7452557
FE2714 UG/LITER 43234.07 70.63 .1633600
MG2790 K_7664 UG/LITER UG/LITER 11193.13 H302461.7 768.9 51.68 .4617447 .2542251
MN2576 UG/LITER 2387.341 4.946 .2071677
NA3302 UG/LITER 120309.5 397.0 .3299862
ttl tf2 #3
13.71404 13.72367 13.09039
19.96899 20.21047 19.93749
43314.62 43204.87 43182.73
11251.67 H303331.1 11153.82 H301871.0 11173.89 H302182.9
2393.051 2384.392 2384.581
120765.8 120119.3 120043.4
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC HIGH 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 336.4582 1.0581 .3144855
TL1908 UG/LITER -2.52345 1.38290 54.80173
V_2924 UG/LITER 2.477276 .263492 10.63635
ZN2138 UG/LITER 1141.055 2.801 .2465164
PB2203 UG/LITER 1.944009 .408603 21.01856
SE1960 UG/LITER 5.323790 2.204518 41.40880
SB2068 UG/LITER 2.362369 .152861 6.470645
#1 #2 ff3
337.0541 337.0841 335.2365
-3.99001 -1.24307 -2.33731
2.340110 2.781055 2.310664
1144.289 1139.400 1139.475
2.398036 1.605861 1.828130
6.230707 6.930191 2.810471
2.187844 2.426780 2.472483
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 50000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .5012739 1.260941 251.5474
22031 UG/LITER 4.269311 .811175 19.00015
22032 UG/LITER .7694213 .8150880 105.9352
20681 UG/LITER 1.173979 1.233907 105.1047
20682 UG/LITER 2.946014 .588740 19.98427
19601 UG/LITER 1.830640 4.132490 225.7401
19602 UG/LITER 7.058082 1.912864 27.10175
til tf2 tt3
1.563431 .8468019 -.895411
4.291635 5.069095 3.447204
1.440509 -.137611 1.005366
.9508609 .0668641 2.504221
2.795691 3.595342 2.447010
5.652574 2.393959 -2.55461
6.509623 9.185266 5.479357
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 7.341434 1.346693 18.34373
BI2230 UG/LITER .4245967 3.001473 706.8998
MO2020 UG/LITER -.282295 .253057 89.64262
TI3349 UG/LITER 4.885675 1.248896 25.56241
B_2496 UG/LITER 3661.313 8.815 .2482251
Y_3710 PPM 1266.022 6.445 .5090537
tfl tf2 ti3
8.792850 6.132378 7.099074
3.866580 -1.64768 -.945113
-.449324 -.405420 .0088579
3.904781 6.291614 4.460629
3560.404 3542.802 3550.732
1258.600 1269.267 1270.200
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
276
279 08/12/10 03:15:34 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0081015-MSl RUN TIME: 08/12/10 15:08:37 COMMENT: SDG:MY71S3 CLIENTID:MY71T5S MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 49.60770 .28208 .5686147
AL3082 UG/LITER 25202.89 53.26 .2113424
BA4934 UG/LITER 1944.402 4.402 .2263943
BE3130 UG/LITER 45.64048 .12364 .2650838
CA3179 UG/LITER 114597.3 310.3 .2708015
CD2265 UG/LITER 47.25454 .06597 .1396100
C02286 UG/LITER 582.9840 1.6333 .2801550
#1 #2 #3
49.30074 49.65683 49.85552
25249.51 25144.84 25214.32
1949.341 1940.894 1942.970
46.78038 45.59516 46.54589
114262.9 114876.0 114653.1
47.30380 47.28025 47.17959
584.5324 583.1422 581.2774
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.OOOOO
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 197.3255 .7806 .3955795
CU3247 UG/LITER 379.9113 10.9544 2.883413
FE2714 UG/LITER 44142.71 87.75 .1987840
K_7664 MG2790 UG/LITER UG/LITER 11202.20 H302586.9 761.0 23.39 .2088149 .2514980
MN2576 UG/LITER 2842.970 6.147 .2162303
NA3302 UG/LITER 120265.1 134.2 .1116098
#1 #2 #3
198.2212 196.9649 196.7904
367.3476 384.9228 387.4635
44241.31 44113.61 44073.21
11223.08 H303463.1 11176.92 H302090.7 11206.62 H302207.0
2850.068 2839.469 2839.373
120354.6 120110.8 120330.1
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC HIGH 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 804.5638 .2450 .0304466
TL1908 UG/LITER 45.46667 3.43963 7.566169
V_2924 UG/LITER 472.2047 .7962 .1685235
ZN2138 UG/LITER 1612.583 3.499 .2169995
PB2203 UG/LITER 20.57795 .79642 3.870274
SE1960 UG/LITER 52.57599 3.39275 6.453047
SB2063 UG/LITER 99.20914 1.93058 1.945965
#1 #2 #3
804.8187 804.5424 804.3302
48.59690 41.78441 46.01868
472.9327 472.3272 471.3543
1616.577 1611.118 1610.054
21.05304 21.02232 19.65849
48.77730 53.64572 55.30494
98.90022 101.2755 97.45164
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 39.23927 2.42633 6.183419
22031 UG/LITER 22.56817 1.24716 5.526170
22032 UG/LITER 19.57227 .70831 3.618931
20681 UG/LITER 97.62025 2.32631 2.383024
20682 UG/LITER 99.99274 2.88910 2.889309
19601 UG/LITER 47.94378 3.63107 7.573605
19602 UG/LITER 54.87891 3.27795 5.973069
ftl #2 ff3
37.03749 38.83975 41.84055
23.80516 22.58827 21.31109
19.55692 20.22850 18.82140
94.94019 99.11751 98.80304
100.8676 102.3433 96.76734
43.94041 48.86639 51.02455
51.18242 56.02219 57.43211
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 3.939689 1.488090 37.77177
BI2230 UG/LITER 3.356776 1.231706 36.69311
MO2020 UG/LITER .0681613 .0436832 64.08799
TI3349 UG/LITER 4.540979 8.811156 194.0365
B_2496 UG/LITER 3561.358 7.496 .2110844
Y_3710 PPM 1267.978 6.127 .4832039
#1 #2 #3
4.528221 5.043506 2.247340
1.934526 4.066496 4.069307
.0351744 .0516075 .1177020
-5.44597 7.851574 11.21734
3560.014 3547.120 3546.941
1260.933 1272.065 1270.933
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
277
280 08/12/10 03:22:34 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: SDI1007157-07 RUN TIME: 08/12/10 15:15:37 COMMENT: SDG:MY71S3 CLIENTID:MY71T5L 1:5 MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.436986 .191766 43.88385
AL3082 UG/LITER 4768.878 11.070 .2321405
BA4934 UG/LITER 8.036259 .046451 .5780160
BE3130 UG/LITER .4027659 .0043159 1.071678
CA3179 UG/LITER 24332.04 51.94 .2134721
CD2265 UG/LITER .4335811 .0637753 12.40260
C02286 UG/LITER 25.18261 .32770 1.301287
ftl #2 #3
-.341188 -.657776 -.311993
4773.476 4776.910 4756.250
8.078634 8.043547 7.986594
.4073144 .4022554 .3987279
24387.08 24325.15 24283.88
.4730284 .3723277 .4563873
25.14706 24.87413 26.52663
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 2.426203 .337837 13.92452
CU3247 UG/LITER 2.820717 .021856 .7748237
FE2714 UG/LITER 9187.912 11.869 .1291835
K_7664 UG/LITER 1901.321 6.544 .3441983
MG2790 UG/LITER 61911.87 104.75 .1591892
1^2576 UG/LITER 505.2552 .9873 .1954143
NA3302 UG/LITER 24892.58 70.83 .2845493
#1 #2 #3
2.090376 2.766015 2.422219
2.813717 2.803219 2.845215
9195.330 9194.184 9174.223
1908.438 1899.964 1895.562
61987.15 61956.21 61792.24
506.1628 505.3988 504.2039
24923.78 24942.46 24811.51
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 71.94 003 .39141 .5440753
TL1908 UG/LITER -2.34592 1.88478 80.34276
V_2924 UG/LITER .6735524 .0856479 12.71585
ZN2138 UG/LITER 229.4790 .4099 .1786258
PB2203 UG/LITER .3419353 .1793514 52.45186
SE1950 UG/LITER .1801895 2.805373 1556.902
SB2068 UG/LITER .5160472 1.098323 212.8338
#1 #2 #3
72.02441 71.51331 72.28236
-4.25441 -.485790 -2.29756
.7588433 .5875518 .6742620
229.5979 229.8164 229.0228
.4180054 .4707136 .1370860
-1.94054 -.880055 3.361165
-.657239 1.502897 .7124836
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -1.65175 1.06974 68.93760
22031 UG/LITER 4.153158 1.562048 37.37030
22032 UG/LITER -1.57195 .86855 55.25328
20581 UG/LITER .1895432 .4330798 228.4860
20682 UG/LITER .5691936 1.715647 256.5247
19601 UG/LITER 2.274117 3.819267 167.9451
19502 UG/LITER -.875066 2.326388 265.8528
#1 #2 #3
-1.65241 -2.56759 -.435237
2.389598 5.311061 4.758815
-.577430 -1.95703 -2.18139
.4865254 .3893767 -.307372
-1.25319 2.048964 1.211805
-.173856 .3212528 6.674953
-2.83245 -1.48967 1.696916
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.910855 2.344193 80.53278
BI2230 UG/LITER .2897491 2.195081 757.5801
MO2020 UG/LITER -.731368 .353057 48.27356
TI3349 UG/LITER -2.72851 1.07242 39.30413
B_2496 UG/LITER 746.7336 1.6149 .2162599
Y_3710 PPM 1238.755 2.614 .2110147
ftl #2 #3
2.597332 .7392013 5.396031
-1.15866 2.815332 -.787428
-.716804 -.385818 -1.09148
-2.19325 -3.96319 -2.02908
747.4739 747.8457 744.8813
1236.000 1239.066 1241.200
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
278
281 08/12/10 03:29:34 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 0081015-PSl RUN TIME: 08/12/10 16:22:37 COMMENT: SDG:MY71S3 CLIENTID:MY71T5A MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 17.73714 .62033 3.497365
AL3082 UG/LITER 23578.76 415.00 1.760042
BA4934 UG/LITER 40.69877 .71582 1.761277
BE3130 UG/LITER 10.93237 .23762 2.173583
CA3179 UG/LITER 115444.4 2823.4 2.445690
CD2265 UG/LITER 11.37025 .47740 4.198675
C02286 UG/LITER 215.9996 4.3000 1.990751
#1 #2 #3
17.41620 17.34302 18.45219
24054.00 23394.38 23287.90
41.51994 40.37810 40.19826
11.20637 10.80788 10.78286
118675.4 114205.5 113452.1
11.91068 11.19468 11.00550
220.9488 213.8702 213.1797
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 31.78793 .55573 1.748241
CU3247 UG/LITER 69.07605 .07880 .1140744
FE2714 UG/LITER 43586.56 785.84 1.802950
K_7664 MG2790 UG/LITER UG/LITER 11362.32 H305984.3 184.06 5416.0 1.619941 1.770017
MN2576 UG/LITER 2432.561 43.920 1.805489
NA3302 UG/LITER 121221.3 1786.4 1.473690
#1 #2 ft3
32.33696 31.80110 31.22573
69.16704 69.03056 69.03056
44490.88 43199.23 43069.55
11572.00 H312204.0 11287.60 H303440.3 11227.37 H302308.8
2482.914 2412.622 2402.149
123265.3 120439.8 119958.8
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC HIGH 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 416.1005 6.4743 1.655941
TL1908 UG/LITER 44.67376 3.07172 6.875896
V_2924 UG/LITER 100.8212 1.7275 1.713428
ZN2138 UG/LITER 1271.706 23.903 1.879595
PB2203 UG/LITER 21.54288 .14871 .6903124
SE1960 UG/LITER 73.62397 2.18504 2.967840
SB2068 UG/LITER 123.9506 2.6426 2.131979
#1 #2 #3
423.5622 412.7668 411.9724
47.87938 41.75624 44.38564
102.8017 100.0372 99.62477
1299..062 1251.204 1254.852
21.55217 21.38974 21.68673
75.11717 74.63867 71.11607
127.0015 122.3767 122.4737
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 2 0.77641 .20577 .9903804
22031 UG/LITER 24.84079 .72599 2.922555
22032 UG/LITER 19.88624 .44502 2.237804
20581 UG/LITER 121.8877 2.4135 1.980090
20682 UG/LITER 124.9708 2.9042 2.323923
19501 UG/LITER 67.42333 3.22495 4.783142
19602 UG/LITER 76.70966 1.95288 2.545801
#1 #2 #3
21.01334 20.67338 20.64251
25.66898 24.53904 24.31433
19.48568 19.80779 20.36527
124.4096 119.5997 121.6538
128.2856 123.7534 122.8735
68.11092 70.24902 63.91002
78.60486 76.82029 74.70381
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 5.767112 .854515 14.84277
BI2230 UG/LITER 2.789190 .266680 9.561210
MO2020 UG/LITER .2103201 .2649818 125.9897
TI3349 UG/LITER 2.604423 1.398369 53.69206
B_2496 UG/LITER 3594.831 67.766 1.606930
Y_3710 PPM 1255.555 19.959 1.589671
#1 #2 #3
6.566835 5.840570 4.863930
3.030412 2.502816 2.834342
-.087423 .2981427 .4202409
3.244453 1.000584 3.568233
3661.155 3567.820 3555.519
1232.667 1254.667 1269.333
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
279
282 08/12/10 04:07:26 PM
ANALYSIS REPORT METHOD: ALT-P3Q3 SAMPLE NAME: IBL RUN TIME: 08/12/10 16:00:29 COMMENT: SDG: CLIENTID: MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR: 1:1
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.313648 .384522 122.5966
AL3082 UG/LITER -32.9512 5.8959 17.89277
BA4934 UG/LITER -.373483 .120613 32.29422
BE3130 UG/LITER .2933390 .0971008 33.10192
CA3179 UG/LITER 118.2148 490.3002 414.7536
CD2265 UG/LITER .1929883 .1662152 85.12706
C02286 UG/LITER .0203598 .2739927 1346.752
itl
#2 #3
-.358057 -.674037 .0911502
-39.5548 -31.0829 -28.2158
-.501810 -.252451 -.356187
.1834657 .3675266 .3289247
-305.024 4.187626 655.4811
.0417613 .3709506 .1662531
-.075553 -.192705 .3294373
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2 577 UG/LITER -.422078 .378086 89.57719
CU3247 UG/LITER -.566943 .151629 28.50891
FE2714 UG/LITER -5.60918 6.29861 112.2910
K_7664 UG/LITER 6.179041 2.290718 37.07239
MG2790 UG/LITER 14.32475 5.38655 37.60314
MN2576 UG/LITER -.133896 .136883 102.2305
NA3302 UG/LITER -70.3020 54.5050 77.52978
#1 ft2 #3
-.740809 -.521085 -.004339
-.703429 -.608938 -.388450
-11.4370 -6.46361 1.073022
8.823298 4.914505 4.799320
8.126287 16.97757 17.87039
-.291945 -.056360 -.053383
-73.3431 -14.3401 -123.223
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.520543 .254645 48.91916
V_2924 TL1908 UG/LITER UG/LITER -1.04242 .0207870 3 .37519 .1465510 323.7849 705.0125
ZN2138 UG/LITER -.323196 .181424 55.13451
PB2203 UG/LITER -.080741 .574025 710.9477
SE1960 UG/LITER -1.48008 .77098 62.09052
SB2068 UG/LITER .9730697 .5787221 59.47386
#1 #2 #3
-.715080 -.614221 -.232327
-2.59035 -3.36601 2.829103
-.094801 -.028456 .1855173
-.510211 -.311442 -.147934
.4630918 -.680817 -.024497
-.934114 -2.36204 -1.14408
.5165852 1.623955 .7786587
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 50000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .2070143 .6225962 300.7504
22031 UG/LITER 3.282442 .502329 15.30351
22032 UG/LITER -1.76987 .92891 52.48483
20681 UG/LITER -.251671 1.235068 490.7481
20682 UG/LITER 1.574467 1.471691 93.47229
19601 UG/LITER .3982239 1.585166 398.0590
19602 UG/LITER -2.42788 .36751 15.13726
ftl ft2 #3
-.472909 .3447263 .7492250
3.545412 3.598695 2.703219
-1.08581 -2.82738 -1.39640
.9609449 -1.50803 -.207927
.2846848 3.177596 1.261121
1.590758 -1.40060 1.004516
-2.20471 -2.85205 -2.22586
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.117949 2.032793 95.97931
BI2230 UG/LITER .4797714 2.870343 598.2731
MO2020 UG/LITER -.104295 .466220 447.0222
TI3349 UG/LITER -4.68303 4.25996 90.96588
B_24 96 UG/LITER -.416898 .056287 13.50141
Y_3710 PPM 1214.511 4.267 .3513642
ttl tf2 tf3
4.455274 1.135176 .7623959
-.154233 -2.02057 3.614113
-.456507 -.280780 .4244033
-6.09544 -8.05741 .1037464
-.384080 -.481891 -.384721
1214.600 1218.733 1210.200
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
280
283 ANALYSIS REPORT
QC STANDARD
08/12/10 04:14:27 PM
METHOD: ALT-P3Q3 SAMPLE NAME: CCV RUN TIME: 08/12/10 16:07:30 COMMENT: CCV CVSl MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 97.75993 .18263 .1867121
AL3082 UG/LITER 48987.81 216.73 .4424230
BA4934 UG/LITER 997.3065 4.8808 .4893946
BE3130 UG/LITER 993.3170 5.6053 .5642973
CA3179 UG/LITER 48423.72 75.61 .1561414
CD2265 UG/LITER 985.6899 5.0360 .5109142
C02286 UG/LITER 989.3227 5.8473 .5910383
ftl If2 tf3
97.62142 97.69160 97.96677
49074.01 48741.24 49148.19
1000.727 991.7172 999.4750
994.7875 987.1231 998.0405
48467.99 48336.41 48466.75
987.4320 980.0142 989.6237
990.5253 982.9677 994.4752
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 989.0518 5.7257 .5789111
CU3247 UG/LITER 975.3309 1.0913 .1118899
FE2714 UG/LITER 24774.83 146.76 .5923605
K_7664 UG/LITER 47562.20 171.82 .3604926
MG2790 UG/LITER 48986.91 267.97 .5470166
MN2576 UG/LITER 983.5684 5.2065 .5293441
NA3302 UG/LITER 48881.26 182.23 .3728059
#1 #2 #3
988.9879 983.3583 994.8092
974.7220 976.5908 974.6800
24812.08 24613.04 24899.38
47791.68 47467.28 47727.64
49086.81 48683.35 49190.59
985.2493 977.7291 987.7268
48973.77 48571.31 48998.66
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 994.4406 5.3205 .5350213
TL1908 UG/LITER 995.3224 5.9075 .5935283
V_2924 UG/LITER 1005.441 5.120 .5091821
PB2203 ZN2138 UG/LITER UG/LITER 1070.991 985.7898 4.6419 6.228 .5814777 , .4704071
SE1960 UG/LITER 988.1326 6.0404 .6112994
SB2068 UG/LITER 1025.543 3.009 .2934248
ttl #2 tt3
994.7629 988.9662 999.5925
993.8804 990.2694 1001.817
1006.875 999.7570 1009.690
1072.828 1054.052 1076.093
988.2611 981.5905 990.5178
987.1719 982.6300 994.5958
1025.693 1022.461 1028.474
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1005.187 5.652 .6622424
22031 UG/LITER 982.4811 5.1603 .6270141
22032 UG/LITER 988.9306 4.0906 .4136403
20681 UG/LITER 1017.156 4.749 .4668957
20682 UG/LITER 1029.725 2.181 .2117781
19601 UG/LITER 985.0503 5.0011 .5077010
19602 UG/LITER 989.6610 6.7252 .6795434
#1 tf2 #3
1008.666 998.6657 1008.228
986.2387 975.3716 985.8329
989.2605 984.6851 992.8463
1016.695 1012.655 1022.119
1030.181 1027.353 1031.542
986.0572 979.6224 989.4714
987.7180 984.1213 997.1438
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 1009.078 10.156 1.006475
BI2230 UG/HTER 1008.969 4.676 .4534584
MO2020 UG/LITER 1008.193 6.842 .6786724
TI3349 UG/LITER 1011.944 9.127 .9019039
B_2496 UG/LITER 1014.737 5.741 .6643446
Y_3710 PPM 1189.044 6.312 .5308778
#1 #2 tf3
1010.766 998.1832 1018.284
1010.745 1003.565 1012.497
1006.702 1002.220 1015.569
1012.158 1002.712 1020.952
1016.869 1007.188 1020.155
1185.400 1196.333 1185.400
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
281
284 ANALYSIS REPORT
QC STANDARD
08/12/10 04:21:29 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCB RUNTIME: 08/12/10 16:14:31 COMMENT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.093106 .125594 134.8931
AL3082 UG/LITER -35.5883 2.8216 7.928356
BA4 934 UG/LITER -.441367 .013785 3.123336
BE3130 UG/LITER .2108956 .0146490 6.946105
CA3179 UG/LITER 4.713254 .079167 1.679558
CD2265 UG/LITER .1773810 .1345610 75.85425
C02286 UG/LITER .0399470 .0340960 85.35325
ftl ft2 S3
.0096165 -.065812 -.233124
-34.6345 -38.7631 -33.3672
-.446512 -.425749 -.451840
.2043312 .2006768 .2276787
4.797303 4.702362 4.640098
.0639142 .1422018 .3260271
.0315062 .0774705 .0108541
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS
.OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 6.000000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER -.104505 .164192 157.1143
CU3247 UG/LITER -.724426 .209716 20.94926
PE2714 UG/LITER -1.03058 4.05221 393.1967
K_7664 UG/LITER 3.087848 4.414772 142.9724
MG2790 UG/LITER 11.35093 .42339 3.730016
MN2576 UG/LITER -.221846 .014833 5.686333
NA3302 UG/LITER 28.51215 75.28322 264.0391
til tl2 tl3
-.223224 -.173161 .0828713
-.587940 -.619437 -.965902
3.547847 -3.43780 -3.30179
6.152496 5.083436 -1.97239
11.25261 11.81483 10.98535
-.211504 -.215191 -.238841
88.43875 53.08475 -55.9871
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.148814 .447342 300.5056
TL1900 UG/LITER 1.465169 1.081092 73.78514
V_2924 UG/LITER .0095207 .1831944 1924.179
ZN2138 UG/LITER -.271121 .123035 45.38024
PB2203 UG/LITER .1459099 .6191625 424.3458
SE1960 UG/LITER -.411460 .796283 193.5261
SB2068 UG/LITER 1.489782 1.051664 70.69180
tfl tf2 tl3
-.626948 .2595344 -.079028
2.494226 .3386434 1.562638
-.073636 .2195445 -.117347
-.145131 -.277259 -.390972
.8594448 -.171958 -.249757
.3943892 -1.19782 -.430951
.9921389 .7793017 2.697906
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.392807 .578166 147.1884
22031 UG/LITER 3.410836 1.880621 55.13657
22032 UG/LITER -1.49416 1.15794 77.49792
20681 UG/LITER -.988607 1.383886 139.9834
20682 UG/LITER 2.717068 2.168858 79.82347
19501 UG/LITER .4546331 1.535571 359.7562
19602 UG/LITER -.853911 .549887 64.39632
tfl ff2 ff3
-.799962 -.647426 .2689679
4.043947 1.295360 4.893200
-.740533 -.914485 -2.82746
-1.34193 .5376884 -2.16158
2.147316 .8899588 5.113930
2.334839 -.639455 -.331484
-.684495 -1.48655 -.490586
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SNI899 UG/LITER 3.721821 .564368 15.16377
BI2230 UG/LITER -.241615 .924035 382.4415
MO2020 UG/LITER 1.403744 .985461 70.20231
TI3349 UG/LITER -1.12280 1.11676 99.46259
B_2496 UG/LITER .5905049 .7158135 121.2206
Y_3710 PPM 1214.733 8.983 .7395220
tfl #2 #3
3.209273 4.326639 3.629551
-1.28655 .0939713 .4677335
2.446104 1.277849 .4872814
.1547209 -1.60950 -1.91361
1.380156 .4071680 -.015809
1207.533 1224.800 1211.867
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
282
285 08/12/10 04:31:53 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: 1007157-07RE1 RUN TIME: 08/12/10 16:24:57 COMMENT: SDGiittSXaa. CLIENTID:MY71T5 1: MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.256451 .192895 75.21687
AL3082 UG/LITER 12268.39 706.38 5.757740
BA4 934 UG/LITER 21.08223 1.14669 5.439139
BE3130 UG/LITER 1.046240 .104804 10.01724
CA3179 UG/LITER 61672.56 3776.19 6.121337
CD2265 UG/LITER 1.020024 .117840 11.55264
C02286 UG/LITER 63.40011 3.23631 5.104584
#1 #2 #3
-.281257 -.052354 -.435744
13082.78 11900.55 11821.83
22.40571 20.45517 20.38581
1.165307 .9679660 1.005446
66021.53 59756.65 59239.50
.8839786 1.085819 1.090274
67.13652 61.58774 61.47606
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 7.625199 .646192 8.474430
CU3247 UG/LITER 7.587237 .099232 1.307881
FE2714 UG/LITER 23206.62 1309.76 5.643903
K_7654 UG/LITER 5365.787 275.194 5.128674
MG2790 UG/LITER 159568.0 9057.8 5.676481
MN2576 UG/LITER 1278.644 72.408 5.652837
NA3302 UG/LITER 63088.32 2871.94 4.552253
tfl #2 ft3
8.342081 7.445989 7.087526
7.622234 7.664229 7.475249
24715.66 22539.12 22365.09
5683.110 5221.656 5192.595
170003.2 154962.1 153738.6
1362.053 1241.939 1231.939
66391.23 61694.09 61179.65
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 181.1144 10.2436 5.655864
TL1908 UG/LITER .8763031 3.763078 429.4265
V_2924 UG/LITER 1.314941 .233260 17.73917
ZN2138 UG/LITER 598.7527 34.7406 5.802166
PB2203 UG/LITER 1.951926 1.328822 58.07751
SE1960 UG/LITER 1.513009 .732183 48.39251
SB2068 UG/LITER 1.655114 .602144 36.38079
ttl #2 ff3
192.8860 176.2294 174.2276
-3.45207 3.371576 2.709408
1.197745 1.583560 1.163518
638.7121 581.8309 575.7153
3.081246 .4876848 2.285847
1.204196 .9858231 2.349007
2.349857 1.331750 1.283736
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 50000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.111491 .464491 416.6182
22031 UG/LITER 3.655628 2.067752 56.56353
22032 UG/LITER 1.088476 1.320138 121.2831
20681 UG/LITER -1.52746 1.84057 120.4982
20682 UG/LITER 3.233853 .384658 11.89469
19601 UG/LITER -.542403 1.474350 271.8180
19602 UG/LITER 2.529016 .393668 15.56606
#1 ff2 #3
.3962245 -.215612 -.515085
4.091178 1.404795 5.470909
2.563361 .0174184 .5845488
.4419502 -3.20408 -1.82026
3.291572 3.586345 2.823573
-1.42780 -1.35898 1.159566
2.507505 2.146545 2.932999
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 3.288909 .504345 15.33472
BI2230 UG/LITER 1.335435 1.789605 134.0091
MO2020 UG/LITER .1255285 .4065955 323.9059
TI3349 UG/LITER .4131133 3.717127 899.7840
B_2496 UG/LITER 1890.219 103.910 5.497242
Y_3710 PPM 1206.155 54.826 4.545514
#1 #2 #3
2.715048 3.489952 3.661727
1.094662 3.233239 -.321594
.5645516 .0501137 -.238080
4.017014 .6300640 -3.40774
2009.961 1836.953 1823.742
1143.133 1232.467 1242.857
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
283
286 ANALYSIS REPORT
08/12/10 04:38:53 PM
METHOD: ALT-P3Q3 SAMPLE NAME: 0001015 DUPI- ' RUNTIME: 08/12/10 16:31:57 o &. I 3 . I t> 'ScS^t v.-^ COMMENT: SDG:MYS1S3 CLIENTID:MY71T5D 1:2 MODE: CONC . CORR. FACTOR: 1
PAGE 1
OPERATOR:
1*3^
AG3280 UG/LITER -.248771 .182452 73.34119
AL3082 UG/LITER 11658.75 126.54 1.085343
BA4934 UG/LITER 19.97386 .23455 1.174297
BE3130 UG/LITER .8796341 .0206861 2.351669
CA3179 UG/LITER 58227.21 602.57 1.034855
CD2265 UG/LITER 1.013706 .136483 13.46374
C02286 UG/LITER 60.27311 .88718 1.471930
.045419 .398139 .302756
11762.77 11517.88 11695.61
20.18498 19.72137 20.01522
.8982104 .8573419 .8833600
58909.98 57769.81 58001.83
1.085870 1.098957 .8562903
60.85415 59.25192 60.71326
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.OOOOO
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 6.548715 .115042 1.756708
CU3247 UG/LITER 7.454251 .137692 1.847166
FE2714 UG/LITER 22081.97 252.87 1.190439
K_7664 UG/LITER 5138.260 43.898 .8543319
MG2790 UG/LITER 151914.4 1617.7 1.064849
MN2576 UG/LITER 1216.128 13.691 1.125760
NA3302 UG/LITER 60624.41 434.39 .7177109
#1 #2 #3
6.612990 6.617256 6.415899
7.580238 7.307266 7.475249
22309.32 21794.13 22142.47
5174.616 5089.493 5150.670
153223.8 150106.0 152413.4
1227.742 1201.033 1219.609
60871.54 60037.29 60664.40
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 173.3079 1.8712 1.079684
TL1908 UG/LITER -1.25917 .90360 71.76135
V_2924 UG/LITER 1.444173 .044747 3.098416
ZN2i38 UG/LITER 569.0771 6.1566 1.081851
PB2203 UG/LITER 1.331816 .614799 46.15245
SE1960 UG/LITER .0292958 1.639258 5595.536
SB2068 UG/LITER 1.066606 1.472085 138.0158
#1 #2 ft3
174.5949 171.1614 174.1674
-2.09065 -.297564 -1.38930
1.419036 1.495836 1.417649
573.8715 552.1341 571.2256
1.165808 .8170666 2.012573
1.759700 -1.50032 -.171494
2.754535 .3956531 .0495209
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.235651 .487777 206.9912
22031 UG/LITER 3.712295 .807857 21.76166
22032 UG/LITER .1309266 .5278244 403.1452
20681 UG/LITER -.915911 1.452506 158.5859
20682 UG/LITER 2.046568 1.627759 79.53602
19501 UG/LITER -3.79411 2.14190 56.45341
19602 UG/LITER 1.928321 1.392732 72.22515
#1 #2 #3
-.204014 -.738477 .2355374
3.645047 2.940164 4.551674
-.084313 -.255268 .7323606
.4122423 -.692981 -2.46699
3.914189 .9294698 1.296047
-1.60772 -5.88857 -3.88603
3.430996 .6808200 1.673145
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 3.481843 2.100742 62.63183
BI2230 UG/LITER -.824157 1.806568 228.9089
MO2020 UG/LITER -.395450 .328962 82.97692
TI3349 UG/LITER -1.54917 .41759 25.95603
B_2495 UG/LITER 1801.458 16.881 .9370720
Y_3710 PPM 1246.889 12.374 .9932048
#1 #2 #3
1.615181 5.878839 2.951509
1.296981 -2.31462 -1.45494
-.622143 -.019004 -.548203
-1.26669 -1.35198 -2.02885
1814.580 1782.443 1807.250
1236.333 1259.867 1241.457
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
ELEM UNITS AVGE SDEV %RSD itl
#2 #3
284
287 08/12/10 04:45:63 PM
ANALYSIS REPORT
METHOD: ALT-P3Q3 SAMPLE NAME: SDI1007157-07RE1 RUN TIME: 08/12/10 15:38:67 COMMENT: SDG:MYC1C3. CLIENTID:MY71T5L 1:10 MODE: CONC CORR. FACTOR: 1
t^r^i'==.3
06.1-^.10
"^y)
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.322800 .240766 74.58565
AL3082 UG/LITER 2359.468 3.720 .1576465
BA4934 UG/LITER 3.772591 .053650 1.422377
BE313 0 UG/LITER .2975144 .0139996 4.705495
CA3179 UG/LITER 12489.43 366.24 2.932412
CD2265 UG/LITER .2131698 .0537480 25.21373
C02286 UG/LITER 12.72039 .12117 .9526312
ftl #2 #3
-.577796 -.291223 -.099381
2357.149 2353.758 2357.496
3.817299 3.713084 3.787390
.2834506 .3114487 .2976439
12308.52 12910.92 12248.85
.2500640 .1515027 .2379427
12.81333 12.76448 12.58335
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.00000
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 1.016918 .122818 12.07748
CU3247 UG/LITER 1.105889 .303260 27.42230
FE2714 UG/LITER 4613.511 3.265 .0707967
K_7654 UG/LITER 879.2783 8.1794 .9302365
MG2790 UG/LITER 30865.84 60.60 .1963192
MN257 6 UG/LITER 254.2236 .5978 .2351533
NA3302 UG/LITER 12359.02 94.71 .7663533
#1 #2 #3
.9472904 .9447355 1.158729
.7559243 1.270372 1.291371
4616.578 4614.145 4610.111
888.5574 876.1639 873.1137
30909.85 30890.94 30796.73
254.8418 254.1807 253.6485
12381.92 12440.19 12254.95
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 36.48012 .51587 1.414124
TL190a UG/LITER .5084125 1.354656 222.6542
V_2924 UG/LITER .2783796 .1393610 50.06151
ZN213a UG/LITER 113.0556 .3397 .3004725
PB2203 UG/LITER .4112923 .5662679 137.6802
SE1960 UG/LITER -.322148 2.055776 538.1462
SB2068 UG/LITER .5129296 .8917894 173.8620
tfl it2 #3
36.76258 35.88514 36.80264
2.171232 -.230341 -.115654
.2338130 .1667531 .4345729
113.0872 113.3784 112.7012
.7519899 .7242685 -.242382
-2.55706 .1024297 1.488189
1.434414 .4502300 -.345855
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.835235 1 .118877 133.9596
22031 UG/LITER 3.788361 1.656147 43.71672
22032 UG/LITER -1.28718 .68023 52.84634
20581 UG/LITER -2.54872 1.64950 64.71899
20682 UG/LITER 2.031483 1.743186 85.80856
19601 UG/LITER -.405281 3.324142 820.2071
19602 UG/LITER -.290619 1.484167 510.6911
lfl #2 #3
-.507482 -2.08139 .0831637
3.246074 5.647669 2.471340
-.505687 -1.74620 -1.60965
-2.17135 -4.35421 -1.12060
3.224587 2.838880 .0309810
-4.19682 .9726980 2.008277
-1.74842 -.342019 1.218580
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.270665 .784994 34.67109
BI2230 UG/LITER -1.44452 1.92583 133.3193
MO2020 UG/LITER -.660086 .118895 18.01200
TI3349 UG/LITER -1.19417 3.28116 274.7659
B_2496 UG/LITER 374.7320 1.6491 .4400788
Y_3710 PPM 1224.489 2.958 .2416069
#1 #2 if3
2.072824 3.135552 1.603517
.7791643 -2.57148 -2.54126
-.585256 -.597820 -.797182
-4.67849 -.740656 1.836656
374.6628 376.4147 373.1186
1221.200 1225.333 1226.933
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
285
288 ANALYSIS REPORT
08/12/10 04:55:17 PM
PAGE 1
«''7fe|'Z.-l2>S2METHOD: ALT-P3Q3 SAMPLE NAME: mi7?fii p-RgO— RUNTIME: 08/12/10 16:48:20 O^.C^.IO COMMENT: SDG:MY71L3 CLIENTID:LCSS $ ^ V / V 1:2 MODE: CONC CORR. FACTOR:
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 24.48506 .14167 .5786009
AL3082 UG/LITER 491.6299 2.7389 .5570993
BA4934 UG/LITER 7.652432 .018688 .2442164
BE3130 UG/LITER 25.26067 .04942 .1956425
CA3179 UG/LITER 242914.9 298.2 .1227554
CD2265 UG/LITER 56.41708 .13590 .2408844
C02286 UG/LITER 196.5901 .2146 .1091469
#1 if2 #3
24.50936 24.33282 24.61302
494.7687 490.3960 489.7261
7.663116 7.630853 7.663328
25.30932 25.21050 25.26190
243258.7 242726.0 242760.0
56.56830 56.30515 56.37780
196.5351 196.4084 196.8268
ERRORS HIGH LOW
LC PASS 1000.000 -10.0000
LC PASS 400000.0 -200.000
LC PASS 50000.00 -200.000
LC PASS 4000.000 -5.OOOOO
LC PASS 400000.0 -1000.00
LC PASS 10000.00 -5.00000
LC PASS 50000.00 -50.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 140.5765 .8513 .6055432
CU3247 UG/LITER 8610.789 27.202 .3159070
FE2714 UG/LITER 32332.58 21.24 .0656936
K_7664 UG/LITER 66.45917 4.00539 6.026844
MG2790 UG/LITER 150964.4 30.8 .0203596
MN2576 UG/LITER 312.3908 .3056 .0978218
NA3302 UG/LITER 622.3071 66.7796 10.73097
ttl fl2 tf3
139.7608 140.5093 141.4594
8579.401 8625.460 8627.507
32328.19 32313.88 32365.68
70.55094 66.28042 62.54615
150961.2 150995.6 150935.4
312.0523 312.4737 312.6463
660.3065 661.4156 545.1993
ERRORS HIGH LOW
LC PASS 60000.00 -10.0000
LC PASS 60000.00 -25.0000
LC PASS 700000.0 -100.000
LC PASS 400000.0 -1000.00
LC PASS 300000.0 -1000.00
LC PASS 40000.00 -15.0000
LC PASS 700000.0 -2000.00
ELEM UNITS AVGE SDEV %RSD
N12316 UG/LITER 83.92566 .39595 .4717913
TL1908 UG/LITER 46.26203 .83329 1.801230
V_2924 UG/LITER 93.43066 .17470 .1869871
ZN2138 UG/LITER 219.0822 .1534 .0700050
PB2203 UG/LITER 301.8603 1.0147 .3361652
SE1960 UG/LITER 49.63703 2.17082 4.373389
SB2068 UG/LITER 300.2760 1.2754 .4247468
#1 #2 fl3
84.00771 83.49511 84.27416
47.01311 45.36565 46.40734
93.34740 93.31317 93.63142
218.9887 219.2592 218.9986
302.8854 301.8394 300.8562
48.24856 48.52389 52.13863
301.4450 300.4672 298.9158
ERRORS HIGH LOW
LC PASS 60000.00 -40.0000
LC PASS 60000.00 -10.0000
LC PASS 50000.00 -50.0000
LC PASS 10000.00 -20.0000
LC PASS 60000.00 -3.00000
LC PASS 30000.00 -5.00000
LC PASS 40000.00 -60.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 1218.769 1.63 5 .1341893
22031 UG/LITER 309.2087 1.8969 .6134594
22032 UG/LITER 298.1794 1.8495 .6202966
20681 UG/LITER 297.2373 .4076 .1371275
20682 UG/LITER 301.7848 1.7125 .5674489
19601 UG/LITER 40.29310 3.93968 9.777544
19602 UG/LITER 54.29149 1.41322 2.603016
itl #2 tf3
1220.362 1217.094 1218.849
308.0037 311.3952 308.2272
300.3142 297.0582 297.1658
297.5467 297.3895 296.7754
303.3825 301.9950 299.9770
38.70560 37.39484 44.77886
53.00235 54.06959 55.80253
ERRORS
LC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
HIGH LOW
20000.00 -10.0000
ELEM UNITS AVGE SDEV %RSD
SNI 8 99 UG/LITER 15.44100 2.78128 18.01234
BI2230 UG/LITER 105.8611 .8883 .8391460
MO2020 UG/LITER 67.23395 .53742 .9480655
TI3349 UG/LITER 30.30575 3.23405 10.67145
B_2496 UG/LITER 8.517642 .630841 7.406290
Y_3710 PPM 1167.400 3.880 .3324017
ftl tf2 #3
15.52692 12.51775 18.17833
105.4798 106.8764 105.2270
66.97154 66.75962 67.96069
27.41508 29.70361 33.79857
9.064483 7.827467 8.660977
1163.000 1168.867 1170.333
ERRORS HIGH LOW
LC PASS 40000.00 -20.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -10.0000
LC PASS 40000.00 -30.0000
LC PASS 40000.00 -50.0000
NOCHECK
286
289 ANALYSIS REPORT
QC STANDARD
08/12/10 05:02:17 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CRI RUN TIME: 08/12/10 15:55:20 COMMENT: CRI MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 7.374454 .342896 4.649783
AL3082 UG/LITER -40.6864 .8402 2.064943
BA4 934 UG/LITER -.493612 .014682 2.954076
BE3130 UG/LITER 4.978596 .016048 .3223458
CA3179 UG/LITER -89.9781 178.9145 198.8424
CD2265 UG/LITER 4.956358 .026089 .5263686
C02286 UG/LITER 49.59969 .15790 .3183558
#1 #2 It3
7.761969 7.289123 7.082282
-39.8716 -40.6380 -41.5498
-.495262 -.478276 -.507299
4.996894 4.966911 4.971982
13.26281 13.37376 -296.571
4.944158 4.938596 4.986311
49.44383 49.75956 49.59559
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS .OOOOOOO 400.0000
QC PASS .OOOOOOO 400.0000
QC PASS 5.000000 1.500000
QC PASS .OOOOOOO 2000.000
QC PASS 5.000000 1.500000
QC PASS 50.00000 15.00000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 9.582826 .427917 4.465460
CU3247 UG/LITER 23.76261 .25227 1.061607
FE2714 UG/LITER -7.28615 6.56068 90.04314
K_7664 UG/LITER .7839671 2.085043 266.0880
MG2790 UG/LITER 6.697803 1.623946 24.24594
MN2576 UG/LITER 14.26532 .03017 .2115088
NA3302 UG/LITER -12.1483 24.4200 201.0151
ttl ff2 #3
9.363606 10.07593 9.308937
23.74851 24.02158 23.51763
-6.52908 -1.07873 -14.1506
-.508146 3.190537 -.330489
8.117098 7.049476 4.926836
14.27573 14.28891 14.23133
-35.1493 13.47840 -14.7741
ERRORS VALUE RANGE
QC PASS 10.00000 3.000000
QC PASS 25.00000 7.500000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 2000.000
QC PASS .OOOOOOO 2000.000
QC PASS 15.00000 4.500000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 39.32257 .69796 1.774955
TL1908 UG/LITER 25.19079 .69406 2.755214
V_2924 UG/LITER 49.30474 .19398 .3934388
ZN2138 UG/LITER 52.11883 .24232 .4649283
PB2203 UG/LITER 9.503007 .668663 7.036335
SE1960 UG/LITER 33.10121 1.24134 3.750138
SB2068 UG/LITER 60.76561 .65006 1.069784
#1 #2 #3
39.22407 40.06455 38.67909
25.59930' 49.33673 24.38941 49.48074 25.68365 49.09675
51.98785 52.39845 51.97021
8.806282 9.563199 10.13954
33.99252 33.62773 31.68339
61.14767 60.01502 61.13412
ERRORS VALUE RANGE
QC PASS 40.00000 12.00000
QC PASS 25.00000 12.50000
QC PASS 50.00000 15.00000
QC PASS 60.00000 18.00000
QC PASS 10.00000 5.000000
QC PASS 35.00000 10.50000
QC PASS 60.00000 30.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 8.373795 .361953 4.322452
22031 UG/LITER 13.80171 1.67222 12.11602
22032 UG/LITER 7.341788 1.817798 24.75961
20681 UG/LITER 57.65562 2.04702 3.550419
20682 UG/LITER 62.30821 .25603 .4109026
19601 UG/LITER 33.64642 3.82859 11.37890
19602 UG/LITER 32.81895 .78442 2.390151
ftl ft2 #3
8.138111 8.192723 8.790552
15.22907 14.21422 11.96185
5.584592 7.226109 9.214663
58.31155 55.36102 59.29421
62.55349 62.32849 62.04265
37.56432 33.46105 29.91387
32.19922 33.70090 32.55677
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
10.00000 3.000000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 52.31014 1.20790 2.309119
BI2230 UG/LITER 49.61898 1.54143 3.106531
MO2020 UG/LITER 48.88490 .33204 .6792205
TI3349 UG/LITER 42.92623 2.84649 6.631119
B_2496 UG/LITER 48.91474 .68659 1.403651
Y_3710 PPM 1214.133 1.600 .1317843
ttl #2 #3
53.70351 51.56754 51.55936
51.24709 49.42777 48.18207
48.50362 49.04070 49.11039
43.60228 45.37383 39.80258
49.12510 49.47154 48.14758
1212.533 1215.733 1214.133
ERRORS VALUE RANGE
NOCHECK
QC PASS 50.00000 15.00000
NOCHECK
NOCHECK
QC PASS 50.00000 15.00000
NOCHECK
287
290 ANALYSIS REPORT
QC STAWDARD
08/12/10 05:09:17 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSA RUN TIME: 08/12/10 17:02:20 COMMENT: ICSA MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER -.303780 .338681 111.4889
AL3082 UG/LITER 246184.8 1352.0 .5491735
BA4934 UG/LITER 2.492774 .067757 2.718118
BE3130 UG/LITER .9085756 .0126196 1.388944
CA3179 UG/LITER 243892.4 1913.0 .7843704
CD2265 UG/LITER 2.548882 .208494 7.871021
C02286 UG/LITER 5.159429 .229299 4.444268
ttl #2 it3
-.694331 -.126040 -.090969
244823.9 246203.0 247527.7
2.457068 2.450339 2.570916
.8980827 .9050655 .9225787
241772.3 244415.2 246489.7
2.805385 2.729060 2.412201
5.035897 5.018382 5.424007
ERRORS VALUE RANGE
QC PASS .OOOOOOO 20.00000
QC PASS 243900.0 49997.06
QC PASS 2.000000 400.0000
QC PASS .OOOOOOO 10.00000
QC PASS 234100.0 47990.00
QC PASS .OOOOOOO 10.00000
QC PASS 3.000000 100.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 44.00748 .23783 .5404223
CU3247 UG/LITER 22.34175 .23217 1.039158
FE2714 UG/LITER 98465.09 658.20 .6684603
K_7664 UG/LITER 4.464153 1.943736 43.54097
MG2790 UG/LITER 254768.0 1602.5 .6290061
t«I2576 UG/LITER 17.86173 .14315 .8014193
NA3302 UG/LITER 990.0743 54.2348 5.477854
tfl tf2 tf3
43.86904 43.87130 44.28210
22.16327 22.60422 22.25776
97778.43 98526.30 99090.55
6.350660 4.573956 2.467844
253083.8 17.72083 254946 .3 17.85735 256273.9 18.00702
930.1602 1004.247 1036.816
ERRORS VALUE RANGE
QC PASS 36.00000 20.00000
QC PASS 15.00000 50.00000
QC PASS 94900.00 19454.00
QC PASS .OOOOOOO 2000.000
QC PASS 248800.0 51003.00
QC PASS 19.00000 30.00000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 21.38799 .27821 1.300800
TL1908 UG/LITER -1.55747 4.42676 284.2284
V_2924 UG/LITER 1.013690 .447611 44.15658
ZN2138 UG/LITER 23.06852 .28505 1.015540
PB2203 UG/LITER 12.16767 .58667 4.821557
SE1960 UG/LITER -1.54052 .19354 12.56339
SB2068 UG/LITER 3.277855 .892818 27.23787
til ff2 #3
21.30656 21.69780 21.15950
-4.74712 3.496525 -3.42180
.6690270 1.519579 .8524628
27.83591 27.98314 28.38650
11.52698 12.29747 12.67858
-1.33218 -1.71472 -1.57466
2.386344 3.275248 4.171974
ERRORS VALUE RANGE
QC PASS 10.00000 80.00000
QC PASS .OOOOOOO 50.00000
QC PASS 1.000000 100.0000
QC PASS 39.00000 120.0000
QC PASS 5.000000 20.00000
QC PASS .OOOOOOO 70.00000
QC PASS .OOOOOOO 120.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER .5887148 1.028682 174.7335
22031 UG/LITER -3.36854 .54841 16.28036
22032 UG/LITER 19.90959 .91444 4.592972
20681 UG/LITER .9011372 3.797567 421.4194
20682 UG/LITER 4 .454316 1.912076 42.92636
19601 UG/LITER -4.47834 2.83555 63.31700
19602 UG/LITER -.084372 1.187438 1407.381
ifl tf2 ft3
1.243103 1.120019 -.596977
-3.17821 -3.98676 -2.94065
18.85406 20.41283 20.46188
1.680771 -3.22574 4.248384
2.729406 6.510315 4.123227
-1.29004 -5.42722 -6.71777
-1.36373 .1281834 .9824333
ERRORS
OC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 20.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.953136 3.487276 117.6887
BI2230 UG/LITER 4.151650 1.539875 37.09067
MO2020 UG/LITER -.355874 .283288 79.50335
TI3349 UG/LITER -1.27709 3.17595 248.6867
B_2496 UG/LITER -5.10026 .41002 8.039153
Y_3710 PPM 1162.156 4.801 .4130776
til ft2 ti3
6.831689 1.996750 .0609679
2.440689 5.426256 4.587994
-.109948 -.292043 -.665631
-4.84737 1.233677 -.217583
-5.55667 -4.75306 -4.98104
1167.000 1162.057 1157.400
ERRORS VALUE RANGE
NOCHECK
NOCHECK
NOCHECK
NOCHECK
QC PASS .OOOOOOO 200.0000
NOCHECK
288
291 ANALYSIS REPORT
QC STANDARD
08/12/10 05:16:17 PM
PAGE 1
OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: ICSAB RUN TIME: 08/12/10 17:09:20 COMMENT: ICSAB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 197.5913 .4311 .2181935
AL3082 UG/LITER 248302.9 1026.6 .4134602
BA4934 UG/LITER 511.2613 2.4025 .4699217
BE3130 UG/LITER 488.3202 2.0206 .4137812
CA3179 UG/LITER 246247.2 398.5 .1618159
CD2265 UG/LITER 983.9527 4.5443 .4618436
C02286 UG/LITER 502.6020 1.9771 .3933817
11 #2 #3
197.2554 198.0774 197.4411
248254.4 249353.0 247301.4
511.3815 513.6014 508.8008
488.0146 490.4761 486.4698
246302.5 246615.2 245824.0
984.5923 988.1433 979.1224
602.7386 504.5073 500.5601
ERRORS VALUE RANGE
QC PASS 210.0000 43.00000
QC PASS 248400.0 50922.00
QC PASS 475.0000 400.0000
QC PASS 482.0000 98.00001
QC PASS 234300.0 48031.00
QC PASS 916.0000 187.0000
QC PASS 455.0000 100.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 534.8631 1.8463 .3451930
CU3247 UG/LITER 522.6969 .8623 .1649787
FE2714 UG/LITER 99500.61 424.96 .4270934
K_7654 UG/LITER 14.15241 4.26741 30.13195
MG2790 UG/LITER 257229.8 1057.7 .4112026
MN2576 UG/LITER 514.4127 2.0751 .4033879
NA3302 UG/LITER 979.9514 27.5555 2.812041
ftl 12 #3
534.8746 536.7036 533.0110
522.2909 523.6873 522.1125
99478.96 99935.98 99086.88
18.90127 10.62328 12.96267
257188.3 258307.7 256193.4
514.4887 516.4488 512.3007
1010.488 972.4301 956.9352
ERRORS VALUE RANGE
QC PASS 506.0000 103.0000
QC PASS 537.0000 110.0000
QC PASS 95100.00 19495.00
QC PASS .OOOOOOO 2000.000
QC PASS 254100.0 52090.00
QC PASS 483.0000 99.00000
QC PASS .OOOOOOO 2000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 1029.425 4.411 .4285268
TL1908 UG/LITER 98.55780 1.69825 1.723096
V_2924 UG/LITER 505.8034 2.2444 .4437275
ZN2138 UG/LITER 1023.730 4.654 .4546344
PB2203 UG/LITER 63.35514 .77786 1.227779
SE1960 UG/LITER 44.88772 3.35288 7.469483
SB2068 UG/LITER 621.4973 2.8698 .4517487
#1 it2 ff3
1030.047 1033.493 1024.736
98.93527 95.70258 100.0356
505.7317 508.0828 503.5957
1023.133 1028.654 1019.403
62.45732 63.82656 63.78154
41.03085 45.52420 47.10811
622.0272 624.0551 618.3995
ERRORS VALUE RANGE
QC PASS 930.0000 190.0000
QC PASS 96.00000 50.00000
QC PASS 481.0000 99.99999
QC PASS 975.0000 199.0000
QC PASS 51.00000 20.00000
QC PASS 51.00000 70.00000
QC PASS 585.0000 120.0000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER 101.4234 .5866 .5783662
22031 UG/LITER 45.55674 2.07822 4.661818
22032 UG/LITER 72.22862 2.09072 2.894580
20681 UG/LITER 618.8804 5.2340 .8457210
20682 UG/LITER 622.7972 2.2289 .3578886
19501 UG/LITER 38.71837 7.21471 18.63382
19602 UG/LITER 47.95713 1.65614 3.453371
#1 #2 #3
102.0063 100.8331 101.4309
47.43255 43.32269 45.91498
69.94604 74.05070 72.68909
622.2814 621.5065 612.8533
621.8937 625.3360 621.1519
30.43927 43.66074 42.05509
46.30805 47.94311 49.62024
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
97.00000 20.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 999.4022 7.2514 .7255726
BI2230 UG/LITER 1030.398 5.469 .5307238
MO2020 UG/LITER 989.8129 4.3256 .4370068
TI3349 UG/LITER 1013.625 7.678 .7574353
B_2496 UG/LITER 1016.272 4.028 .3963280
Y_3710 , PPM 1154.489 3.554 .3078049
tfl ff2 ii3
999.1926 1005.756 992.2579
1029.727 1035.171 1025.296
985.5461 994.1949 989.6979
1015.083 1020.471 1005.325
1015.950 1020.451 1012.415
1153.067 1151.867 1158.533
ERRORS VALUE RANGE
QC PASS 1000.000 205.0000
QC PASS 1000.000 205.0000
QC PASS 1000.000 205.0000
QC PASS 1000.000 205.0000
QC PASS 1000.000 200.0000
NOCHECK
289
292 ANALYSIS REPORT
QC STANDARD
08/12/10 05:23:19 PM
METHOD: ALT-P3Q3 SAMPLE NAME: CCV RUN TIME: 08/12/10 17:16:21 COMMENT: CCV CVSl MODE: CONC CORR. FACTOR: 1
PAGE 1
OPERATOR:
ELEM UNITS AVGE SDEV %RSD
AG3280 UG/LITER 97.97191 .13572 .1395457
AL3082 UG/LITER 48445.18 222.40 .4590803
BA4 934 UG/LITER 986.6097 4.7047 .4768532
BE3130 UG/LITER 977.3016 3.6920 .3777741
CA3179 UG/LITER 47418.02 246.60 .5200525
CD2265 UG/LITER 968.2211 3.0699 .3170638
C02286 UG/LITER 973.5599 3.2825 .3371637
#1 #2 #3
97.81472 98.06317 98.03783
48503.00 48199.58 48632.96
988.2604 981.3021 990.2666
976.8691 973.8450 981.1909
47206.24 47359.07 47688.75
967.4388 965.6180 971.6064
973.6547 970.2310 976.7939
ERRORS VALUE RANGE
QC PASS 100.0000 10.40000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER 972.6111 3.7148 .3819442
CU3247 UG/LITER 985.2804 1.4357 .1457134
FE2714 UG/LITER 24406.60 84.61 .3466762
K_7664 UG/LITER 47452.44 242.69 .5114337
MG2790 UG/LITER 48279.92 186.58 .3866561
MN2576 UG/LITER 967.8136 3.8583 .3986617
NA3302 UG/LITER 48643.84 160.16 .3292601
#1 ft2 it3
972.8796 968.7694 975.1844
986.1858 983.6251 986.0294
24417.22 24317.18 24485.40
47605.83 47172.64 47578.84
48269.50 48098.67 48471.59
967.9309 963.8980 971.6119
48693.11 48464.82 48773.57
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 25000.00 2600.000
QC PASS 50000.00 5200.000
QC PASS 50000.00 5200.000
QC PASS 1000.000 104.0000
QC PASS 50000.00 5200.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER 977.7737 4.4005 .4500516
TL1908 UG/LITER 980.9985 4.5703 .4658874
V_2924 UG/LITER 990.4458 3.7029 .3738573
ZN2138 UG/LITER 1053.950 4.847 .4598986
PB2203 UG/LITER 973.3630 4.2485 .4364803
SE1960 UG/LITER 978.9324 4.3406 .4433965
SB2068 UG/LITER 1016.048 4.296 .4228247
ftl #2 #3
977.8497 973.3357 982.1357
976.4111 981.0328 985.5516
990.3135 986.8109 994.2131
1053.392 1049.406 1059.052
973.1227 969.2397 977.7266
975.9945 975.8846 983.9180
1013.873 1013.273 1020.996
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1100.000 114.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
ELEM LTNITS AVGE SDEV %RSD
AS1890 UG/LITER 991.8718 4.2579 .4292824
22031 UG/LITER 969.9846 2.8969 .2986553
22032 UG/LITER 975.0396 4.9389 .5065304
20681 UG/LITER 1008.657 7.143 .7081519
20582 UG/LITER 1019.735 2.921 .2864939
19601 UG/LITER 973.8349 2.3970 .2461365
19602 UG/LITER 981.4672 5.9546 .6077229
#1 #2 #3
992.5663 987.3093 995.7398
970.2529 966.9628 972.7380
974.5453 970.3665 980.2070
1005.867 1003.331 1016.774
1017.868 1018.234 1023.101
974.8865 971.0919 975.5263
976.5375 979.7667 988.0974
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
1000.000 104.0000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 988.4454 3.1591 .3195003
BI2230 UG/LITER 995.6310 2.4181 .2428689
MO2020 UG/LITER 995.0039 4.1762 .4197178
TI3349 UG/LITER 995.6885 1.0075 .1011843
B_2495 UG/LITER 1002.343 3.727 .3718448
Y_3710 PPM 1207.889 4.128 .3417625
#1 #2 #3
987.1019 986.1821 992.0554
998.1255 993.2974 995.4702
992.4190 992.7707 999.8218
995.1179 995.0959 996.8518
1001.821 998.9042 1006.303
1207.333 1212.267 1204.067
ERRORS VALUE RANGE
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
QC PASS 1000.000 104.0000
NOCHECK
290
293 ANALYSIS REPORT
QC STANDARD
08/12/10 05:30:20 PM OPERATOR:
METHOD: ALT-P3Q3 SAMPLE NAME: CCB RUN TIME: 08/12/10 17:23:22 C0MME3TT: CCB MODE: CONC CORR. FACTOR: 1 ELEM UNITS AVGE SDEV %RSD
PAGE 1
AG3280 UG/LITER -.286344 .077613 27.10471
AL3082 UG/LITER -34.9651 11.0701 31.65044
BA4934 UG/LITER -.369782 .051103 13.81972
BE3130 UG/LITER .2062993 .0481868 23.35771
CA3179 UG/LITER -92.5546 168.3815 181.9266
CD2265 UG/LITER .3117756 .1577045 50.58269
C02286 UG/LITER .1564508 .1551267 99.15360
-.283803 -.210032 -.365195
-47.5481 -26.7248 -30.6223
-.337607 -.343031 -.428707
.1561617 .2522639 .2104722
-286.985 4.743157 4.577777
.3340755 .4571432 .1441081
.0473042 .3340263 .0880220
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 200.0000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
ELEM UNITS AVGE SDEV %RSD
CR2677 UG/LITER .1551380 .1308793 84.36316
CU3247 UG/LITER -.577441 .121080 20.96834
FE2714 UG/LITER 2.910436 1.133676 38.95210
K_7664 UG/LITER 6.097290 5.938049 97.38833
MG2790 UG/LITER 22.51745 4.64156 20.61316
MN2576 UG/LITER -.159743 .054978 34.41669
NA3302 UG/LITER 53.40189 62.12603 116.3368
ttl it2 #3
.2977817 .1270481 .0405843
-.461953 -.566942 -.703429
3.641368 3.485462 1.604478
6.376442 11.89084 .0245888
24.61063 25.74379 17.19792
-.104120 -.161057 -.214054
67.47751 107.2825 -14.5543
ERRORS VALUE RANGE
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 5.000000
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 5000.000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 5000.000
ELEM UNITS AVGE SDEV %RSD
NI2316 UG/LITER -.153641 .397703 258.8521
TL1908 UG/LITER 3.104457 3.965026 127.7204
V_2924 UG/LITER .1578345 .1534634 97.23051
ZN2138 UG/LITER -.310659 .043812 14.10295
PB2203 UG/LITER -.701370 .751719 107.1787
SE1960 UG/LITER -.016866 1.044173 6190.972
SB2068 UG/LITER 1.498032 ,500734 33.42615
ftl ff2 ft3
.0707008 -.612829 .0812051
7.195204 2.839751 -.721584
.1932973 .2904620 -.010256
-.266671 -.311013 -.354293
-1.49385 .0015619 -.611819
.8617330 -1.17125 .2589184
1.616422 .9487117 1.928962
ERRORS VALUE RANGE
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 10.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 20.00000
QC PASS .OOOOOOO 3.000000
QC PASS .OOOOOOO 5.000000
QC PASS OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
AS1890 UG/LITER -.059707 .349484 585.3335
22031 UG/LITER 3.063344 1.194608 38.99684
22032 UG/LITER -2.69075 .67132 25.91207
20581 UG/LITER -.339481 1.413391 415.3386
20682 UG/LITER 2.405567 .375582 15.61304
19501 UG/LITER 3.791385 2.428638 64.05674
19602 UG/LITER -1 .92808 1.97630 102.5010
ttl tt2 #3
-.417449 .2808886 -.042560
2.236388 4.432958 2.520687
-3.36566 -2.22085 -2.18574
-.839518 -1.43488 1.255954
2.833082 2.128680 2.254941
5.720460 4.589597 1.064099
-1.57347 -4.05767 -.153089
ERRORS
QC PASS
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
NOCHECK
VALUE RANGE
.OOOOOOO 10.00000
ELEM UNITS AVGE SDEV %RSD
SN1899 UG/LITER 2.246679 2.242619 99.81932
BI2230 UG/LITER .2259616 1.087095 481.0974
MO2020 UG/LITER 1.303596 .949133 72.80325
TI3349 UG/LITER -1.33843 1.39158 103.9714
B_2496 UG/LITER .5322856 .2116203 39.73804
Y_3710 PPM 1240.400 40.258 3.245585
ftl tt2 #3
4.828355 1.130624 .7810568
-.605416 -.172833 1.456135
2.399655 .7588066 .7526271
-2.14840 .2684147 -2.13529
.6176311 .6878014 .2914275
1286.867 1216.000 1218.333
ERRORS VALUE RANGE
QC PASS .OOOOOOO 100.0000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 50.00000
QC PASS .OOOOOOO 40.00000
QC PASS .OOOOOOO 50.00000
NOCHECK
Itl tt2 #3
291
294 Maintenance: Method(s)
(circle one): ILM04.1
Operator(s): ^\S-/^
\1<1
/ILMOST)
DateATime
X ^ t - " ^ ^ P Ww.-^Jl 4tA.bv^
ORIGINAL
Others
Q^Mg
to
^illiiiLj/I^
Printed: 8/2/2010 11:54:03 AM
Specified elementfs) fail(s) hiqh Specified elementfs) fail(s) low RR Re-run sample(s) neat RR#X Re-run at a #-fold dilution Sample run at a #-fold dilution (aliquot of sample diluted with acidified water) #X Vlatrix = leachate L W Vlatrix = water Vlatrix = solid s Vlatrix = bioloqical tissue B t
1
Matrix Water
SDG MY71S3
Batch
Comments
^.L 4n
*i^
0072822
HG Run Log (V4) File Name: V408020G Seq
Sample ID
Cup
Client ID
Sample Type
DF
Date
Time
Results
1
SO
SO
CALIB STD
1.0
02 AUG 1
09:48:11
512
2
S0.2
S0.2
CALIB STD
1.0
02 AUG 1
09:50:12
1984
3
S0.5
80.5
CALIB STD
1.0
02 AUG 1
09:52:04
5489
4
SI.O
SI.O
CALIB STD
1.0
02 AUG 1
09:54:29
10327
5
S5.0
S5.0
CALIB STD
1.0
02 AUG 1
09:56:20
49357
6
S10.0
SIO.O
CALIB STD
1.0
02 AUG 1
09:58:15
93769
7
ICVl
ICV
ICV
1.0
02 AUG 1
10:00:18
4.15
8
ICBI
ICB
ICB
1.0
02 AUG 1
10:02:13
.032
CRLI
CRI
CRI
1.0
02 AUG 1
10:04:07
.176
: -10
CCV1
CCV1
CCV
1.0
02 AUG 1
10:06:00
4.97
11
CCBl
CCBl
CCB
1.0
02 AUG 1
10:07:52
-.074
: 12
0072822-BLK1
PBW
BLANK
1.0
02 AUG 1
10:09:54
-.019
H3
1007157-07
MY71T5
SAMPLE
1.0
02 AUG 1
10:11.56
4.82
1-14
0072822-DUPl
MY71T5D
DUPLICATE
1.0
02 AUG 1
10:14:00
4.75
-15
0072822-MS1
MY71T5S
MATRIX SPIKE
1.0
02 AUG 1
10:16:02
5.71
1007157-01
MY71S3
SAMPLE
1.0
02 AUG 1
10:18:12
.084
yi-
1007157-02
MY71S5
SAMPLE
1.0
02 AUG 1
10:20:18
.035
-1-8
1007157-03
MY71S7
SAMPLE
1.0
02 AUG 1
10:22:18
.276
-•19
1007157-04
MY71S9
SAMPLE
1.0
02 AUG 1
10:24:11
.020
-
9
Me- -
.
,
.
_
•
:
•
Comments
1.,
,The presence of the Chemist's/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials df the lab supervisor and a QA department representative, signifying approval of the deviation.
Reviewed By:
y
Date:
o^cruo
Page 1 of 2
292
295 HG Run Log (V4) File Name: V408020G Seq
Cup
Sample ID
Client ID
Sample Type
DF
Date
Time
Results
1:20
1007157-05
MY71T1
SAMPLE
1.0 02 AUG 1 10:26:04
19.7
::2;i
1007157-06
MY71T3
SAMPLE
1.0 02 AUG 1 10:28:18
4.88
[;;'22;.,
CCV2
CCV2
CCV
1.0 02 AUG 1 10:30:08
5.05
'••'23 •
CCB2
CCB2
CCB
1.0 02 AUG 1 10:32:03
-.046
\:^
1007157-08
MY71T7
SAMPLE
1.0 02 AUG 1 10:34:04
4.58
i:j5
1007157-09
MY71T9
SAMPLE
1.0 02 AUG 1 10:35:56
.104
".26
1007157-10
MY71W1
SAMPLE
1.0 02 AUG 1 10:37:49
.792
27
1007157-11
MY71W5
SAMPLE
1.0 02 AUG 1 10:39:41
.016
28
1007157-12
MY71W9
SAMPLE
1.0 02 AUG 1 10:41:35
-.037
:-29
1007157-13
MY71X1
SAMPLE
1.0 02 AUG 1 10:43:50
4.70
•;30
1007157-14
MY71X3
SAMPLE
1.0 02 AUG 1 10:45:56
19.7
^31
1007157-15
MY71X5
SAMPLE
1.0 02 AUG 1 10:48:12
-.033
;::??
1007157-16
MY71X6
SAMPLE
1.0 02 AUG 1 10r50r03
.036
CRL2
CRI
CRI
1.0
02 AUG 1 10r51r54
.242
1M"
CCV3
CCV3
CCV
1.0
02 AUG 1 10:53:48
5.27
;f|5
CCB3
CCB3
CCB
1.0 02 AUG 1 10:55:41
-.058
L::33".-
-
•
-
•
Comments
1 - - - ' • •
Z':
if
i
s -••The presence of the Chemist's/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP has r i. occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the ii .•:.; initials of the lab supervisor and a QA department representative, signifying approval of the deviation.
- •;Reviewed By:
/
Date:
OiOfrt>
Page 2 of 2
293
296
Standard^/QG l?r6|iaration Log for .Analysis Of Gold Vapor Mercuriy COMPUCHEM a division ofLiberty Analytical Corp WPRKSHEETI.NNN _
REF#'
REAGENTS
Sodium Chloride (NaCL)
1m2-188-15
Hydrochloric Acid (HCL)
0G12010
|
0D25009
Stannous Chloride (SnCL2-2H20)
H14614
08/12
Caledon ! JT BAKER ! JT BAK^R
72420
07/15
J07600
04/13
J14618
04/15
PREPARATION INSTRUCTIONS
SnCL,- 08-02-10-NB
i Place in a 1000 mL volumetric flask containing 500 mL of reagent water: 100 g of SnCl2-2H20 Baker Instra-ana yzed or equivalent 250 mL of HCL Baker Instra-analyzedjor equivalent Dilute to 1000 mL with reagent water, i Prepare as needed Place in a 2 L volumetric flask: 1 1000 mL of deionized water 1 200 mL of concentrated HCL Baker Inbtra-analyzed or equivalent Dilute to 2000 mL with reagent water. Prepare as needed
HCL- 08-02-10 - NB Hydrochloric Acid
Place in a 2000 ml volumetric flask: 240.0 g of NH2OH-HCI Baker Instra-analyzed or equivalent 240.0 g NaCl Baker Instra-analyzed or equivalent Dilute to 2000 mL with reagent water. Place solution in a repipetor bottle. Prepare as needed
NH,OH-HCL- 07-30-10 -NB Hydroxylamine hydrochloride
Standard Solutions Prepared By:
EXPIRATION DATE
JTBAKER
STANDARD LOT NUMBER ^
Stannous chloride
CNJ
\)Hu0^^ ^'
LOT#
MANUFACTURER 1
OD13004
Hydroxylamine Hydrochloride (NH2OH-HCL)
iu^5f^-r^ Seq. File Name:
(U^-^^^
M
Entered By:
Date:
Reviewed By:
Date: :
^ l ^ / ^
^Ref# = Logbook ID, Page number, and item number from Materials Receipt Log ^Standard Lot Number consists of standard ID, date prepared, and initials of preparer. The presence of the Chemist's/Analyst's employe J ID number, or signature, on this run log attests that strict compliance with the method's SOP has occun-ed. Any SOP deviations require documenta:ion by the responsible chemist/analyst toget[ier with the chemist's/analyst's initials and the initials of the lab supervisor and a QA department represent tive. signifying approval of the deviation. !
7/24/07: VR
297
Protocol r INSTIDV4
[SSH nAbs.
!^ Calibrated
937G9
:
A1
1^ Accepted
B 1 1.0G548e-4 C 1 -8.34841 e-2 Rhe 1 Accepted
Conc.
s ,01 •
02 03," '04.: 05 •
06 07, 08 09 10
Conc .00000 .20000 .50000 1.0000 5.0000 10.000
Calc -.029 .128 .501 1.02 5.18 9.91
Dev. -.029 -.072 .001 .017 .175 -.093
Mean 513 1984 5489 10328 49357 93769
D a t sr
.999714
02-Aug-10 09:58
10.0
SD or %RSD
d 0% 0% 0% 0% 0%
Rep1 512 1984 5489 10327 49357 93769
Rep 2
Rep 3
Rep 4
Rep 5
yi>i/
5 5.0
C5^v
'-
295
298 y. .y.i.. yi: "
Line
Gone.
Units
Folder: V4 0802 0G Protocol: INSTIDV4 ***POST-RUN REPORT*** SD/RSD 1 2 3
*** Standard: 1 Rep: 1 Sf^
Page 4
5
Seq:
1
09:48:11 02 Aug 10
HG
Seq:
2
09:50:12 02 Aug 10
HG
^^'^-
"^
09:52:04 02 Aug 10
HG
,,
Seq:
4
09:54:29 02 Aug 10
HG
\
Seq:
5
09:56:20 02 Aug 10
HG
Seq:
6
09:58:15 02 Aug 10
HG
*** Check Standard: 3 Ck3 ICV Seq: 7 10:00:18 02 Aug 10 Line Flag %Rcv. Found True Units SD/RSD Hg 104. 4.15 4.00 ppb .000 Tjf> i\Aw *** Check Standard: 1 Ckl I^TCB Seq: 8 10:02:13 02 Aug 10 Line Flag Found Range (-i-/-) Units SD/RSD Hg .032 .200 ppb .000
HG
Hg
.000
ppb
512
*** Standard: 2 Rep: 1 $1),^ Hg
.200
ppb
1984
*** Standard: 3 Rep: 1 50'^ Hg
.500
ppb
*** Standard: 4 Rep: 1 Hg
1.00
ppb
*** Standard: 5 Rep: 1 Hg
5.00
ppb
*** Standard: 6 Rep: 1 Hg
10.0
ppb
5489 C\ ^ 10327 ^'''O 49357 <^\^),o 93769
HG
*** Check Standard: 4 Ck4 CRI Line Flag %Rcv. Found True Hg 88.2 .176 .200
Seq: Units ppb
9
10:04:07 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 99.3 4.97 5.00
Seq: Units ppb
10
10:06:00 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 1 Ckl CCB Seq: 11 Line Flag Found Range (-)-/-) Units SD/RSD Hg -.074 .200 ppb .000
10:07:52 02 Aug 10
HG
*** Sample ID: PBW Hg
-.019
ppb
*** Sample ID: MY71T5 Hg
4.82
ppb
*** Sample ID: MY71T5D Hg
4.75
ppb
*** Sample ID: MY71T5S Hg
5.71
ppb
Seq: 0072822-BLKl .000 -.019
12
10:09:54 02 Aug 10
HG
Seq: 1007157-07 .000 4.82
13
10:11:56 02 Aug 10
HG
Seq: 0072822-DUPl .000 4.75
14
10:14:00 02 Aug 10
HG
Seq: 0072822-MSl .000 5.71
15
10:16:02 02 Aug 10
HG
^96
299
Line
Conc.
Units
*** Sample ID: MY71S3 Hg
.084
ppb
*** Sample ID: MY71S5 Hg
.035
ppb
*** Sample ID: MY71S7 Hg
.276
ppb
*** Sample ID: MY71S9 Hg
.020
ppb
*** Sample ID: MY71T1 Hg
19.7
H ppb
*** Sample ID: MY71T3 Hg
4.88
ppb
Folder: V408020G Protocol: INSTIDV4 ***POST-RUN REPORT*** SD/RSD 1 2 3
4.58
ppb
*** Sample ID: MY71T9 Hg
.104
ppb
*** Sample ID: MY71W1 Hg
.792
ppb
*** Sample ID: MY71W5 Hg
.016
ppb
*** Sample ID: MY71W9 Hg
-.037
ppb
5
16
10:18:12 02 Aug 10
HG
Seq: 1007157-02 .000 .035
17
10:20:18 02 Aug 10
HG
Seq: 1007157-03 .000 .276
18
10:22:18 02 Aug 10
HG
Seq: 1007157-04 .000 .020
19
10:24:11 02 Aug 10
HG
Seq: 1007157-05 .000 19.7
20
10:26:04 02 Aug 10
HG
Seq: 1007157-06 .000 4.88
21
10:28:18 02 Aug 10
HG
10:30:08 02'Aug 10 SD/RSD .000
HG
10:32:03 02 Aug 10
HG
*** Check Standard: 1 Ckl CCB Line Flag Found Range (-f/-) Units Hg -.046 .200 ppb
Hg
4
Seq: 1007157-01 .000 .084
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 101. 5.05 5.00
*** Sample ID: MY71T7
Page
Seq: Units ppb Seq:
22
23 SD/RSD .000
Seq: 1007157-08 .000 4.58
24
10:34:04 02 Aug 10
HG
Seq: 1007157-09 .000 .104
25
10:35:56 02 Aug 10
HG
Seq: 1007157-10 .000 .792
26
10:37:49 02 Aug 10
HG
Seq: 1007157-11 .000 .016
27
10:39:41 02 Aug 10
HG
Seq: 1007157-12 .000 -.037
28
10:41:35 02 Aug 10
HG
297
300
Line
Conc.
Units
*** Sample ID: MY71X1 Hg
4.70
ppb
*** Sample ID: MY71X3 Hg
19.7
H ppb
*** Sample ID: MY71X5 Hg
-.033
ppb
*** Sample ID: MY71X6 Hg
.036
ppb
Folder: V408020G Protocol: INSTIDV4 ***POST-BUN REPORT*** SD/RSD 1 2 3
Page
Seq: 1007157-13 ,000 4.70
29
10:43:50 02 Aug 10
HG
Seq: 1007157-14 .000 19.7
30
10:45:56 02 Aug 10
HG
Seq: 1007157-15 000 -.033
31
10:48:12 02 Aug 10
HG
Seq: 1007157-16 .000 .036
32
10:50:03 02 Aug 10
HG
*** Check Standard: 4 Ck4 CRI Line Flag %Rcv. Found True Hg 121. .242 .200
Seq: Units ppb
33
10:51:54 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 105. 5.27 5.00
Seq: Units ppb
34
10:53:48 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 1 Ckl CCB Line Flag Found Range (-H/-) Units Hg -.058 .200 ppb
Seq:
10:55:41 02 Aug 10
HG
35 SD/RSD .000
298
301 Maintenance: V\ r \ A ^ ^ Method{s) (circle one): ILM04.1 Operator(s): f ^ T ; RR RR#X #X L W s B
\l5\
YLM05.4J) Others
Date/Time
v L L
M ^
to
^|a-l.r>
h^\
Printed: 8/2/2010 5:24:02 PM
Specified elementfs) fail(s) hiqh Specified elementfs) fail(s) low Re-run sample(s) neat Re-run at a #-foId dilution Sample run at a #-fold dilution (aliquot of sample diluted with acidified water) Matrix = leachate Matrix = vvater Matrix = solid Matrix = biological tissue
SDG
Matrix
MY71S3
Water
Batch
Comments
KO-^\^^,Y\t.?^S
0072813
^ ] \ \ K \ ' ^ i ^ S ^ . ^il4
HG Run Log {V4) File Name: V40802OQ |:M.:..
1 Seq"
S a m p l e ID
Cup
C l i e n t ID
Sample Type
DF
Date
!
Time
Results
1
SO
SO
CALIBSTD
1.0
02 AUG 1
16:17:17
-150
2
80.2
80.2
CALIB STD
1.0
02 AUG 1
16:19:07
1673
80.5
80.5
CALIB STD
1.0
02 AUG 1
16:21:01
5596
SI.O
S1.0
CALIB STD
1.0
02 AUG 1
16:22:57
10593
5
85.0
85.0
CALIB STD
1.0
02 AUG 1
16:25:09
53185
6
810.0
810.0
CALIB STD
1.0
02 AUG 1
16:27:03
102334
7
ICVl
ICV
ICV
1.0
02 AUG 1
16:29:04
4.06
8
ICBI
ICB
ICB
1.0
02 AUG 1
16:31:06
-.008
9
CRLI
CRI
CRI
1.0
02 AUG 1
16:32:58
.217
CCVl
CCV1
CCV
1.0
02 AUG 1
16:34:48
5.20
|-1-1-
CCB1
CCBl
CCB
1.0
02 AUG 1
16:36:50
.078
ri2
1007157-17
MY71X8
SAMPLE
1.0
02 AUG 1
16:38:42
.056
1-13
1007157-18
MY71Y0
SAMPLE
1.0
02 AUG 1
16:42:17
.040
1.0
02 AUG 1
16:44:10
.125
1 ^ 1 "^
yy 1 •::>'.; i -
^-'14
..-„,
Comments
1..', 1 •
/nJ^U\vo ^ ^ -eOrzOla-BLKI- ^ })V-.
friJs'^lli
15
CRL2
CRI
CRI
1.0
02 AUG 1
16:46:02
.211
16
CCV2
CCV2
CCV
1.0
02 AUG 1
16:47:56
5.20
--t7
CCB2
CCB2
CCB
1.0
02 AUG 1
16:49:57
.072
[ —
I ., The presence of the Chemist's/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP has ^_^'j&ccurreU_ Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the 'initials of the lab supervisor and a QA department representative, signifying approval of the deviation.
,L.: Reviewed By:
Date: ^
^1)0100
Page 1 of 1
299
302
?sn'tiiv5g;if=StaVid^rdsyQG Preparatloii^^lLo.gilop Analysis of Cold Vapor Mercury Seq. File Name:
r-v, COMPUCHEM a division of Liberty Analytical Corp. WORKSHEET 1 NNN
REAGENTS
REF#^
Sodium Chloride (NaCL) Hydrochloric Acid (HCL) Hydroxylamine Hydrochloride (NH2OH-HCL) Stannous Chloride (SnCL2-2H20) STANDARD L O T NUMBER ^
SnCL,- 08-02-10-NB Stannous chloride HCL-
08-02-10 - NB
Hydrochloric Acid NH,OH-HCL-
07-30-10 - N B
Hydroxylamine hydrochloride
Standard Solutions Prepared By: Entered By:
•liHftVD^Ot^
LOT#
MANUFACTURER
; 0 O CO
EXPIRATION DATE
1m2-188-15
JTBAKER
H14614
08/12
0G12010
Caledon
72420
07/15
ODI3004
JT BAKER
J07600
04/13
0D25009
JT BAKER
J14618
04/15
PREPARATION INSTRUCTIONS
Place in a 1000 mL volumetric flask containing 500 mL of reagent water: 100 g of SnCl2-2H20 Baker Instra-analyzed or equivalent 250 mL of HCL Baker Instra-analyzed or equivalent Dilute to 1000 mL with reagent water. Prepare as needed Place in a 2 L volumetric flask: 1000 mL of deionized water 200 mL of concentrated HCL Baker Instra-analyzed or equivalent Dilute to 2000 mL with reagent water. Prepare as needed Place in a 2000 ml volumetric flask: 240.0 g of NH2OH-HCI Baker Instra-analyzed or equivalent 240.0 g NaCl Baker Instra-analyzed or equivalent Dilute to 2000 mL with reagent water. Place solution in a repipetor bottle. Prepare as needed
MA;^4W—
w^^{W^^^—
Reviewed By:
Date: Date:
%i^ 1 0 ojjeyr^
ier from Materials M< ^Ref# = Logbook ID. Page number, and item number Receipt Log ^Standard Lot Number consists of standard ID, date prepared, and initials of preparer. The presence of the Chemist's/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials of the lab supervisor and a QA department representative, signifying approval of the deviation. 7/24/07: VR
303
Protocol: INSTIDV4
ZJ •' n Abs.
102334
1
A1
r
B 1 9.71887e-5 C 1 -226831 e-2 Rhe 1
Accepted
s
•-•
0405 06.. 07';
Cohfc,!
.ooood .2000C .5000C: 1.000C 5.000C
lo.ooq
Calc -.037 .140 .521 1.01 5.15 9.92
Dev -.037 -.060 .021 .007 .146 -.077
Mean -150 1674 5596 10593 53186 102335
02-Aug-101G:27
10.0
Conc.
01 '02 • 03 •
Date:
.999794
SDor%RSD
0 0% 0% 0% 0% 0%
Rep 1 -150 1673 5596 10593 53185' 1023341
Rep 2
Rep 3
Rep 4
Rep 5
08 10
5Qc5 C s ^ ^ l , < l r^^-^
U4.a7.
301
304
Line
Conc.
Units
*** Standard: 1 Rep: 1 Hg
.000
ppb
*** Standard: 2 Rep: 1 Hg
.200
ppb
*** Standard: 3 Rep: 1 Hg
.500
ppb
*** Standard: 4 Rep: 1 Hg
1.00
ppb
*** Standard: 5 Rep: 1 Hg
5.00
ppb
*** Standard: 6 Rep: 1 Hg
10.0
ppb
Folder: V408020Q Protocol: INSTIDV4 ***POST-RUN REPORT*** SD/RSD 1 2 3 Q/)
,.
Page 4
5
Seq:
1
16:17:17 02 Aug 10
HG
^®^=
^
16:19:07 02 Aug 10
HG
^^'^'-
^
16:21:01 02 Aug 10
HG
Seq:
4
16:22:57 02 Aug 10
HG
^^^'-
^
16:25:09 02 Aug 10
HG
Seq:
6
16:27:03 02 Aug 10
HG
Seq: Units ppb
7
16:29:04 02 Aug 10 SD/RSD .000
HG
-150 ' 50' ^ 1673 S()-^ 5596 fI
'
10593 L,^-^ 53185 ^iO-t) 102334
* * *Check Standard: 3 Ck3 ICV Line Flag %Rcv. Found True Hg 102. 4.06 4.00
*** Check Stajidard: 1 Ckl JZCB Seq: 8 Line Flag Found Range (-1-/-) Units SD/RSD Hg -.008 .200 ppb .000
16:31:06 02 Aug 10
HG
*** Check Standard: 4 Ck4 CRI Line Flag %Rcv. Found True Hg 108. .217 .200
Seq: Units ppb
9
16:32:58 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 104. 5.20 5.00
Seqr Units ppb
10
16:34:48 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 1 Ckl CCB Seq: 11 Line Flag Found Range {-!-/-) Units SD/RSD Hg .078 .200 ppb .000
16:36:50 02 Aug 10
HG
*** Sample ID: MY71X8
Seq: 1007157-17 .000 .056
12
16:38:42 02 Aug 10
HG
Seq: 1007157-18 .000 .040
13
16:42:17 02 Aug 10
HG
*** Sample ID:-PftS ^ifct- 'SUl-^i S e q ^ 14 16:44:10 02 Aug 10 00720-J-^DL!tl- _L O L / ^ I Hg .125 ppb .000 .125 "8l>-//»
HG
*** Check Standard: 4 Ck4 CRI Line Flag %Rcv. Found True Hg 105. .211 .200
HG
Hg
.056
ppb
*** Sample ID: MY71Y0 Hg
.040
ppb
Seq: Units ppb
15
16:46:02 02 Aug 10 SD/RSD .000
302
305
Line
Conc.
Units
Folder: V408020Q Protocol: INSTIDV4 ***POST-RUN REPORT*** SD/RSD 1 2 3
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 104. 5.20 5.00
Seq: Units ppb
16
Page 4
5
16:47:56 02 Aug 10 SD/RSD .000
*** Check Standard: 1 Ckl CCB Seq: 17 Line Flag Found Range (-(-/-) Units SD/RSD Hg .072 .200 ppb .000
16:49:57 02 Aug 10
HG
HG
303
306 Maintenance: Method(s)
(circle one): ILM04.1
Operator(s): J s [ 3 5 _ _ [ | | ^
iTyi^yv-JC
( u M 0 5 ^ Others
Date/Time
^\3-U'> \ ^ ' 3
to
^Ltb
^1->3
Printed:
8/3/2010 9:24:58 AM
Specified elementfs) fail(s) high Specified elementfs) fail(s) low RR COPY Re-run sample(s) neat RR #X Re-run at a #-foId dilution ^ 3 G a * « . DOCUMENTS BCLUOtD IN CSF-W\Vt1|l^3 Sample run at a #-fold dilution (aliquot of sample diluted with acidified water) #X Vlatrix = leachate DATE % \ ^ \ li B3Cf«TURE. Vlatrix = water Matrix = solid Matrix = biological tissue
SDG MY71L3
Matrix Soil
MY71M9
Soil
MY:riN3
Soil
MY71S3
Water
Batch
Comments
i\tas hAys^
0072813
i
0072817 0072819
J^^^^h^t^r^Jj^^C^^
^fv^^\.Wo
HG Run Log (V4) File Name: V408020T Seq
[•Cup
S a m p l e ID
C l i e n t ID
Sample Type
DF
Date
Time
Results
1
80
SO
CALIB STD
1.0
02 AUG 1
18:03:57
29
2
S0.2
S0.2
CALIB STD
t.O
02 AUG 1
18:05:49
2673
3
80.5
80.5
CALIB STD
1.0
02 AUG 1
18:07:39
5394
4
81.0
81.0
CALIB STD
1.0
02 AUG 1
18:10:02
10132
5
85.0
S5.0
CALIBSTD
1.0
02 AUG 1
18:11:58
46932
810.0
810.0
CALIB STD
1.0
02 AUG 1
18:13:59
93741
1CV1
ICV
ICV
1.0
02 AUG 1
18:16:10
4.63
ICBI
ICB
ICB
1.0
02 AUG 1
18:18:10
-.064
CRL1
CRI
CRI
1.0
02 AUG 1
18:20:05
.200
CCVl
CCV1
CCV
1.0
02 AUG 1
18:21:59
5.05
CCBl
CCB1
CCB
1.0
02 AUG 1
18:23:59
-.019
12
0072813-BLKl
PBS
BLANK
1.0
02 AUG 1
18:25:50
-.022
13
0072813-BSl
LCSS
LCS
1.0
02 AUG 1
18:27:44
8.13
1007154-09
MY71M1
SAMPLE
1.0
02 AUG 1
18:29:38
100
-15
0072813-DUP1
MY71M1D
DUPLICATE
1.0
02 AUG 1
18:32:03
112
-16
0072813-MSl
MY71M18
MATRIXSPIKE
1.0
02 AUG 1
18:34:19
107
1007154-01
MY71L3
SAMPLE
1.0
02 AUG 1
18:36:45
.372
6
••
py
.
•
•,?'""^''".'...-
:
•
'<
".••
89
•
.•
V
,...\Q 1
:•<>.
I -11
.
-14
yI j 1
Comments
:
•
•
—
:
-
t^^aox 9.9. MH.
ut%^
TFe'presence of Ihe Chemist's/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP has Occurred; Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials ofthe lab supervisor and a QA department representative, signifying approval of the deviation.
TReviewed By:
t
Date:'
0^<^5^
Page 1 of 4
304
307 ^
HG Run Log (V4) iFlleName: V408020T Cup
;-§eq
Sample ID
Client ID
Sample Type
DF
Date
Time
Results
Comments
18
1007154-02
MY71L4
SAMPLE
1.0
02 AUG 1
18r38r37
.080
•- ^ 9
1007154-03
MY71L5
SAMPLE
20
02 AUG 1
18:40:32
20.0
^?- \00)t
1 • 20
1007154-04
MY71L6
SAMPLE
20
02 AUG 1
18:42:38
14.5
^t^)C
: ?6
IBL
IBL
SAMPLE
1.0
02 AUG 1
18:44:28
-.185
ZZ2
CCV2
CCV2
CCV
1.0
02 AUG 1
18:46:29
5.06
CCB2
CCB2
CCB
1.0
02 AUG 1
18:48:30
.042
1007154-05
MY71L7
SAMPLE
20
02 AUG 1
18:50:20
46.6
^^ \m
..-25
1007154-06
MY71L8
SAMPLE
1.0
02 AUG 1
18:52:26
80.5
(1.^5^)C
.-26
1007154-07
MY71L9
SAMPLE
1.0
02 AUG 1
18:54:36
7.93
AZJ
1007154-08
MY71M0
SAMPLE
1.0
02 AUG 1
18:56:26
139
ikk^b^
^v28
1007154-10
MY71M2
SAMPLE
1.0
02 AUG 1
18:58:57
56.8
t^(^;w»^
29
1007154-11
MY71M3
SAMPLE
1.0
02 AUG 1
19:01:01
69.6
?v^ z ^ r
--30
IBL
IBL
SAMPLE
1.0
02 AUG 1
19:03:08
-.373
r--:31
1007154-12
MY71M4
SAMPLE
1.0
02 AUG 1
19:05:02
.371
P32
CRL2
CRI
CRI
1.0
02 AUG 1
19:06:56
.210
CCV3
CCV3
CCV
1.0
02 AUG 1
19:08:58
5.27
pg^-r^v ..'.'•:r-.".. CCB3
CCB3
CCB
1.0
02 AUG 1
19:11:01
-.051
-. :,-.;.,::. 1007154-13
MY71M5
SAMPLE
1.0
02 AUG 1
19:12:54
9.67
1007154-14
MY71M6
SAMPLE
1.0
02 AUG 1
19:14:48
11.6
1007154-15
MY71M7
SAMPLE
1.0
02 AUG 1
19:16:51
32.4
d^ m
i-fs, •
1007154-16
MY71M8
SAMPLE
1.0
02 AUG 1
19:19:02
15.9
^IL3A
-39
1007154-17
MY71N0
SAMPLE
1.0
02 AUG 1
19:20:56
41.3
P.P. v(^
40
1007154-18
MY71N1
SAMPLE
1.0
02 AUG 1
19:23:01
11.7
\^^
- ^
1007154-19
MY71N2
SAMPLE
1.0
02 AUG 1
19:25:02
11.8
:-42
0072817-BLKl
PBS
BLANK
1.0
02 AUG 1
19:26:55
-.091
k-^-S
0072817-BSl
LCSS
LCS
1.0
02 AUG 1
19:28:48
9.89
CCV4
CCV4
CCV
1.0
02 AUG 1
19:30:41
5.29
-,..._,: CCB4
CCB4
CCB
1.0
02 AUG 1
19:32:34
-.049
1007155-01
MY71M9
SAMPLE
1.0
02 AUG 1
19:34:35
83.5
Ufl M
0072817-DUPl
MY71M9D
DUPLICATE
1.0
02 AUG 1
19:36:50
86.8
KfSa^)>
0072817-MSl
MY71M9S
MATRIX SPIKE
1.0
02 AUG 1
19:39:03
91.7
ilP- 9-bf
•
y 1L...-A:
•
-.24.
r —^fir'-
~y -36 -37
•'
• ' ' ' - :
^L;^yc
SL^
fvii. Q2f
..^^i^
f : ^ . .
•r
Nfl 1
' • • • - - • : ; • '
-•••.r'
-47 •
• • - . ; "
V7. •
_..
The presence of the Chemist's/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's inilials and the initials of the lab supervisor and a QA department representative, signifying approval of the deviation.
.: Reviewed By:
ZLy
Date:
O^&ffP
Page 2 of 4
305
308 H G R u n L o g (V4) File N a m e :
Client ID
Sample ID
Cup
-§)Bq
V408020T
Sample Type
DF
Date
Time
Results
Comments
ii49
1007155-02
MY71Q3
SAMPLE
1.0
02 AUG 1
19:41:14
2.25
ii-.-.m
1007155-03
MY71Q4
SAMPLE
1.0
02 AUG 1
19:43:15
2.03
..^hr
1007155-04
MY71Q5
SAMPLE
1.0
02 AUG 1
19:45:08
2.13
1007155-05
MY71Q6
SAMPLE
1.0
02 AUG 1
19:47:01
.067
1007155-06
MY71Q7
SAMPLE
1.0
02 AUG 1
19:48:52
2.20
CRL3
CRI
CRI
1.0
02 AUG 1
19:50:44
.220
55
CCV5
CCV5
CCV
1.0
02 AUG 1
19:52:34
5.43
56
CCB5
CCB5
CCB
1.0
02 AUG 1
19:54:35
-.010
:•. 57
1007155-07
MY71Q9
SAMPLE
1.0
02 AUG 1
19:56:47
20.0
P.aS)C
::-,.58
1007155-08
MY71R0
SAMPLE
1.0
02 AUG 1
19:58:44
10.6
^ ^ ^
1007155-09
MY71R1
SAMPLE
1.0
02 AUG 1
20:00:46
2.82
1007155-10
MY71R2
SAMPLE
1.0
02 AUG 1
20:02:39
.099
m^y':- • ••v~.,-,-
1007155-11
MY71R3
SAMPLE
1.0
02 AUG 1
20:04:31
11.7
l-.zQ2.y
1007157-05
MY71T1
SAMPLE
3
02 AUG 1
20:06:23
7.06
1007157-14
MY71X3
SAMPLE
3
02 AUG 1
20:08:24
6.70
0072819-BLKl
PBS
BLANK
1.0
02 AUG 1
20:10:19
-.008
yp
0072819-BSl
LCSS
LCS
1.0
02 AUG 1
20:12:20
6.42
•' 66
1007156-17
MY71P9
SAMPLE
1.0
02 AUG 1
20:14:37
3.40
CCV6
CCV6
CCV
1.0
02 AUG 1
20:16:32
5.51
CCB6
CCB6
CCB
1.0
02 AUG 1
20:18:32
-.022
0072819-DUPl
MY71P9D
DUPLICATE
1.0
02 AUG 1
20:20:42
2.56
0072819-MSl
MY71P98
MATRIX SPIKE
1.0
02 AUG 1
20:22:47
3.05
1007156-01
MY71N3
SAMPLE
1.0
02 AUG 1
20:24:44
73.1
1007156-02
MY71N4
SAMPLE
1.0
02 AUG 1
20:26:51
-.135
1007156-03
MY71N5
SAMPLE
1.0
02 AUG 1
20:28:44
22.7
1007156-04
MY71N6
SAMPLE
1.0
02 AUG 1
20:30:48
3.52
1007156-05
MY71N7
SAMPLE
1.0
02 AUG 1
20:32:50
.161
1007156-06
MY71N8
SAMPLE
1.0
02 AUG 1
20:34:44
12.6
77
CRL4
CRI
CRI
1.0
02 AUG 1
20:36:39
.151
-:78
CCV7
CCV7
CCV
1.0
02 AUG 1
20:38:40
5.43
CCB7
CCB7
CCB
1.0
02 AUG 1
20:40:42
.003
\^..^.1
i::M
^ 4 :
-
1 - - ^
>
1
• •
:••.,.^v-.
t^^
-
Zm y"^'\
67 -68 r':y .
•m
,„,::,,,
•t-ry- .
y:y. r^r.1 \^•'^.Tt::-.•':
.-•
•r-ii-r
^4
r-76
y r
^s^-m
m "¥ Hd y^
•.•; „ ' , • »
t-feV -,^!fThe presence of the Chemist's/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP has ^ypcciimeci. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the yjr^nitials of the lab supervisor anda QA department representative, signifying approval of the deviation. ..-a^^eyiewed By:
/
r^atoDate:
^ <'uG'^Cb I/-A/'A O
P d / i o3 ^ nof f /4 i Page
oOo
309 H G R u n L o g {V4) :;g|:^« '^File N a m e : Seq
Cup
V408020T
S a m p l e ID
C l i e n t ID
Sample Type
DF
Date
Time
Results
1007156-07
MY71N9
SAMPLE
1.0
02 AUG 1 20:42:33
3.36
1007156-08
MY71P0
SAMPLE
1.0
02 AUG 1
20:44:26
10.2
im
1007156-09
MY71P1
SAMPLE
1.0
02 AUG 1
20:46:23
5.37
83
1007156-10
MY71P2
SAMPLE
1.0
02 AUG 1 20:48:24
.135
,84
1007156-11
MY71P3
SAMPLE
1.0
02 AUG 1 20:50:18
28,3
r-§5
1007156-12
MY71P4
SAMPLE
1.0
02 AUG 1 20:52:12
2.58
^1
1007156-13
MY71P5
SAMPLE
1.0
02 AUG 1 20:54:07
1.18
f!rS?
1007156-14
MY71P6
SAMPLE
1.0
02 AUG 1
20:56:10
.797
o*WU
1.0
02 AUG 1
20:58:03
.289
if
•
rfSI.
Comments
?.(La'/
•'"•ii-r
-§.§
, . . . ' • • .
j i f i ^ % y CCV8
CCV8
CCV
1.0
02 AUG 1
21:00:06
5.60
-go
CCB8
CCB8
CCB
1.0
02 AUG 1
21:01:58
-.092
trjl-
1007156-15
MY71P7
SAMPLE
1.0
02 AUG 1
21:03:51
11.4
-im
1007156-16
MY71P8
SAMPLE
1.0
02 AUG 1 21:05:45
4.68
'i 93
1007156-18
MY71Q0
SAMPLE
1.0
02 AUG 1 21:07:40
2.98
'. 94
1007156-19
MY71Q1
SAMPLE
1.0
02 AUG 1 21:09:31
2.14
1=^95
1007156-20
MY71Q2
SAMPLE
1.0
02 AUG 1
21:11:24
4.54
1007154-09
MY71M1
SAMPLE
20
02 AUG 1
21:13:17
7.19
0072813-DUP1
MY71M1D
DUPLICATE
20
02 AUG 1
21:15:11
8.36
0072813-M81
MY71M1S
MATRIX SPIKE
20
02 AUG 1 21:17.05
4.31
CRL6
CRI
CRI
1.0
02 AUG 1
21:19:10
.192
CCV9
CCV9
CCV
1.0
02 AUG 1
21:21:12
5.40
CCB9
CCB9
CCB
1.0
02 AUG 1
21:23:01
-.023
. ,j,.:...
iULS)^
^c.^
1 ri:'.J.'r
fiW
rm:0^y
H|.::
r-yr-
|'-">if:
- j j j h e presence of the Chemist's/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP has L.^^pccurred. /\ny SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's inilials and the ,.,.f;initials of.the lab supervisor and a QA department representative, signifying approval of the deviafion.
7/ Reviewed By:
Date: -
^
>yx/?/^
Page 4 of 4
307
310 00
o
Standards/QC tRr^;0^ratiQn Log for Analysis of Gold Vapor Mercury COMPUCHEM a division ofLiberty Analytical Corp. WORKSHEET 1 l^JWf
REF#^
REAGENTS
Sodium Chloride (NaCL) Hydrochloric Acid (HCL) Hydroxylamine Hydrochloride (NH2OH-HCL) Stannous Chloride (SnCL2-2H20) STANDARD LOT NUMBER ^
\|Hb^^^ ^^
LOT#
MANUFACTURER
EXPIRATION DATE
1m2-188-15
JTBAKER
H14614
08/12
0G12010
Caledon
72420
07/15
ODI3004
JT BAKER
J07600
04/13
0D25009
JT BAKER
J14618
04/15
PREPARATION INSTRUCTIONS
Place in a 1000 mL volumetric flask containing 500 mL of reagent water: 100 g of SnCl2-2H20 Baker Instra-analyzed or equivalent 250 mL of HCL Baker Instra-analyzed or equivalent Dilute to 1000 mL with reagent water. Prepare as needed
SnCL,- 08-02-10-NB Stannous chloride
Place in a 2 L volumetric flask: 1000 mL of deionized water 200 m l of concentrated HCL Baker Instra-analyzed or equivalent Dilute to 2000 mL with reagent water. Prepare as needed
HCL- 08-02-10 - NB Hydrochloric Acid
Place in a 2000 ml volumetric flask: 240.0 g of NH2OH-HCI Baker Instra-analyzed or equivalent 240.0 g NaCl Baker Instra-analyzed or equivalent Dilute to 2000 mL with reagent water. Place solution in a repipetor bottle. Prepare as needed
NH,OH-HCL- 07-30-10 -NB Hydroxylamine hydrochloride
Standard Solutions Prepared By:
CO
Seq. File Name:
{W:^
Entered By: Reviewed By:
- ^
llll.
^ ^ ^ A
^Ref# = Logbook ID, Page number, and item number from Materials Receipt Log ^Standard Lot Number consists of standard ID, date prepared, and initials of preparer. The presence of the Chemist's/Analyst's employee ID number, or signature, on this run log attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials of the lab supervisor and a QA department representative, signifying approval of the deviation. 7/24/07: VR
311
Protocol: INSTIDV4
^'\yno<^tAM p~~3
4-«* St;*
.
fr,"'.
nAbs ^-u".
.r r
93741
B j 1.07383e-4 C I -G.05481e-2 ! Accepted
Conc.
Rhe I Date:
.9999B5
02-Aug-10 18:14
10.0
f TC '-«.'
s ^ 02'^ 03:;; • 04,05 06 07 08 09 ; 10
Conc .00000 .20000 .50000 1.0000 5.000C 10.00C
Calc -.057 .226 .519 1.03 4.98 10.0
Dev -.057 .026 .019 .027 -.021 .006
Mean 30 2673 5395 10132 46933 93742
SD or %RSD 0 0% 0% 0% 0% 0%
Rep 1 29 2673 5394 10132 46932 93741
Rep 2
Rep 3
Rep 4
Rep 5
00
s> l o o Clo-&/|t>0 (X\\
S\o^^s
•''^^ aM. i>);4K,^ I s 7 ,
8-^ -Vv^ ^^^^^^
309
312
\y. ^y 'y/y : I" %
: '
H
Line
Conc.
Folder: V408020T Protocol: INSTIDV4 ***POST-RUN REPORT*** SD/RSD 1 2 3
Units
*** standard: 1 Rep: 1
\
Hg
5
Seq:
1
18:03:57 02 Aug 10
HG
Seq:
2
18:05:49 02 Aug 10
HG
Seq:
3
18:07:39 02 Aug 10
HG
Seq:
4
18:10:02 02 Aug 10
HG
^^^'-
^
18:11:58 02 Aug 10
HG
6
18:13:59 02 Aug 10
HG
**•" Check Standard: 3 Ck3 ICV Seq: 7 18:16:10 02 Aug 10 Line Flag %Rcv. Found True Units SD/RSD Hg 116. 4.63 4.00 ppb .0 00 *** Check Standard: 1 Ckl 0 0 ^ ^ seq: 8 18:18:10 02 Aug 10 Line Flag Found Range (-f/-) Units SD/RSD
HG
.000
ppb
^^ 29 ^(y
*** standard: 2 Repr 1 fi
Hg ***
.200
ppb
yy.
tig
.500
^
2673 ^Q^y
Standard: 3 Rep: 1 ppb
5394
*** Standard: 4 Rep: 1 -
4
•• -
^
.!•
Page
C
O |^
VTN
-::,•:
Hg
1.00
ppb
10132
ZZ
/-rD
^
yp
0
l^y
*** standard: 5 Rep: 1
|::--^: f; f
Hg 5.00 ppb 4 6932 *** Standard: 6 Rep: 1 ^ i ^ ' Hg 10.0 ppb 93741
I" y
^
\A Seq: ^
I t~..r. f ;,•; y/::ErZ I ?,r; I?-E':-', 'f-
Hg
-.0 64
.200
ppb
HG
.00 0
.; ,:•.•
•I
:
'^
r„::;:::v.r l---y. y.i2/
*** Check Standard: 4 Ck4 CRI Line Flag %Rcv. Found True Hg 100. .200 .200
Seq: Units ppb
9
18:20:05 02 Aug 10 SD/RSD .000
HG
yy y/.|..-v.:,:.
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 101. 5.05 5.00
Seq: Units ppb
10
18:21:59 02 Aug 10 SD/RSD .000
HG
|;
*** Check Standard: 1 Ckl CCB Line Flag Found Range (-<-/-) Units Hg -.019 .200 ppb
Seq:
11 SD/RSD .000
18:23:59 02 Aug 10
HG
j t
ly-2 I ;. y^ ; ij!. /yI "% 't:yi
l^--y
*** Sample ID: PBS Hg
ppb
*** Sample ID: LCSS • Hg
8.13
ppb
*** Sample ID: MY71M1 Hg
(C.
-.022
100.
H ppb
Seq: 0072813-BLKl .000 -.022
12
18:25:50 02 Aug 10
HG
Seq: 0072813-BSl .000 8.13
13
18:27:44 02 Aug 10
HG
Seq: 1007154-09 .000 100.
14
18:29:38 02 Aug 10
HG
Seq: 0072813-DUPl .000 112.
15
18:32:03 02 Aug 10
HG
-.
*** Sample ID: MY71M1D Hg
112.
H ppb
=310
313
Line
Conc.
Units
*** Sample ID: MY71M1S Hg
107.
H ppb
*** Sample ID: MY71L3 Hg
.372
ppb
*** Sample ID: MY71L4 Hg
.080
ppb
*** Sample ID: MY71L5 Hg
20.0
H ppb
*** Sample ID: MY71L6 Hg
14.5
H ppb
Folder: V408020T Protocol: INSTIDV4 ***POST-RUN REPORT*** SD/RSD 1 2 3
-.185
ppb
4
16
18:34:19 02 Aug 10
HG
Seq: 1007154-01 .000 .372
17
18:36:45 02 Aug 10
HG
Seq: 1007154-02 .000 .080
18
18:38:37 02 Aug 10
HG
Seq: 19 1007154-03 20X .000 20.0
18:40:32 02 Aug 10
HG
Seq: 20 1007154-04 20X .000 14.5
18:42:38 02 Aug 10
HG
18:44:28 02 Aug 10
HG
18:46:29 02 Aug 10 SD/RSD .000
HG
Seq: IBL .000
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 101. 5.06 5.00
21
-.185 Seq: Units ppb
22
*** Check Standard: 1 Ckl CCB Seq: 23 Line Flag Found Range (-i-/-) Units SD/RSD Hg .042 .200 ppb .000
18:48:30 02 Aug 10
HG
*** Sample ID: MY71L7
Seq: 24 1007154-05 20X .000 46.6
18:50:20 02 Aug 10
HG
Seq: 1007154-06 .000 80.5
25
18:52:26 02 Aug 10
HG
Seq: 1007154-07 .000 7.93
26
18:54:36 02 Aug 10
HG
Seq: 1007154-08 .000 139.
27
18:56:26 02 Aug 10
HG
Seq: 1007154-10 .000 56.8
28
18:58:57 02 Aug 10
HG
Hg
46.6
H ppb
*** Sample ID: MY71L8 Hg
80.5
H ppb
*** Sample ID: MY71L9 Hg
7.93
ppb
*** Sample ID: MY71M0 Hg
139.
H ppb
*** Sample ID: MY71M2 Hg
56.8
H ppb
2
5
Seq: 0072813-MSl .000 107.
*** Sample ID: IBL Hg
Page
311
314
Line
Conc.
Units
*** Sample ID: MY71M3 Hg
69.6
H ppb
Folder: V408020T Protocol: INSTIDV4 ***POST-RUN REPORT*** SD/RSD 1 2 3
-.373
ppb
*** Sample ID: MY71M4 Hg
.371
ppb
4
29
19:01:01 02 Aug 10
HG
Seq:
30
19:03:08 02 Aug 10
HG
31
19:05:02 02 Aug 10
HG
IBL .000
-.373
Seq: 1007154-12 .000 .371
*** Check Standard: 4 Ck4 CRI Line Flag %Rcv. Found True Hg 105. .210 .200
Seq: Units ppb
32
19:06:56 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 105. 5.27 5.00
Seq: Units ppb
33
19:08:58 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 1 Ckl CCB Line Flag Found Range (-f-/-) Units Hg -.051 .200 ppb
Seq:
34 SD/RSD .000
19:11:01 02 Aug 10
HG
*** Sample ID: MY71M5 Hg
9.67
ppb
*** Sample ID: MY71M6 Hg
11.6
H ppb
*** Sample ID: MY71M7 Hg
32.4
H ppb
*** Saraple ID: MY71M8 Hg
15.9
H ppb
*** Sample ID: MY71N0 Hg
41.3
H ppb
*** Sample ID: MY71N1 Hg
11.7
H ppb
*** Saraple ID: MY71N2 Hg
11.8
H ppb
3
5
Seq: 1007154-11 .000 69.6
*** Sample ID: IBL Hg
Page
Seq: 1007154-13 .000 9.67
35
19:12:54 02 Aug 10
HG
Seq: 1007154-14 .000 11.6
36
19:14:48 02 Aug 10
HG
Seq: 1007154-15 .000 32.4
37
19:16:51 02 Aug 10
HG
Seq: 1007154-16 .000 15.9
38
19:19:02 02 Aug 10
HG
Seq: 1007154-17 .000 41.3
39
19:20:56 02 Aug 10
HG
Seq: 1007154-18 .000 11.7
40
19:23:01 02 Aug 10
HG
Seq: 1007154-19 .000 11.8
41
19:25:02 02 Aug 10
HG
312
315
Line
Conc.
Units
*** Saraple ID: PBS Hg
-.091
ppb
*** Sample IDr LCSS Hg
9.89
ppb
Folder: V408020T Protocol: INSTIDV4 ***POST-RUN REPORT*** SD/RSD 1 2 3
19:26:55 02 Aug 10
HG
Seq: 0072817-BSl .000 9.89
43
19:28:48 02 Aug 10
HG
19:30:41 02 Aug 10 SD/RSD .000
HG
19:32:34 02 Aug 10
HG
*** Check Standard: 1 Ckl CCB Line Flag Found Range (-)-/-) Units Hg -.049 .200 ppb
Seq:
83.5
H ppb
*** Sample ID: MY71M9D Hg
86.8
H ppb
*** Sample ID: MY71M9S Hg
91.7
H ppb
*** Sample ID: MY71Q3 Hg
2.25
ppb
*** Sample ID: MY71Q4 Hg
2.03
ppb
*** Sample ID: MY71Q5 Hg
2.13
ppb
*** Sample ID: MY71Q6 Hg
.067
ppb
*** Sample ID: MY71Q7 Hg
2.20
ppb
44
45 SD/RSD .000
4
5
42
Seq: Units ppb
Hg
4
Seq: 0072817-BLKl .000 -.091
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 106. 5.29 5.00
*** Sample ID: MY71M9
Page
Seq: 1007155-01 .000 83.5
46
19:34:35 02 Aug 10
HG
Seq: 0072817-DUPl .000 86.8
47
19:36:50 02 Aug 10
HG
Seq: 0072817-MSl .000 91.7
48
19:39:03 02 Aug 10
HG
Seq: 1007155-02 .000 2.25
49
19:41:14 02 Aug 10
HG
Seq: 1007155-03 .000 2.03
50
19:43:15 02 Aug 10
HG
Seq: 1007155-04 .000 2.13
51
19:45:08 02 Aug 10
HG
Seq: 1007155-05 .000 .067
52
19:47:01 02 Aug 10
HG
Seq: 1007155-06 .000 2.20
53
19:48:52 02 Aug 10
HG
*** Check Standard: 4 Ck4 CRI Line Flag %Rcv. Found True Hg 110. .220 .200
Seq: Units ppb
54
19:50:44 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 109. 5.43 5.00
Seq: Units ppb
55
19:52:34 02 Aug 10 SD/RSD .000
HG 313
316
Line
Conc.
Units
Folder: V408020T Protocol: INSTIDV4 ***POST-RUN REPORT*** SD/RSD 1 2 3
*** Check Standard: 1 Ckl CCB Line Flag Found Range (-f/-) Units Hg -.010 .200 ppb *** Sample ID: MY71Q9 Hg
20.0
H ppb
*** Sample ID: MY71R0 Hg
10.6
H ppb
*** Sample ID: MY71R1 Hg
2.82
ppb
*** Sample ID: MY71R2 Hg
.099
ppb
*** Sample ID: MY71R3 Hg
11.7
H ppb
*** Sample ID: MY71T1 Hg
7.06
ppb
*** Sample ID: MY71X3 Hg
6.70
ppb
*** Sample ID: PBS Hg
-.008
ppb
*** Sample ID: LCSS Hg
6.42
ppb
*** Sample ID: MY71P9 Hg
3.40
ppb
Seq:
56 SD/RSD .000
Page 4
5
19:54:35 02 Aug 10
HG
Seq: 1007155-07 .000 20.0
57
19:56:47 02 Aug 10
HG
Seq: 1007155-08 .000 10.6
58
19:58:44 02 Aug 10
HG
Seq: 1007155-09 .000 2.82
59
20:00:46 02 Aug 10
HG
Seq: 1007155-10 .000 .099
60
20:02:39 02 Aug 10
HG
Seq: 1007155-11 .000 11.7
61
20:04:31 02 Aug 10
HG
Seq: 1007157-05 3X .000 7.06
62
20:06:23 02 Aug 10
HG
Seq: 1007157-14 3X .000 6.70
63
20:08:24 02 Aug 10
HG
Seq: 0072819-BLKl .000 -.008
64
20:10:19 02 Aug 10
HG
Seq: 0072819-BSl .000 6.42
65
20:12:20 02 Aug 10
HG
Seq: 1007156-17 .000 3.40
66
20:14:37 02 Aug 10
HG
20:16:32 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 110. 5.51 5.00
Seq: Units ppb
67
*** Check Standard: 1 Ckl CCB Seq: 68 Line Flag Found Range (-*-/-) Units SD/RSD Hg -.022 .200 ppb .000
20:18:32 02 Aug 10
5
HG
314
317
Line
Conc.
Units
*** Sample ID: MY71P9D Hg
2.56
ppb
*** Sample ID: MY71P9S Hg
3.05
ppb
*** Sample ID: MY71N3 Hg
73.1
H ppb
*** Sample ID: MY71N4 Hg
-.135
ppb
*** Sample ID: MY71N5 Hg
22.7
H ppb
*** Sample ID: MY71N6 Hg
3.52
ppb
*** Sample ID: MY71N7 Hg
.161
ppb
*** Sample ID: MY71N8 Hg
12.6
H ppb
Folder: V408020T Protocol: INSTIDV4 ***POST-RUN REPORT*** SD/RSD 1 2 3
Page 4
5
Seq: 0072819-DUPl .000 2.56
69
20:20:42 02 Aug 10
HG
Seq: 0072819-MSl .000 3.05
70
20:22:47 02 Aug 10
HG
Seq: 1007156-01 .000 73.1
71
20:24:44 02 Aug 10
HG
Seq: 1007156-02 .000 -.135
72
20:26:51 02 Aug 10
HG
Seq: 1007156-03 .000 22.7
73
20:28:44 02 Aug 10
HG
Seq: 1007156-04 .000 3.52
74
20:30:48 02 Aug 10
HG
Seq: 1007156-05 .000 .161
75
20:32:50 02 Aug 10
HG
Seq: 1007156-06 .000 12.6
76
20:34:44 02 Aug 10
HG
*** Check Standard: 4 Ck4 CRI Line Flag %Rcv. Found True Hg 75.6 .151 .200
Seq: Units ppb
77
20:36:39 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 109. 5.43 5.00
Seq: Units ppb
78
20:38:40 02 Aug 10 SD/RSD .000
HG
20:40:42 02 Aug 10
HG
*** Check Standard: 1 Ckl CCB Line Flag Found Range (-H/-) Units Hg .003 .200 ppb *** Sample ID: MY71N9 Hg
3.36
ppb
*** Sample ID: MY71P0 Hg
10.2
H ppb
Seq: 79 SD/RSD .000
6
Seq: 1007156-07 .000 3.36
80
20:42:33 02 Aug 10
HG
Seq: 1007156-08 .000 10.2
81
20:44:26 02 Aug 10
HG
315
318
Line
Conc.
Units
*** Sample ID: MY71P1 Hg
5.37
ppb
*** Sample ID: MY71P2 Hg
.135
ppb
*** Sample ID: MY71P3 Hg
28.3
H ppb
*** Sample ID: MY71P4 Hg
2.58
ppb
*** Sample ID: MY71P5 Hg
1.18
ppb
*** Sample ID: MY71P6 Hg
.797
ppb
Folder: V408020T Protocol: INSTIDV4 ***POST-RUN REPORT*** SD/RSD 1 2 3
Page 4
5
.
Seq: 1007156-09 .000 5.37
82
20:46:23 02 Aug 10
HG
Seq: 1007156-10 .000 .135
83
20:48:24 02 Aug 10
HG
Seq: 1007156-11 .000 28.3
84
20:50:18 02 Aug 10
HG
Seq: 1007156-12 .000 2.58
85
20:52:12 02 Aug 10
HG
Seq: 1007156-13 .000 1.18
86
20:54:07 02 Aug 10
HG
Seq: 1007156-14 .000 .797
87
20:56:10 02 Aug 10
HG
*** Check Standard: 4 Ck4 'Cftt/^ Line Flag %Rcv. Found True Hg H 144. .289 .200
Seq: Units ppb
88
20:58:03 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 112. 5.60 5.00
Seq: Units ppb
89
21:00:06 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 1 Ckl CCB Line Flag Found Range (-t-/-) Units Hg -.092 .200 ppb
Seq:
90 SD/RSD .000
21:01:58 02 Aug 10
HG
*** Sample ID: MY71P7 Hg
11.4
H ppb
*** Sample ID: MY71P8 Hg
4.68
ppb
*** Sample ID: MY71Q0 Hg
2.98
ppb
*** Sample ID: MY71Q1 Hg
2.14
ppb
7
Seq: 1007156-15 .000 11.4
91
21:03:51 02 Aug 10
HG
Seq: 1007156-16 .000 4.68
92
21:05:45 02 Aug 10
HG
Seq: 1007156-18 .000 2.98
93
21:07:40 02 Aug 10
HG
Seq: 1007156-19 .000 2.14
94
21:09:31 02 Aug 10
HG
316
319
Line
Conc.
Units
*** Sample ID: MY71Q2 Hg
4.54
ppb
*** Sample ID: MY71M1 Hg
7.19
ppb
*** Sample ID: MY71M1D Hg
8.36
ppb
*** Sample ID: MY71M1S Hg
4.31
ppb
Folder: V408020T Protocol: INSTIDV4 ***POST-RUN REPORT*** SD/RSD 1 2 3 Seq: 1007156-20 .000 4.54
Page 4
5
95
21:11:24 02 Aug 10
HG
Seq: 96 1007154-09 20X .000 7.19
21:13:17 02 Aug 10
HG
Seq: 97 0072813-DUPl 20X .000 8.36
21:15:11 02 Aug 10
HG
Seq: 98 0072813-MSl 20X .000 4.31
21:17:06 02 Aug 10
HG
*** Check Standard: 4 Ck4 CRI Line Flag %Rcv. Found True Hg 96.1 .192 .200
Seq: Units ppb
99
21:19:10 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 2 Ck2 CCV Line Flag %Rcv. Found True Hg 108. 5.40 5.00
Seq: Units ppb
100
21:21:12 02 Aug 10 SD/RSD .000
HG
*** Check Standard: 1 Ckl CCB Line Flag Found Range (-)-/-) Units Hg . -.023 .200 ppb
Seq:
21:23:01 02 Aug 10
HG
101 SD/RSD .000
8
317
320
4. Digestion and Distillation Logs The following logs shall be submitted, as appropriate, for each preparation procedure: digestion logs for ICP-AES, ICP-MS, mercury preparations, and cyanide. The logs shall include: (1) date; (2) sample weights and volumes, with initial sample weight/volume and final volume clearly indicated; (3) sufficient information to unequivocally identify which QC samples (i.e., LCS, PB) correspond to each batch digested; (4) comments describing any significant sample changes or reactions which occur during preparation shall be entered in the log and noted in the SDG Narrative; (5) indication of pH less than 2 or greater than 12, as applicable; (6) identification of the sample preparer(s) [signature (s)].
318
321
METALS/MERCURY PREPARATION LOG
O^ T—
Metals Method
ILM05.4 / H W I
Mercury Method
lLMq5.4 / C W I
i o m p u i fhem
Preparation Time: A DiviooaOf
Prepared By:
COMPUCHEM SAMPLE ID
SAMPLE TYPE
CLIENT SAMPLE ID
0072821/22-BLK1
PBW
0072821-BSl
LCSW
0072B21/22-DUP1
MY71T5D
0O72821/22-MS1
MY71T5S
1007157-01
MY71S3
1007157-02
MY71S5
1007157-03
MY71S7
SAMPLE
MY71S9
SAMPLE
LCS
MY71T1
1007157-06
MY71T3
yy
ICP Final
SO
SAMPLE
SAMPLE SAMPLE SAMPLE
SAMPLE
1007157-09 1007157-10
MY71W1
SAMPLE
1007157-11
MY71W5
SAMPLE
1007157-12
MY71W9
SAMPLE
1007157-13
MY71X1
SAMPLE SAMPLE
HG
*Description
'Description
Final
Berore
After
S'O •ge>
j ^ e
(Qg
-SSL yo
A50_ VCO
_£»_ -gg
ICO
_cs_
ct
j r s
.SSL_££ /
cc
JJ_
Cf...
(y
_Cfl^
«rC
cr
uso V<^o
J P
Loa \e.o
-.ro
voe
.ya
SAMPLE
Sc.
MY71X6
SAMPLE
SO
MY71X8
SAMPLE
go
MY71Y0 .•t'.virj.'/jfi?; ir:
^^iM//2^y& 5S;te9as^j^iJi*jas;^ s^i&iS ^ i i ^
iw#^^^^
cL c*-
CJC
JSul
Jck.
<-:i gL
Cj^
<-A CA
cU
<-A
c<^
t,.a
CS
I
<-s
-Ct-
-4fiO-
(Qg
cr
d<-
-^sd
/
cr -Ol rx
ec
cy ^aagEsSte;^
i J
-££-
Cl
Cr -C!L
M^^S
'^•g
CS ' c*-
-CSI
J_o^
f*-
<.J
Ci
_Ci_
J[6d_
^J2 <^^
c> cc;£ I f U cT/
^
*^t>4-
/ t«-
-i^L
-CJL
LO'
J
N
r.f
too
£ ^
O"
_ai.
_lfi,0_ -ira
.-/ cs V /
-CC
J,CQ_
_Jto
pH
ICP
(mL) /OO
-4Cfitoo tea
SAMPLE
MY71T7
Green Water
^
JO SAMPLE
HG Initial (mL)
(mL)
MS
1007157-07
1007157-18
ICP Initial (mL)
•
1007157-05
0072821/22
Batch Number:
Liberty Analytical Corp.
MY71S3-40334
Case/SDG:
CO
Preparation Date:
<.^
C
<-.5
c*c-
c>-
^A
<•
;>iiMi;,V!*-r!:i.'Si'
'IM^^^
mm. Mercury Standards and QC
SO S0.2 S0.5S1 S5 S10 ICV ICB CRI CCV CCB
NOTE'. All standards and QC for metziiry were prepared at the same day as the associated samples. Reter to the attached. Standard/QC Preparation Log, wtth date matching Ihe above preparation date, for preparation method and instruction.
Record of Tempature/Time
Time Hq out water bath: Water Bath Temp In:
£0_ -4f-T"
Waler Bath Temp Out: "TTie presence of the Chemist's/analyst's employee ID number, cr signature, cn this log attests that stnct compliance with the method' s SOP has occurred. Any SOP deviations requires documentation by the chemist/analyst together with the chemist's/analysrs initials and the initials of Ihe lab supervisor and a QA department representative, signffying approval of the deviation,"
• ^ V , 7 ^
S a m p l e V e r i f i c a t i o n Signature:!
This signature conoborates that the sample idenification numbers appearing on the digestion cups are the same as those appearing on the field sample conlainers.
OO
-S£L
Reviewed By: _ Date:
l^Wl
S h a d i n g h a s b e e n a p p l i e d to u n u s e d p o r t i o n s o f t h i s w o r k s h e e t as a s u b s t i t u t e f o r 'Z-out. JCF 120209
MS Reference ICAP: 0.5 mL of ILI^05.3 f^alrtx Spllie
Hot Block Temp Out". Tirre Hg in waler bath:
* R=red, BL=b1ue, Y=yellow, G=green, 0=orange, V=violet, V/=white, CS=colorless, BR=brown, BK=black GY= grey, F=fine, M^medium, C=coarse, CL=clear, CY=cloudy, OP=opaque
'^fy c
Hot Block Terrp In:
HG: L O m L lOOppb H g
•m .
H^v(!g>ft!A»c>'>pqi^oocft
LCS Reference ICAI*: 5.bmLoflCVa367
(3 £.30013
322
o
S t a n d a r d s / Q C P r e p a r a t i o n Log for I C P Metals/Mercury Page 1 of 3 COMPUCHEM a division ofLiberty Analytical Corp. Worksheet I Q (1) 2
REAGENTS SULFURIC ACID (H2SO4) NITRIC ACID (HNO3) POTASSIUM PERMANGANATE (K2vln04) HYDROCHLORIC ACID (HCL) POTASSIUM PERSULFATE (KjSjOs) HYDROGEN PEROXIDE (H2O2)
ENTERED BY: REVIEWED BY:
. p^
v.i2>^y
A)v'7/-C2-C/Q:!.3M
REF#^
MANUFACTURER
LOT#
EXPIRATION DATE
0E20027 0F15001 0D13009 0E20028 0A07004 0F08009
CALEDON JTBAKER JTBAKER CALEDON JTBAKER CALEDON
71645 J12036 J04613 72420 H44465 72923
05/15 06/15 04/15 05/15 11/12 05/11
0925409 0935232 540 0405 0307 1004722 0934323 0934202 0911221 1015809 0508
09/11/10 12/10/10 02/24/15 05/17/15 05/17/15 02/18/11 12/15/10 12/10/10 12/05/10 06/07/11 05/17/15
STANDARDS HIGH PURITY XCL 20R 0B26007 HIGH PURITY XCLLCS lOXR 9L15003 ERA PPT (540) ERA OB24007 EPA LCS (0405) EPA 0E20016 ICV-1 (0307) EPA 0E20013 ILM05.3 MATRIX SPIKE HIGH PURITY 0B23010 SILVER (Ag) lOOppm HIGH PURITY 9L15009 HIGH PURITY 9L21002 TCLP 500 ARSENIC (As) lOOOppm HIGH PURITY 9F17001 MERCURY (Hg) 20ppm HIGH PURITY 0F16001 ICV-5 (0508) Hg EPA 0E20020 Ref#=Logbook ID, Page number, and item number from Materials Receipt Log Standard Lot Number consist of standard ID, date prepared, and initials of preparer Pb lOOOppm 9F17005 HIGH PURITY STANDARD SOLUTIONS PREPARED BY:
Case/SDG;
/JcT^
fllbif^J^
(uUr^
^
0831553 DATE:
12/05/10 rt7--?9-t.o
DATE: OJ>2^^V-10_ DATE;'?-a'?-^<3
The presence ofthe Chemist's/Analyst's employee ID number, or signature, on this worksheet attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials ofthe lab supervisor and a QA department representative, signifying approval ofthe deviation. 12/03/07:RM
CNJ CO
323
S t a n d a r d s / Q C P r e p a r a t i o n Log for I C P Metals/Mercury Page 2 of 3 COMPUCHEM a division ofLiberty Analytical Corp. Worksheet IQ (1) 2 STANDARD LOT NUMBER^ Hg lOOppb-07-29-10-DD
Case/SDG:
^ V ^ ' 5 3 - t o 3:VH
PREPARATION INSTRUCTIONS Place in a lOOmL volumetric flask: O.SmL of 20ppm Hg stock solution 2.5mL of concentrated HNO3 Baker instra-analyzed Trace Metals grade or equivalent Dilute to lOOmL volume with reagent water (PREPARE DAILY) Place in a 1 OOOmL Erlenmeyer to a re-pipettor bottle (PREPARE AS NEEDED)
K2S2O8-07-01-10-DD Potassium Persulfate Kmn04- 07-14-10-DD Potassium Permanganate
Place in a 2000mL volumetric flask: lOO.Og of Kmn04 Baker instra-analyzed Trace Metals grade or equivalent Dilute to 2000mL witli reagent water (PREARE AS NEEDED)
HNO3- 07-27-10-DD Nitric Acid
Place in a 2000mL volumetric flask: SOOmL of Deionized water 1 OOOmL of concentrated HNO3 Baker instra-analyzed Trace Metals grade or equivalent Dilute to 2000mL with reagent water (PREPARE AS NEEDED)
HCI- 07-26-10-DD Hydrochloric Acid
Place in a 2000mL volumetric flask: SOOmL of Deionized water 1 OOOmL of concentrated HCI Baker instra-analyzed Trace Metals grade or equivalent Dilute to 2000mL with reagent water (PREPARE AS NEEDED)
Aqua Regia- 07-27-10-NB
Place in a 1 OOOmL container: 600mL of Concentrated HCL 200mL of Concentrated HN03 (PREPARE AS NEEDED)
RefW=Logbook ID, Page number, and item munber from Materials Receipt Log ^Standard Lot Number consist of standard ID, date prepared, and initials of preparer STANDARD SOLUTIONS PREPARED BY: ENTERED BY: REVIEWED
BY:
(iSbsCiiJy^—
J> ^ V 1^
(IsUf^J^
DATE: 0-7 --»qKQ DATE: c? - ^ q - i o DATE:
7 - 3.'=i'yo
The presence of the Chemist's/Analyst's employee ID number, or signattire, on this worksheet attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the Initials of the lab supervisor and a QA department representative, signifying approval of the deviation. 12/03/07 :RM
CN CO
324
S t a n d a r d s / Q C P r e p a r a t i o n Log for I C P Metals/Mercury Page 3 of 3 COMPUCHEM a division ofLiberty Analytical Corp. Worksheet IQ (1) 2
STANDARD LOT NUMBERS ICV-5-07-29-10-DD SO/ICB/CCB- 07-29-10-DD S0.2/CRA/CRI- 07-29-10-DD S0.5-07-29-10-DD SI.O-07-29-10-DD S5.0/CCV 07-29-10-DD SIO.O-07-29-10-DD
PREPARATION INSTRUCTIONS
Case/SDG:
/ ^ V 7) s 2 - i o -^^iH
Resultant Analyte Concentration
Pipet into a 300mL BOD Bottle l.OmL of ICV-5 and 99mL of reagent water. Digest according to sample preparation instructions Pipet into a 300mL BOD Bottle lOOmL of reagent water Digest according to sample preparation instructions Pipet into a 300mL BOD Bottle 0.2mL of Hg lOOppb and 99.8mL of reagent water Digest according to sample preparation instructions Pipet into a 300mL BOD Bottle O.SmL of Hg lOOppb and 99.SmL of reagent water Digest according to sample preparation instructions Pipet into a 300mL BOD Bottle l.OmL of Hg lOOppb and 99mL of reagent water Digest according to sample preparation instructions Pipet into a 300mL BOD Bottle S.OmL of Hg lOOppb and 95mL of reagent water Digest according to sample preparation instructions Pipet into a 300mL BOD Bottle lOmL of Hg lOOppb and 90mL of reagent water Digest according to sample preparation instructions
4.0ng/L 0.0|ag/L 0.2|ag/L 0.5|ag/L l.OMg/L 5.0^g/L lO.O^ig/L
Reftf=Logbook ID, Page number, and item number from Materials Receipt Log Standard Lot Number consist of standard ID, date prepared, and initials of preparer STANDARD SOLUTIONS PREPARED BY: ENTERED BY: REVIEWED BY:
{hiu>^y7NL)td4^-^
7^
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DATE: o-?-=>^-i^ DATE:
01-.>^-io
DATE: 7 - J 2 ^ ~ / ^
The presence of the Chemist's/Analyst's employee ID number, or signattire, on this worksheet attests that strict compliance with the method's SOP has occurred Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials of the lab supervisor and a QA department representative, signifying approval of the deviation. 12/03/07:RM
CM CNJ CO
325
CompuChem. a Division of Uberty Analytical Corp. METALS/MERCURY PREPARATION LOG Green Water DATE/Tlt^lE PREPPED
Metals Melhod: ILM05,4 / H W I Mercury Method: 1LM05.4/CW1 Case/SDG:
or Red
MY71S3-40334
Prepared by:
0081015-BLK1
PBW
MB
0081015-BSl
LCSW
LCS
0081015-DUPl
MY71T5D
DUP
0081015-MSl
MY71T5S
MS
10C7157-07RE1
MY71T5
SAMPLE
So So Sa .5o_ So
B-<0-(O /
i3io
CO CM CO
81015
Batch No.:
jXpP
c b /Cl,
s?:>
c-t> 'ir-t
c s ^cu cS / a .
'WMM
cs / c u
C5 ^CL cS /Cl-
cS / c u C5 / c u cS /du-
/X <:2.
^/;
•^/t,.;':
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^aSgj^^i '@iv:lS46M; I g i l J i ^ t j a E ^ J i
S i ^ ^ j j i ggiJMil
j^^Kgii
mmmi^ iiil^i^i^iilgiitllMi^
•rl-irt'^-uS.-:.
¥rA&i^iiysMMM&M^yiyyMAmA
NOT£- All standards and QC for mercury were prepared at lhe same day as the associated samples. Refer to lhe attached Standard/QC Preparation Log. with date matching the above preparation date, for preparation method and instruction.
• R=red, BL=b!ue, Y=yellow, G=green, O=orange. V=violet, W=white, CS=colorless, BR=brown, BK=black, GY=grey F=fine
M=medium
C=coarse
CL=clear,
CY=cloudy,
OP=opaque
tv
*t v ) » f B s y ^ h * yi>P>*afl3S& '>^v
i ^ M r . o.uriiu l o v - i
"The presence of lhe Chemist's/analysl's employee ID number, or signature, on this log attests that strict compliance wriih the method's SOP has occuned Any SOP deviations require documentation by the responsible chemist/analyst together wllti the cnemlst'syanalyst's Initials and me Initials of the lab supervisor and a QA department representative, signifying approval cf the deviation.'
Shading has been applied to unused portions of this worksheet as a substitute for 'Z-out
p^ui;
c>£2ooi3
08/09/06TMG
326
Standards/QC Preparation Log for ICP Metals/Mercury Page 1 of 3 COMPUCHEM a division ofLiberty Analytical Corp. Worksheet IQ (1) 2
REAGENTS SULFURIC ACID (H2SO4) NITRIC ACID (HNO3) POTASSIUM PERMANGANATE (BCMn04) HYDROCHLORIC ACID (HCL) POTASSIUM PERSULFATE (KzSzOg) HYDROGEN PEROXIDE (H2O2)
REF#'
MANUFACTURER
LOT#
EXPIRATION DATE
0E20027 0G09001 ODI3009 0E20028 0A07004 0F08009
CALEDON JT BAKER JT BAKER CALEDON JTBAKER CALEDON
71645 J10038 J04613 72420 H44465 72923
05/15 07/15 04/15 05/15 11/12 05/11
0925409 1021106 540 0405 0307 1004722 0934323 0934202 0911221 1015809 0508
09/11/10 08/02/11 02/24/15 05/17/15 05/17/15 02/18/11 12/15/10 12/10/10 12/05/10 06/07/11 05/17/15
STANDARDS XCL 20R 0B26007 HIGH PURITY 0H03016 HIGH PURITY XCL LCS lOXR ERA PPT (540) ERA OB24007 EPA LCS (0405) 0E20016 EPA 0E20013 EPA ICV-1 (0307) ILM05.3 MATRIX SPIKE 0B23010 HIGH PURITY 9L15009 HIGH PURITY SILVER (Ag) lOOppm 9L21002 HIGH PURITY TCLP 500 HIGH PURITY ARSENIC (As) lOOOppm 9F17001 MERCURY (Hg) 20ppm HIGH PURITY OF16001 ICV-5 (0508) Hg 0E20020 EPA Refif^^Logbcok ID, Page number, and item number from Materials Receipt Log ^Standard Lot Number consist of standard ID, date prepared, and initials of preparer Pb lOOOppm 9F17005 HIGH PURITY STANDARD SOLUTIONS PREPARED BY ^ 3 2 J 2 C ^ i ^ ^ ENTERED BY: REVIEWED BY:
a>I)v:K-^
yi
Case/SDG; MY7JS^-H33S-
0831553
12/05/10
DATE:
^-\0-\C>
DATE:
^-\oyt:>
DATE:
^^^67^
The presence ofthe Chemist's/Analyst's employee ID number, or signature, on this worksheet attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials ofthe lab supervisor and a QA department representative, signifying approval ofthe deviation. 12/03/07:RM
CM CO
327
S t a n d a r d s / Q C P r e p a r a t i o n Log for I C P Metals/Mercury Page 2 of 3 COMPUCHEM a division ofLiberty Analytical Corp. Worksheet IQ (1) 2
Case/SPG: M V T I & 3 - ' 4 6 3 3 ^
STANDARD LOT NUMBER^
PREPARATION INSTRUCTIONS
Hg lOOppb-08-10-10-DD
Place in a lOOmL volumetric flask: 0.5mL of 20ppin Hg stock solution 2.5mL of concentrated HNO3 Baker instra-analyzed Trace Metals grade or equivalent Dilute to lOOmL volume with reagent water (PREPARE DAILY)
K2S2O8-O8-O5-IO-DD Potassium Persulfate
Place in a lOOOmL Erlenmeyer to a re-pipettor bottle (PREPARE AS NEEDED)
Kmji04- 08-05-10-DD Potassium Permanganate
Place in a 2000mL volumetric flask: lOO.Og of Kjmn04 Baker instra-analyzed Trace Metals grade or equivalent Dilute to 2000mL with reagent water (PREARE AS NEEDED)
HNO3- 08-10-10-DD Nitric Acid
Place in a 2000mL volumetric flask: SOOmL of Deionized water lOOOmL of concentrated HNO3 Baker instra-analyzed Trace Metals grade or equivalent Dilute to 2000mL with reagent water (PREPARE AS NEEDED)
HCI- 08-10-10-DD Hydrochloric Acid
Place in a 2000mL volumetric flask: SOOmL of Deionized water 1 OOOmL of concentrated HCI Baker instra-analyzed Trace Metals grade or equivalent Dilute to 2000mL with reagent water (PREPARE AS NEEDED)
Aqua Regia- 08-10-10 - DD
Place in a 1 OOOmL container: 600mL of Concentrated HCL 200mL of Concentrated HN03 (PREPARE AS NEEDED)
RefW=Logbook ID, Page number, and item number from Materials Receipt Log ^Standard Lot Number consist of standard ID, date prepared, and initials of preparer STANDARD SOLUTIONS PREPARED BY
)-CU-^
DATE:
R-lO-lL>
DATE: ^ - 1 0 - 1 0
ENTERED BY: JP- DkjftL-—C REVIEWED BY:
: v-y^z
1
DATE: <^^A<7y^
The presence ofthe Chemist's/Analyst's employee ID number, or signature, on this worksheet attests that strict compliance with the method's SOP has occurred. Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the initials ofthe lab supervisor and a QA department representative, signifying approval ofthe deviation. I2/03/07:RM
CM CO
328
Standards/QC Preparation Log for ICP Metals/Mercury Page 3 of 3 COMPUCHEM a division ofLiberty Analytical Corp. Worksheet IQ (1) 2 STANDARD LOT NUMBER^ ICV-5-08-10-10-DD SO/ICB/CCB- 08-10-10-DD S0.2/CRA/CRI- 08-10-10-DD S0.5-08-10-10-DD Sl.O-08-lO-lO-DD S5.0/CCV08-10-10-DD SIO.O-08-10-10-DD
PREPARATION INSTRUCTIONS
Case/SDG; M^ll 53 - HoBS^-
Resultant Analyte Concentration
Pipet into a 300mL BOD Bottle l.OmL of ICV-5 and 99mL of reagent water. Digest according to sample preparation instructions Pipet mto a 300ml, BOD Bottle lOOmL of reagent water Digest according to sample preparation instructions Pipet into a SOOmL BOD Bottle 0.2mL of Hg lOOppb and 99.8mL of reagent water Digest according to sample preparation instructions Pipet into a 300mL BOD Bottle O.SmL of Hg lOOppb and 99.5mL of reagent water Digest according to sample preparation instructions Pipet into a 300mL BOD Bottle l.OmL of Hg lOOppb and 99mL of reagent water Digest according to sample preparation instructions Pipet into a SOOmL BOD Bottle S.OmL of Hg lOOppb and 95mL of reagent water Digest according to sample preparation instructions Pipet into a SOOmL BOD Bottle lOmL of Hg lOOppb and 90mL of reagent water Digest according to sample preparation instructions
4.0ng/L O.OiAg/L
0.2^g/L 0.5ng/L l.O^g/L 5.0^g/L lO.O^g/L
RefW=Logbook ID, Page number, and item number from Materials Receipt Log ^Standard Lot Number consist of standard ID, date prepared, and initials of preparer
STANDARD SOLUTIONS PREPARED BY:
ENTERED BY: REVIEWED BY:
cU i J J J Z / ^ — C
W> Z ) { / j ^ ' ^ ^ — K
DATE:_^r^Zl^ DATE:
^-)^-iP
DATE: O ^ y o A .
The presence ofthe Chemist's/Analyst's employee ID number, or signature, on this worksheet attests that strict compliance with the method's SOP has occurred Any SOP deviations require documentation by the responsible chemist/analyst together with the chemist's/analyst's initials and the Initials ofthe lab supervisor and a QA department representative, signifying approval ofthe deviation. 12/03/07:RM
(O CM CO
Page 2 of4 From: Origin ID: OAKA (510)788-3801 Tom Fottner Weston Solutions, Inc. 428 13th street 6th Floor, Suite B Oakland, CA94G12
Ebcpress
Ship Date: 329 26JUL10 ActWgtIO.OLB CAD: 5033501/INET3060 Delivery Address Bar Code
J1D20100SZ5022S
SHIP TO:
(919)379-4081
BILL SENDER
Ref# 12767.064.576.1170 Invoice # PO # Have a nice day Dept#
Joan Purdie Liberty Analytical Corporation 501 MADISON AVE
CARY, NC 27513 2 Of 4
^ 7 9 3 7 6108 3714
TUE - 27 JUL Al STANDARD OVERNIGHT
Mstr# 7937 6108 3622 ^201
ORIGINAL
ml
NC SOFA
27513 NC-US
RDU
After printing this label: 1. Use the 'Print' button on this page to print your lahel to your laser or Inkjet printer. 2. Fold the printed page along fhe horizontal line. 3. Place label in shipping pouch and affix It to your shipment so that the barcode portion of the label can be read and scanned. Warning: Use only the printed original label for shipping. Using a photocopy of this label for shipping purposes is fraudulent and could result in additional billing charges, along with the cancellation of your FedEx account number. Use of this system constitutes your agreement to the service conditions in the current FedEx Service Guide, available on fedex.com.FedEx will not be responsible for any claim in excess of $100 per package, whether the result of loss, damage, delay, non-delivery,misdelivery,or misinformation, unless you declare a higher value, pay an additional charge, document your actual loss and file a timely claim.Limitations found in the current FedEx Service Guide apply. Your right lo recover from FedEx for any loss, including intrinsic valueof the package, loss of sales, income interest, profit, attorney's fees, costs, and other forms of damage whether direct, incidental,consequential, or special is limited to the greater of $100 or the authorized declared value. Recovery cannot exceed actual documented loss.Maximum for items of extraordinary value is $500, e.g. jewelry, precious metals, negotiable Instruments and other Items listed in our ServiceGuide. Written claims must be filed within strict time limits, see current FedEx Service Guide.
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7/26/2010
Page 3 of4 From: Origin ID: OAKA (510)788-3801 Tom Fortner Weston Solutions, Inc. 428 13th Street 6th Floor, Suite B Oakland, CA 94612
Fedl2x«
Ship Date: 26JUL 330 10 ActWgt 10.0 LB CAD: 5033501/iNET3060 Delivery Address Bar Code
J10201005I5027S
SHIP TO:
(919)3794081
BILL SENDER
Joan Purdie Liberty Analytical Corporation 501 MADISON AVE
Ref# 12767.064.576.1170 Invoice # PO # Have a nice day Dept#
CARY, NC 27513 3 Of 4
^ ^ 7 9 3 7 6108 3828 Mstr# 7937 6108 3622
TUE - 27 JUL Al STANDARD OVERNIGHT
^201
ORIGINAL NC SOPA
27513 RDU
5aSG1l3fiQ7;9A24
After printing this label: 1. Use the 'Pnnt' button on this page to print your label to your laser or Inkjet printer. 2. Fold the printed page along the horizontal line. 3. Place label in shipping pouch and affix it to your shipment so that the barcode portion of the label can be read and scanned. Warning: Use only the pnnted original label for shipping. Using a photocopy of this label for shipping purposes is fraudulent and could result in additional billing charges, along with the cancellation of your FedEx account number. Use of this system constitutes your agreement to the service conditions in the current FedEx Service Guide, available on fedex.com.FedEx will not be responsible for any claim in excess of $100 per package, whether the result of loss, damage, delay, non-delivery,misdellvery,or misinformation, unless you declare a higher value, pay an additional charge, document your actual loss and file a timely claim.Limitations found In the current FedEx Service Guide apply. Your right to recover from FedEx for any loss, including intrinsic valueof the package, loss of sales, income interest, profit, attorney's fees, costs, and other forms of damage whether direct, incidental,consequential, or special is limited to the greater of $100 or the authorized declared value. Recovery cannot exceed actual documented loss.Maximum for items of extraordinary value Is $500, e.g. jewelry, precious metals, negotiable instruments and other items listed in our ServiceGuide. Written claims must be filed within sthct time limits, see current FedEx Service Guide.
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7/26/2010
Page 1 of4 From: Origin ID: OAKA (510)788-3801 Tom Fortner Weston Solutions, Inc. 428 13th street 6th Floor, Suite B Oakland, CA 94612
FedM,
Ship Date: 26JUL10 331 ActWgtIO.OLB CAD: 5033501/1NET306D Delivery Address Bar Code
J1020iaD57S0;25
SHIP TO:
(919)379-4081
BILL SENDER
Joan Purdie Liberty Analytical Corporation 501 MADISON AVE
Ref# 12767.064.576.1170 Invoice # PO # Have a nice day Dept#
CARY, NC 27513 1of4
^ 7 9 3 7 6108 3622
TUE - 27 JUL Al STANDARD OVERNIGHT
## MASTER ##
ORIGINAL
riljirirli i.riJIril
MN'
NC SOPA
27513 RDU
5BflG1i380Tj1A?4
After printing this label: 1. l.lse the 'Print' button on this page to print your label to your laser or in.kjet printer. 2. Fold the printed page along the horizontal line. 3. Place label in shipping pouch and affix it to your shipment so that the barcode portion of the label can be read and scanned. Warning: Use only the printed original label for shipping. Using a photocopy of this label for shipping purposes is fraudulent and could result in additional billing charges, along with the cancellation of your FedEx account number. Use of this system constitutes your agreement to the service conditions in the current FedEx Service Guide, available on fedex.com.FedEx will not be responsible for any claim in excess of $100 per package, whether the result of loss, damage, delay, non-delivery,misdelivery,or misinformation, unless you declare a liigher value, pay an additional charge, document your actual loss and file a timely claim.Limitations found in the current FedEx Service Guide apply. Your right to recover from FedEx for any loss, including intrinsic valueof the package, loss of sales, income Interest, profit, attorney's fees, costs, and other forms of damage whether direct, incidental,consequential, or special is limited to the greater of $100 orthe authorized declared value. I^ecovery cannot exceed actual documented loss.Maximum for items of extraordinary value is $500, e.g. jewelry, precious metals, negotiable instruments and other Items listed in our ServiceGuide. Written claims must be filed within strict time limits, see current FedEx Service Guide.
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332
Page
CompuChem, a Division ofLiberty Analytical Corp.- EPA INORGANIC RECEIVING LOG Client / Account CaseNo: 1 ^ ^ Temp. Blk in cooler? Temperature: •^;A4 Tags? Yes / Custody Seals? F e s j No Intact? fVes /)No
Rec'd Date Courier Airbill No.
^'JX m i^ y O
ms
COOLER REC'D BY: SAMPLE LOGIN: Number of TR's? Return Airbill in Cooler? Yes / Cyanide Samples checked for sulfide^& chlorine? YES / (j^A^
o f e?'
TOCO
Comments:
l7MqiO% ?)?)^ ^ 7 (
ZhijL^ ^ •O^v^ua^^'^jba.. REVIEWED BY: fis^ .. ni^^ijai^ SDG#: Work Order No: ' ] 2 ^ i ^ r ( £ f l l 5 l [iJDl\Sfi I'pn-fQ
InorgReclog.doc-03/01/06
333 W O R K ORDER
Printed: 7/27/2010 4:44:22PM
1007157 COMPUCHEM Client: USEPA Region IX Project: NEW ELM05.4 AES 5-10 ELEM.21 DAY TAT SDG: MY71S3 CASE: 40334
Project Manager: Project Number: Status:
Joan Purdie EPW08067 Received
Report To: USEPA Region IX GARRETT PETERSON 1337 South 46th Street Bldg. 201 Richmond, CA 94804 Phone:510-412-2389 Fax:(510)412-2302
Invoice To: EPA Dana Lloyd Financial Management Center Mail Code MD-32 Research Triangle Park, NC 27711 Phone :Fax: -
Date Due:
08/16/2010 00:00 (20 day TAT)
Received By:
Joan Purdie
Date Received:
07/27/2010 09:15
Logged In By:
Joan Purdie
Date Logged In:
07/27/2010 16:32
J & B Flags?: Metals ND to?
TICS?: Spike Level:
Deliverable:
EDD:
ILM05.4~AES~REPORT Al,Ca,Fe,Mg,K,Na,Hg ONLY-1007157-07 IS QC
Analysis
Due
TAT
Expires
Received
Comments
1007157-01 MY71S3 [Water] Sampled 07/22/2010 14:55 Eastern ILM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/18/201114:55
07/27/2010 09:15
ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
1LM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/18/201114:55
07/27/2010 09:15
1007157-02 MY71S5 IWater) Sampled 07/21/2010 10:00 Eastern ILM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/17/201110:00
07/27/2010 09:15
1LM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/17/201110:00
07/27/2010 09:15
ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
1007157-03 MY71S7 |WaterJ Sampled 07/21/2010 17:15 Eastern ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
ILM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/17/201117:15
07/27/2010 09:15
ILM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/17/201117:15
07/27/2010 09:15
1007157-04 MY71S9 [Waterl Sampled 07/22/2010 17:20 Eastern ILM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/18/201117:20
07/27/2010 09:15
1LM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
1LM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/18/201117:20
07/27/2010 09:15
Page?^33
334 W O R K ORDER
Printed: 7/27/2010 4:44:22PM
1007157 COMPUCHEM Client: USEPA Region IX Project: NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT SDG: MY71S3 CASE: 40334
Project Manager: Project Number: Status:
Joan Purdie EPW08067 Received
Analysis
Expires
Comments
Due
TAT
1007157-05 MY71T1 [Water] Sampled 07/21/2010 17:00 Eastern ILM05.4 - ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/17/2011 17:00
07/27/2010 09:15
ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
ILM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/17/2011 17:00
07/27/2010 09:15
1007157-06 MY71T3 [Water] Sampled 07/21/2010 16:25 Eastern 1LM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/17/201116:25
07/27/2010 09:15
ILM05.4-ICP/AES (TM)
08/16/2010 16:00 20
01/17/201116:25
07/27/2010 09:15
ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
1007157-07 MY71T5 [Water] Sampled 07/21/2010 15:05 Eastern 1LM05.4 ICP/AES MS/MSD Invoice
08/16/2010 16:00 20
QC
07/31/2010 15:05
07/27/2010 09:15
ILM05.4-ICP/AES (TM)
08/16/2010 16:00 20
01/17/201115:05
07/27/2010 09:15
ILM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/17/201115:05
07/27/2010 09:15
ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
ILM05.4 Mercury MS/MSD Invoice
08/16/2010 16:00 20
08/16/2010 15:05
07/27/2010 09:15
1007157-08 MY71T7 [Water] Sampled 07/22/2010 12:15 Eastern ILM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/18/201112:15
07/27/2010 09:15
ILM05.4-ICP/AES (TM)
08/16/2010 16:00 20
01/18/201112:15
07/27/2010 09:15
ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
1007157-09 MY71T9 [Water] Sampled 07/22/2010 13:55 Eastern 1LM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
ILM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/18/201113:55
07/27/2010 09:15
ILM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/18/201113:55
07/27/2010 09:15
1007157-10 MY71W1 [Water] Sampled 07/22/2010 11:45 Eastern ILM05.4 - ICP AES (5-10) Invoice
08/16/2010 16:00
20
01/18/2011 11:45
07/27/2010 09:15
1LM05.4 - ICP/AES (TM)
08/16/2010 16:00
20
01/18/2011 11:45
07/27/2010 09:15
ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
1007157-11 MY71W5 [Water] Sampled 07/21/2010 14:05 Eastern ILM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/17/201114:05
07/27/2010 09:15
ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
ILM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/17/201114:05
07/27/2010 09:15
?age3<«?3
335 W O R K ORDER
Printed: 7/27/2010 4:44:22PM
1007157 COMPUCHEM Client: USEPA Region IX Project: NEW ILM05.4 AES 5-10 ELEM.21 DAY TAT SDG: MY71S3 CASE: 40334
Project Manager: Project Number: Status:
Joan Purdie EPW08067 Received
Analysis
Expires
Comments
Due
TAT
1007157-12 MV71W9 [Water] Sampled 07/21/2010 12:00 Eastern ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
1LM05.4-ICP/>LES (5-10) Invoice
08/16/2010 16:00 20
01/17/201112:00
07/27/2010 09:15
ILM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/17/201112:00
07/27/2010 09:15
1007157-13 MV71X1 [Water[ Sampled 07/21/2010 18:05 Eastern ILM05.4 MERCURY
08/16/2010 16:00
20
08/22/2010 09:15
07/27/2010 09:15
1LM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/17/201118:05
07/27/2010 09:15
1LM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/17/201118:05
07/27/2010 09:15
1007157-14 MY71X3 [Water] Sampled 07/21/2010 08:05 Eastern 1LM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/17/201108:05
07/27/2010 09:15
ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
ILM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/17/201108:05
07/27/2010 09:15
1007157-15 MY71X5 [Water] Sampled 07/23/2010 18:05 Eastern
LOW VOLUME-SOOML PLASTIC
1LM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/19/201118 05
07/27/2010 09:15
ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/201009 15
07/27/2010 09:15
ILM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/19/201118 05
07/27/2010 09:15
1007157-16 MY71X6 [Water] Sampled 07/22/2010 15:25 Eastern ILM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/18/201115:25
07/27/2010 09:15
ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
ILM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/18/201115:25
07/27/2010 09:15
1007157-17 MY71X8 [Water] Sampled 07/22/2010 15:47 Eastern ILM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/18/201115:47
07/27/2010 09:15
1LM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/18/201115:47
07/27/2010 09:15
ILM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09:15
07/27/2010 09:15
1007157-18 MY71Y0 [Water] Sampled 07/22/2010 16:02 Eastern 1LM05.4 - ICP/AES (TM)
08/16/2010 16:00 20
01/18/201116 02
07/27/2010 09:15
1LM05.4 MERCURY
08/16/2010 16:00 20
08/22/2010 09 15
07/27/2010 09:15
1LM05.4-ICP AES (5-10) Invoice
08/16/2010 16:00 20
01/18/201116 02
07/27/2010 09:15
Page3333
336 INTERNAL DIGESTION COC
0072821 Printed: 7/28/2010 3:33:01PM
COMPUCHEM
Prepared using: METALS - HW1
Matrix: Water Client ID
Lab Number
Sample Type
0072821-BLK1
PBW
Blank
0072821-BS1
LCSW
LCS
0072821-DUPl
MY71T5D
Duplicate
0072821-MSl
MY71T5S
Matrix Spike
1007157-01
MY71S3
Sample
1007157-02
MY71S5
Sample
1007157-03
MY71S7
Sample
1007157-04
MY71S9
Sample
1007157-05
MY71T1
Sample
1007157-06
MY71T3
Sample
1007157-07
MY71T5
Sample
1007157-08
MY71T7
Sample
1007157-09
MY71T9
Sample
1007157-10
MY71W1
Sample
1007157-11
MY71W5
Sample
1007157-12
MY71W9
Sample
1007157-13
MY71X1
Sample
1007157-14
MY71X3
Sample
1007157-15
MY71X5
Sample
1007157-16
MY71X6
Sample
1007157-17
MY71X8
Sample
1007157-18
MY71Y0
Sample
u L IIM^QJ^
^ ^ Jtt
g7?-J>'?-rO 19HS Date
Date
^^ejyyf'fl Date. KWK OB.Io.b \ \ ^ \
Date
">
Relinquishei
Date
Relinquished By
Date
334 Page 1 of 1
337 INTERNAL DIGESTION COC
0081015 Printed: 8/10/2010 5:00:56PM
COMPUCHEM
Prepared using: METALS - HW1
Matrix: Water Lab Number
Sample Type
Client ID
0081015-BLKl
PBW
Blank
0081015-BS1
LCSW
LCS
0081015-DUPl
MY71T5D
Duplicate
0081015-MSl
MY71T5S
Matrix Spike
1007157-07R^
MY71T5
Sample
From 0072821 on 8/10/2010 by NSB
D^d\^y\ Relinquished By
xcP s Date
Date C?^.l^>c. (7.-.^ Date
Date
IDA^ Relinquished By
^.\I^.\O
tf:5\
^kZ^ Received By
Date
eived By
Date
335 Page 1 of I
338 INTERNAL DIGESTION COC
0072822 Printed: 7/28/2010 3:32:55PM
COMPUCHEM Matrix: Water
Prepared using: METALS - CW1
Lab Number
Sample Type
Client ID
0072822-BLK1
PBW
Blank
0072822-DUPl
MY71T5D
Duplicate
0072822-MSl
MY71T5S
Matrix Spike
1007157-01
MY71S3
Sample
1007157-02
MY71S5
Sample
1007157-03
MY71S7
Sample
1007157-04
MY71S9
Sample
1007157-05
MY71T1
Sample
1007157-06
MY71T3
Sample
1007157-07
MY71T5
Sample
1007157-08
MY71T7
Sample
1007157-09
MY71T9
Sample
1007157-10
MY71W1
Sample
1007157-11
MY71W5
Sample
1007157-12
MY71W9
Sample
1007157-13
MY71X1
Sample
1007157-14
MY71X3
Sample
1007157-15
MY71X5
Sample
1007157-16
MY71X6
Sample
1007157-17
MY71X8
Sample
1007157-18
MY71Y0
Sample
Cy-pfj-tO 1310 ^linquished By
Date
M&
£i^
07-.39-/0
/"^/Q
Received By ^ Date
Relinquished/By Jished/By
VJKK^—
Relinquished By Relinquished By
Date
Received By Date
Date
Received By -yb-i 0 edBy
Date Date
336 Page 1 of 1
339
6/8/2010
CO CO
Metals Intemal Chain of Custody Sheet
Batch: 0072821
Analysis: ILM05.4 - ICP/AES (TM)
Status: Batched
Matrix
Due Date
Add HNOS to pH<2
Water
8/16/2010
HWI
Add HNOS to pH<2
Water
8/16/2010
3q_1 OOOmL Plastic, cool, HN03
HWI
Add HNOS to pH<2
Water
8/16/2010
07/27/10
3q_1 OOOmL Plastic, cool, HN03
HWI
Add HNOS to pH<2
Water
8/16/2010
07/27/10
3q_1 OOOmL Plastic, cool, HNOS
HWI
Add HNOS to pH<2
Water
8/16/2010
HWI
Add HNOS to pH<2
Water
8/16/2010
Extraction
Clientjd
Received
1007157-01 A
MY71S3
07/27/10
3q_1 OOOmL Plastic, cool, HNOS
HWI
1007157-02 A
MY71S5
07/27/10
3q_1 OOOmL Plastic, cool, HN03
1007157-03 A
MY71S7
07/27/10
1007157-04 A
MY71S9
1007157-05 A
MY71T1
Lab Id
Container
Preservative
1007157-06 A
MY71T3
07/27/10
3q_1 OOOmL Plastic, cool, HNOS
1007157-07 B
MY71T5
07/27/10
3q_1 OOOmL Plastic, cool, HNOS
HWI
Add HNOS to pH<2
Water
8/16/2010
1007157-08 A
MY71T7
07/27/10
3q_1 OOOmL Plastic, cool, HNOS
HWI
Add HNOS to pH<2
Water
8/16/2010
1007157-09 A
MY71T9
07/27/10
3q_1 OOOmL Plastic, cool, HNOS
HW1
Add HNOS to pH<2
Water
8/16/2010 8/16/2010
1007157-10 A
MY71W1
07/27/10
3q_1 OOOmL Plastic, cool, HNOS
HWI
Add HNOS to pH<2
Water
1007157-11 A
MY71W5
07/27/10
3q_1 OOOmL Plastic, cool, HNOS
HWI
Add HNOS to pH<2
Water
8/16/2010
1007157-12 A
MY71W9
07/27/10
3q_1 OOOmL Plastic, cool, HNOS
HWI
Add HNOS to pH<2
Water
8/16/2010
1007157-13 A
MY71X1
07/27/10
Sq_1 OOOmL Plastic, cool, HNOS
HWI
Add HNOS to pH<2
Water
8/16/2010
1007157-14 A
MY71X3
07/27/10
3q_1 OOOmL Plastic, cool, HNOS
HWI
Add HNOS to pH<2
Water
8/16/2010
1007157-15 A
MY71X5
07/27/10
3l_500mL Plastic, cool, HNOS
HWI
Add HNOS to pH<2
Water
8/16/2010
1007157-16 A
MY71X6
07/27/10
Sq_1 OOOmL Plastic, cool, HNOS
HW1
Add HN03 to pH<2
Water
8/16/2010
1007157-17 A
MY71X8
07/27/10
Sq_1 OOOmL Plastic, cool, HNOS
HWI
Add HNOS to pH<2
Water
8/16/2010
1007157-18 A
MY71Y0
07/27/10
Sq_1000mL Plastic, cool, HNOS
HWI
Add HNOS to pH<2
Water
8/16/2010
CMkr^l
Tt^jyosss
Relinquished By
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Relinciuished Bv
,
Date/Time
K-AAi'gyuuu/vWLy fecelvechBy
_±2^r0_08f:^ Date/Time ifyy>q-
lr-2^'t0 02^^ Date/Time
ZIMUAOI^^ Received By
Date/Time rjoo
/Joo
Relinquished By
Date/Time
Date/Time
Relinquished By
Date/Time
Date/Time
Cust Date
340
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ny-id
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341
